Method for extracting low-pesticide-residue ginsenoside from ginsengs
A technology for pesticide residues ginsenosides and ginsenosides is applied in the field of extracting ginsenosides with low pesticide residues. Loss, manageable effects
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Embodiment 1
[0066] 1. Take 500kg of ginseng fibrous roots or branch roots (the content of total ginsenosides is 6.95% by UV detection), cut into 2-3cm sections;
[0067] 2. Put the ginseng section into the extraction tank, add 5000kg of ice water at 0°C (equivalent to 10 times the weight of ginseng), extract for 10 hours, filter, collect the filtrate, and add 3000kg of ice water (equivalent to 10 times the weight of ginseng) to the filter residue. 6 times) for the second extraction, the extraction time is 10h, collect the filtrate, and then add 3000kg ice water (equivalent to 6 times the weight of ginseng) for the third extraction, the extraction time is 10h, filter, and collect the filtrate , combined three filtrates;
[0068] 3. Concentration: Concentrate the filtrate obtained in step 2 under reduced pressure in vacuum, and concentrate it to 10 degrees Baume under the conditions of vacuum -0.1Mpa and concentration temperature of 60°C;
[0069] 4. Extraction: Add an equal volume of wate...
Embodiment 2
[0074] 1. Take 500kg of ginseng fibrous roots or branch roots (the content of total ginsenosides is 6.81% as detected by UV), and cut them into 2-3cm sections;
[0075] 2. Put the ginseng section into the extraction tank, add 4500kg of ice water at 0°C (equivalent to 9 times the weight of ginseng), extract for 11 hours, and filter with suction. Add 3000kg of ice water to the filter residue for the second and third times respectively. Extraction, leaching under the same conditions for 11h, and combining three extracts;
[0076] 3. Concentration: Concentrate the extract under vacuum pressure, vacuum range -0.08MPa, temperature 60°C, and concentrate to 12 Baume degrees;
[0077] 4. Extraction: add an equal volume of water-saturated n-butanol to the concentrated solution for extraction, separate the water phase and n-butanol phase, add an equal volume of n-butanol to the water phase for separation and extraction, separate the two phases, and combine them twice before and after Th...
Embodiment 3
[0082] 1. Take 500kg of ginseng fibrous roots or branch roots (the content of total ginsenosides is 6.97% by UV detection), cut into 2-3cm sections;
[0083] 2. Put the ginseng section into the extraction tank, add 4000kg of ice water at 0°C (equivalent to 8 times the weight of ginseng), extract for 12 hours, filter, collect the filtrate, and add 3000kg of ice water to the filter residue (equivalent to 8 times the weight of ginseng) 6 times) for the second extraction, the extraction time is 10h, collect the filtrate, then add 2500kg of ice water (equivalent to 5 times the weight of ginseng) for the third extraction, the extraction time is 10h, filter, and collect the filtrate , combined three filtrates;
[0084] 3. Concentration: Concentrate the filtrate obtained in step 2 under reduced pressure in vacuum, and concentrate it to 10 degrees Baume under the conditions of vacuum -0.09Mpa and concentration temperature of 50°C;
[0085] 4. Extraction: add an equal volume of water-s...
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