A preparation method of room temperature high magnetic energy product corrosion resistant sintered NdFeB
A high magnetic energy product, NdFeB technology, applied in inductor/transformer/magnet manufacturing, magnetic objects, magnetic materials, etc., can solve the problems of unfavorable corrosion-resistant sintered NdFeB, affecting the magnetic energy product at room temperature, etc., and achieve grain boundary improvement. Ideal effect, lower melting point of grain boundary, excellent corrosion resistance effect
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Embodiment 1
[0018] 1. Prepare a master alloy ingot, the atomic percentage of which is: Nd: 9.0%, Pr: 3.0%, Fe: 81.5%, B: 6.5%, and use the vacuum induction quick-setting casting technology to prepare the master alloy quick-setting casting.
[0019] 2. After the master alloy quick-setting cast sheet is crushed by hydrogen explosion, add 0.5% of gasoline, 3.0% of special antioxidant and 0.1% of lubricant to the powder, mix well, and place in the air flow It is further crushed in the mill to make a powder with an average particle size of 5 μm.
[0020] 3. The powder made by jet milling is placed on the rolling sample stage of the magnetron sputtering equipment used for powder particle coating. Select the alloy target, its atomic percentage composition is: Co: 60%, Al: 20%, Ga: 20%; after the magnetron sputtering system is vacuumed, the target material is sputtered on the rolling sample stage in an argon atmosphere On the powder falling with gravity, the average thickness of the sputtered la...
Embodiment 2
[0025] 1. Prepare a master alloy ingot, the atomic percentage of which is: Nd: 13.5%, Fe: 80.2%, B: 6.3%, and use the vacuum induction quick-setting casting technology to prepare the master alloy quick-setting casting.
[0026]2. After the master alloy quick-setting cast sheet is crushed by hydrogen explosion, add 1.0% of gasoline, 0.5% of special antioxidant and 0.05% of lubricant to the powder, mix well, and place in the air flow It is further crushed in the mill to make a powder with an average particle size of 4 μm.
[0027] 3. The powder made by jet milling is placed on the rolling sample stage of the magnetron sputtering equipment used for powder particle coating. Select the alloy target material, its atomic percentage composition is: Co: 20.0%, Al: 40.0%, Ga: 20.0%, Cu: 10.0%, Nb: 10.0%; The target material components are sputtered on the powder falling with gravity in the rolling sample stage, and the average thickness of the sputtered layer on the surface of the powd...
Embodiment 3
[0032] 1. Prepare a master alloy ingot, the atomic percentage of which is: Nd: 12.5%, Fe: 80.8%, B: 6.7%, and use the vacuum induction quick-setting casting technology to prepare the master alloy quick-setting casting.
[0033] 2. After the master alloy quick-setting cast sheet is crushed by hydrogen explosion, add 1.0% of gasoline, 1.5% of special antioxidant and 0.1% of lubricant to the powder, mix well, and place in the air flow It is further crushed in the mill to make a powder with an average particle size of 3 μm.
[0034] 3. The powder made by jet milling is placed on the rolling sample stage of the magnetron sputtering equipment used for powder particle coating. Select the alloy target, its atomic percentage composition is: Co: 20.0%, Al: 60.0%, Cu: 10.0%, Nb: 5.0%, Ga: 5.0%; The target material components are sputtered on the powder falling with gravity in the rolling sample stage, and the average thickness of the sputtered layer on the surface of the powder is 10nm....
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