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Light-storing polyvinyl chloride composite fiber for wig and preparation method

A composite fiber and polyvinyl chloride technology, applied in the field of light-storing artificial filament and its preparation, can solve the problems of poor chemical resistance stability, complicated process and equipment, and high production cost, and achieves good high temperature resistance and water resistance, and high initial luminous brightness. , the effect of satisfying physical properties

Active Publication Date: 2015-09-09
SHANGHAI REBECCA FIBER MATERIAL TECH
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0004] Traditional light-storing fibers are mostly made by coating method, which has poor hand feeling, washing resistance and luminous effect, and the pollution to the environment is serious during use, which will cause damage to the human body
The skin-core composite spinning method has complex processes and equipment, resulting in high production costs, and there are problems with the fastness of the skin-core layer.
Fibers prepared by the blend spinning method have uneven luminescence due to uneven distribution of light-storing materials in the polymer.
Patent CN103184569A discloses a method for manufacturing light storage fibers. In this method, the light storage agent is added through a volumetric powder adding device, mixed with photopolymers, and then extruded by a screw to produce light storage fibers. However, the alkaline earth aluminum used as the light storage agent Salt has poor water resistance, poor chemical stability, and high requirements for raw material purity
Patent CN1107749C discloses a luminescent synthetic fiber and its preparation method. The method is to mix luminescent materials with mixed additives to make luminescent masterbatches and then blend and spin them with polymers. Because the granulation process is involved, the process and equipment are complicated and costly. Higher, and because the wig raw materials have higher requirements, the luminosity needs to be highly uniform, and the masterbatch spinning method is lacking in this aspect

Method used

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0022] In the polyvinyl chloride resin of 100 weight parts, add the chlorinated polyvinyl chloride of 20 weight parts, the thermal stabilizer of 0.5 weight part, the antioxidant of 0.3 weight part, the lubricant of 0.2 weight part join in the mixer and carry out Preliminary mixing; adding an alkaline earth silicate with a particle size of 3 μm in the mixer so that its content in the final light-storing polyvinyl chloride fiber is 20%, then adding 2.0 parts by weight of lubricant and 1.5 parts by weight of coupling agent , mixed at a high speed of 5000 rpm for 15 minutes, and the mixing temperature was 110°C;

[0023] Send the above mixture into a low-speed mixer, keep the temperature at 110°C and mix for 5 minutes, then naturally cool to 65°C and discharge, and send it to the screw extruder, and after metering, melt extrusion, winding, drawing and heat treatment, the final product is The finished product can be used as raw material for wigs. Wherein the melt extrusion tempera...

Embodiment 2

[0025] In the polyvinyl chloride resin of 100 parts by weight, add the chlorinated polyvinyl chloride of 20 parts by weight, the heat stabilizer of 1.0 parts by weight, the antioxidant of 1.0 parts by weight, the lubricant of 0.3 parts by weight joins in the mixer and carries out Preliminary mixing: Adding alkaline earth silicate with a particle size of 5 μm in the mixer so that its content in the final light-storing polyvinyl chloride fiber is 15%, then adding 1.5 parts by weight of lubricant and 1.0 parts by weight of coupling agent , mixed at a high speed of 4500 rpm for 15 minutes, and the mixing temperature was 110°C;

[0026] Send the above mixture into a low-speed mixer, keep the temperature at 110°C and mix for 5 minutes, then naturally cool to 65°C and discharge, and send it to the screw extruder, and after metering, melt extrusion, winding, drawing and heat treatment, the final product is The finished product can be used as raw material for wigs. Wherein the melt ex...

Embodiment 3

[0028] In the polyvinyl chloride resin of 100 parts by weight, add the chlorinated polyvinyl chloride of 20 parts by weight, the heat stabilizer of 2.0 parts by weight, the antioxidant of 1.5 parts by weight, the lubricant of 0.4 parts by weight join in the mixer and carry out Preliminary mixing; adding an alkaline earth silicate with a particle size of 10 μm in the mixer so that its content in the final light-storing polyvinyl chloride fiber is 10%, then adding 1.0 parts by weight of lubricant and 0.75 parts by weight of coupling agent , mixed at a high speed of 3500 rpm for 15 minutes, and the mixing temperature was 110°C;

[0029] Send the above mixture into a low-speed mixer, keep the temperature at 110°C and mix for 5 minutes, then naturally cool to 65°C and discharge, and send it to the screw extruder, and after metering, melt extrusion, winding, drawing and heat treatment, the final product is The finished product can be used as raw material for wigs. Wherein the melt ...

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Abstract

The invention relates to a light-storing polyvinyl chloride composite fiber for a wig and a preparation method thereof. Polyvinyl chloride is adopted as a base material. The light-storing polyvinyl chloride composite fiber mainly comprises the following materials: Eu2<+> and Dy3<+> activated alkine earth silicate, which accounts for 5-20% of total weight of the composite fiber and of which the grain size, and 20 parts of chlorinated polyvinyl chloride added to 100 parts of polyvinyl chloride, wherein the grain size of Eu2<+> and Dy3<+> activated alkine earth silicate is 3-15 microns. The initial luminance is 700-1500mcd / m<2> after the composite fiber is excited for 10 minutes under the illuminance of 1000LX; the composite fiber is fed to a low-speed mixer after adopting sub-step charging and mixing steps, and is metered, melted, extruded, wound, drafted and subjected thermal treatment to be finally prepared into the composite fiber. By adopting the light-storing polyvinyl chloride composite fiber, the Eu2<+> and Dy3<+> activated alkine earth silicate is taken as a light-storing material; the light-storing polyvinyl chloride composite fiber is free of harm to a human body, uniform in light-storing material distribution, good in spinnability of light-storing fiber, high in initial luminance, and long in persistence; a person does not feel discomfort; the requirements for fabricating a wig product can be met by the physical properties.

Description

[technical field] [0001] The invention relates to a light-storage artificial filament and a preparation method thereof, in particular to a light-storage polyvinyl chloride composite fiber for wigs and a preparation method thereof. [Background technique] [0002] Wigs, as a necessary fashion element in life and a must-have consumer product for beauty makeup, have increasingly entered people's daily lives, and increasingly need differentiation and functionalization. The functional upgrade of wig products is fundamentally a Upgrading of wig raw materials. [0003] Polyvinyl chloride fiber is widely used in man-made fibers for hair decoration because of its excellent strength, curl retention and modification properties. Light-storing polyvinyl chloride fiber is a new type of functional fiber. By adding long The afterglow luminescent material has the novel performance of storing light energy and long-term automatic luminescence in the dark. The wig products made to a certain ext...

Claims

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): D01F8/10D01F1/10A41G3/00
Inventor 杨翠平王依民李全民张书军鞠芳英
Owner SHANGHAI REBECCA FIBER MATERIAL TECH
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