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Method for preparing waterproof, antifouling, environment-friendly and flame retardant insulation board by using pitchstone beads

A technology of flame-retardant heat preservation and turpentine rock, which is applied to ceramic products, other household utensils, and household utensils. It can solve the problems of short bonding time, flammability, and low ignition point, and achieve the effect of strong anti-aging ability and long life.

Inactive Publication Date: 2015-03-11
SHANDONG UNIV OF TECH
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0002] At present, there are many kinds of insulation boards for walls at home and abroad. Most of the insulation boards are processed by organic synthesis methods. Commonly there are phenolic boards, polystyrene boards, extruded boards, cement foam insulation boards, etc. The common feature is that chemical organic materials are Made of raw materials, it has the advantages of light weight, small bulk density, excellent thermal insulation, chemical corrosion resistance, closed-cell hydrophobic structure, no water absorption, toughness, water resistance, fiber toughening, etc. It has crack resistance It can be used for internal and external thermal insulation, and has been widely used in building energy-saving demonstration projects. On the other hand, since organic boards are processed from organic matter, in actual construction, bonding Low strength, short bonding time, easy to fall off, difficult to treat and degrade waste, and become white pollution that endangers the atmosphere and groundwater environment. At the same time, harmful substances are gradually released. As an indoor thermal insulation material, it will cause harm to the human body and is flammable during use. , and the ignition point is low, the fire performance is poor, the high temperature produces harmful gases, and with the prolongation of use time, cracks, shrinkage and other phenomena will occur; Very large, high breakage rate, poor thermal conductivity, poor crack resistance, its application has great limitations, the thermal conductivity is 0.07 ~ 0.08W / m.k; the energy saving effect is poor, and the thermal performance needs to be further improved
[0003] The ignition point of the organic board is low, generally at 70-80 degrees, and the current fire-fighting equipment in high-rise buildings cannot reach it, the burning speed is fast, and it is easy to produce toxic gases, causing suffocation and death of people in the room, and causing major property losses in a short time. It is imperative to use internal and external fireproof and thermal insulation materials

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0023] 1. Preparation of raw materials: turpentine rock is spheroidized into spherical particles of 80-150 μm by spheroidizer, and the electric heating tube type air-suction vertically falling puffed micro-bead equipment is used, and the spherical particles of 80-150 μm are preheated at 400°C The intermolecular moisture is removed in the furnace, and the turpentine rock is put into an 800°C puffing furnace. In the puffing furnace, the turpentine rock is heated and expanded, and the expansion volume is controlled at 1:1.1. After sintering at a high temperature of 1400°C, a particle size of 200 ~210μm, density 0.3 g / cm 3 , wall thickness 2μm closed-cell hollow glass microspheres.

[0024] 2. Proportion: 82.5 wt% of closed-cell turpentine hollow glass beads with a particle size of 200-210 μm, 15 wt% of sodium silicate adhesive, and 2.5 wt% of silicone water repellent.

[0025] 3. Spraying and stirring: Spray 15 wt% sodium silicate adhesive and 2.5 wt% silicone water-repellent ev...

Embodiment 2

[0030] 1. Preparation of raw materials: Rosin rock is spheroidized into spherical particles of 80-150 μm by spheroidizer, and electric heating tube type air suction vertical drop puffed micro-bead equipment is used, and spherical particles of 80-150 μm are preheated at 380°C The intermolecular moisture is removed in the furnace, and the turpentine rock is put into an 820°C puffing furnace. In the puffing furnace, the turpentine rock is heated and expanded, and the expansion volume is controlled at 1:1.2. After sintering at a high temperature of 1250°C, a particle size of 220 ~230μm, density 0.25 g / cm 3 , Wall thickness 1.5μm closed-cell hollow glass microspheres.

[0031] 2. Proportion: 88 wt% of closed-cell turpentine hollow glass beads with a particle size of 220-230 μm, 10 wt% of sodium silicate adhesive, and 2.0 wt% of silicone water repellent.

[0032] 3. Spraying and stirring: Spray 10 wt% sodium silicate adhesive and 2.0 wt% silicone water repellent evenly on the surfa...

Embodiment 3

[0037] 1. Preparation of raw materials: turpentine rock is spheroidized into spherical particles of 80-150 μm by spheroidizer, and electric heating tube type air suction vertical drop puffed micro-bead equipment is used, and spherical particles of 80-150 μm are preheated at 360°C The intermolecular moisture is removed in the furnace, and the turpentine rock is put into an 850°C puffing furnace. In the puffing furnace, the turpentine rock is heated and expanded, and the expansion volume is controlled at 1:1.5. After sintering at a high temperature of 1100°C, a particle size of 240 ~250μm, density 0.2 g / cm 3 , wall thickness 1μm closed-cell hollow glass microspheres.

[0038] 2. Proportion: 90 wt% of closed-cell turpentine hollow glass beads with a particle size of 240-250 μm, 8.5 wt% of sodium silicate adhesive, and 1.5 wt% of organic silicon water repellent.

[0039] 3. Spraying and stirring: Spray 8.5 wt% sodium silicate adhesive and 1.5 wt% silicone water repellent evenly on ...

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Abstract

The invention provides a preparation method for making waterproof, anti-fouling, environmental protection, A-level flame-retardant and heat-insulating boards with closed-cell turpentine rock puffed microspheres, including turpentine rock spheroidization treatment, high-temperature expansion sintering, proportioning, mixing, stirring, Briquetting and drying, characterized in that: 80-90wt% closed-cell turpentine hollow glass beads with a particle size of 200-250μm, 8-15wt% sodium silicate adhesive, 1-2.5wt% organosilicon water-repellent, Stir the paste in a mixer for 2 minutes with a water-cement ratio of 0.3-0.4 (W / C), pour it into a test mold, and compact it on an 80-ton press with a compression ratio of 1.8-2:1. After drying, a layer of anti-aging anti-fouling paint is directly sprayed on the outer surface of the insulation board, and the waterproof, anti-fouling, A-class flame retardant, thermal conductivity, and compressive performance tests are carried out.

Description

technical field [0001] The invention relates to a preparation method for making waterproof, anti-fouling, environmental protection, A-level flame-retardant and heat-insulating boards by using closed-cell turpentine puffed microspheres, and belongs to the technical field of heat-insulation materials for interior and exterior walls of buildings. Background technique [0002] At present, there are many kinds of insulation boards for walls at home and abroad. Most of the insulation boards are processed by organic synthesis methods. Commonly there are phenolic boards, polystyrene boards, extruded boards, cement foam insulation boards, etc. The common feature is that chemical organic materials are Made of raw materials, it has the advantages of light weight, small bulk density, excellent thermal insulation, chemical corrosion resistance, closed-cell hydrophobic structure, no water absorption, toughness, water resistance, fiber toughening, etc. It has crack resistance It can be use...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): C04B28/26C04B38/00C04B14/22
Inventor 郭志东郭春瑶
Owner SHANDONG UNIV OF TECH