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Reclaiming agent, reclaimed rubber prepared therefrom, and preparation method of reclaimed rubber

A technology for reclaimed rubber and rejuvenating agent, applied in recycling technology, plastic recycling, etc., can solve the problems of large Mooney viscosity rebound, difficult to promote, too expensive, etc., achieve small regeneration process, improve operating environment and processing technology Simple and efficient results

Inactive Publication Date: 2013-12-11
CHINA RUBBER RESOURCE REGENERATION QINGDAO
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

Although the De-link regenerant invented abroad can regenerate waste rubber under the action of low temperature and mechanical force, it is difficult to promote it in my country because of its high price and the large rebound of Mooney viscosity in the later stage.

Method used

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  • Reclaiming agent, reclaimed rubber prepared therefrom, and preparation method of reclaimed rubber
  • Reclaiming agent, reclaimed rubber prepared therefrom, and preparation method of reclaimed rubber
  • Reclaiming agent, reclaimed rubber prepared therefrom, and preparation method of reclaimed rubber

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0025] Add 50 kilograms of 20-40 mesh waste tire rubber powder into a 200-liter high-speed mixer, add a composite environmental protection regeneration activator as 250 grams of Pitong-22, 5 kilograms of stearic acid, 100 grams of accelerator D, and 100 grams of Antioxidant BHT, a mixture of 100 grams of manganese dioxide, 6 kilograms of environmentally friendly aromatic oil, a mixture of 250 grams of rosin and 5 kilograms of light calcium carbonate as a processing aid, stirred in a high-speed mixer for 8-12 minutes, and then mixed at a high speed The material in the machine will be discharged when the temperature rises to 120°C due to friction. Put the mixed primary mixture into a mill or extruder, and after 5-8 minutes of pressing, it will become a uniform sheet and become recycled rubber.

[0026] According to the national standard GB / T13460-2008, the performance of the regenerated rubber is tested to obtain that the basic performance of the regenerated rubber in this examp...

Embodiment 2

[0029] Add 50 kg of 20-40 mesh waste tire rubber powder into a 200-liter high-speed mixer, add a compound environmental protection regeneration activator as 250 g of Pitong-22, 5 kg of stearic acid, 100 g of urea, and 100 g of antioxidant Agent BHT, the mixture of 100 grams of manganese dioxide, 6 kilograms of plant asphalt, processing aid is the mixture of 250 grams of coumarone resin, 4 kilograms of light calcium carbonate, 1 kilogram of white carbon black, stir 8- After 12 minutes, the temperature of the material in the high-speed mixer is raised to 120°C due to friction, and the material can be discharged. Put the mixed primary mixture into a mill or extruder, and after 5-8 minutes of pressing, it will become a uniform sheet and become recycled rubber.

[0030] According to the national standard GB / T13460-2008, the performance of the regenerated rubber is tested to obtain that the basic performance of the regenerated rubber in this example meets the national A2 standard fo...

Embodiment 3

[0033] Add 50 kilograms of 20-40 mesh waste tire rubber powder into a 200-liter high-speed mixer, add a composite environmental protection regeneration activator as 250 grams of Pitong-22, 5 kilograms of stearic acid, 100 grams of accelerator D, and 100 grams of Antioxidant BHT, a mixture of 100 grams of manganese dioxide, 6 kilograms of pine tar, a mixture of 250 grams of rosin, 4 kilograms of light calcium carbonate, and 0.5 kilograms of carbon black as processing aids, stirred in a high-speed mixer for 8-12 minutes Finally, the material in the high-speed mixer is heated up to 120°C due to friction, and then the material can be discharged. Put the mixed primary mixture into a mill or extruder, and after 5-8 minutes of pressing, it will become a uniform sheet and become recycled rubber.

[0034] According to the national standard GB / T13460-2008, the performance of the regenerated rubber is tested to obtain that the basic performance of the regenerated rubber in this example m...

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Abstract

The invention discloses a reclaiming agent, reclaimed rubber prepared therefrom, and a preparation method of the claimed rubber. The reclaiming agent comprises the following components in parts by mass: 0.5-3 parts of regenerated activator, 5-20 parts of regenerated swelling agent and 1-10 parts of other processing aids. The reclaiming agent, the reclaimed rubber and the preparation method of the claimed rubber have the beneficial effects that crumb rubber powder, used environment-friendly regenerated activator and the swelling agent are uniformly mixed and then added to rubber mixing equipments, such as an open mill and an extruder to reclaim under the condition from room temperature to 50 DEG C in a high-speed mixer in the process of preparing the environment-friendly reclaimed rubber; the regenerating temperature is low, so that bad objectionable odor and staining property of the traditional reclaimed rubber are removed. Compared with the traditional reclaimed rubber, the environment-friendly reclaimed rubber has the advantages that the mechanical property and the processing property are not reduced by a test; chemicals which are not permitted to use are not contained in 'REACH'; the reclaiming agent is simple and efficient in processing technology, and fewer in regenerating procedure; various rubber mixing equipments can carry out regeneration operation.

Description

technical field [0001] The invention belongs to the recycling field of waste rubber, and relates to a regenerant, regenerated rubber prepared by using the regenerant and a preparation method. Background technique [0002] The chemical reaction between the rubber macromolecular chain and the vulcanizing agent such as sulfur, accelerator, etc. makes the chemical cross-linking points between the rubber macromolecular chains change from a linear one-dimensional structure to a three-dimensional space network structure, improving the physical and mechanical properties of the rubber, but cross-linking The combined rubber cannot be naturally degraded for a long time after being discarded, and most of it becomes industrial waste. In the case of high prices, shortage of resources and accelerated deterioration of the environment, it is of great significance to reduce the environmental burden, efficiently recycle waste rubber resources, and realize the green cycle of basic raw material ...

Claims

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Application Information

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IPC IPC(8): C08J11/10C08L17/00
CPCY02W30/62
Inventor 沈梅辛振祥谭钦艳高文廷郭素炎
Owner CHINA RUBBER RESOURCE REGENERATION QINGDAO
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