Composite material with negative ion releasing function and preparation method thereof
A technology of composite materials and negative ions, which is applied in the field of composite materials and preparation, can solve the problems of difficulty in reducing production costs, cumbersome processes, and time-consuming, etc., and achieve the effects of improved elongation at break, scientific preparation methods, and improved mechanical properties
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Embodiment 1
[0020] The concrete steps of preparation are:
[0021] Step 1, first place tourmaline powder, additives and water in a ball mill (or stir and shear in an emulsifier) for 2 hours; wherein, the weight ratio of tourmaline powder, additives and water is 5:10:3 , the auxiliary agent is polyethylene glycol, and the rotating speed during ball milling is 200r / min (the stirring rotating speed when the emulsifier is stirring and shearing is 5000r / min), to obtain a mixed slurry. Then the mixed slurry was dried at 130° C. for 10 h to obtain a powdery intermediate product.
[0022] Step 2, adding the powdery intermediate product to the polymer reaction monomer for in-situ synthesis, or mixing the powdery intermediate product with the polymer matrix and then placing it in a torque rheometer for melt blending for 30 minutes; wherein, The weight ratio of the auxiliary agent in the powdery intermediate product to the polymer matrix is 10:70, the polymer matrix is polyamide, and the comp...
Embodiment 2
[0024] The concrete steps of preparation are:
[0025] Step 1, first place tourmaline powder, additives and water in a ball mill for ball milling (or stirring and shearing in an emulsifier) for 2.5 hours; wherein, the weight ratio of tourmaline powder, additives and water is 9:8: 10. The auxiliary agent is polyethylene glycol, and the rotational speed during ball milling is 270r / min (the stirring rotational speed during emulsifier stirring and shearing is 5800r / min), to obtain a mixed slurry. Then the mixed slurry was dried at 140° C. for 9.5 hours to obtain a powdery intermediate product.
[0026] Step 2, adding the powdery intermediate product to the polymer reaction monomer for in-situ synthesis, or mixing the powdery intermediate product with the polymer matrix and then placing it in a torque rheometer for melt blending for 31 minutes; wherein, The weight ratio of the auxiliary agent in the powdery intermediate product to the macromolecular matrix is 8:75, and the mac...
Embodiment 3
[0028] The concrete steps of preparation are:
[0029] Step 1, first place tourmaline powder, additives and water in a ball mill for ball milling (or stirring and shearing in an emulsifier) for 3 hours; wherein, the weight ratio of tourmaline powder, additives and water is 13:6:16 , the auxiliary agent is polyethylene glycol, and the rotating speed during ball milling is 330r / min (the stirring rotating speed when the emulsifier is stirring and shearing is 6500r / min), to obtain a mixed slurry. Then the mixed slurry was dried at 150° C. for 9 h to obtain a powdery intermediate product.
[0030] Step 2, adding the powdery intermediate product to the polymer reaction monomer for in-situ synthesis, or mixing the powdery intermediate product with the polymer matrix and then placing it in a torque rheometer for melt blending for 32 minutes; wherein, The weight ratio of the auxiliary agent in the powdery intermediate product to the polymer matrix is 6:82, the polymer matrix is ...
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