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Uvioresistant type biomass polyester fiber and preparation method thereof

A polyester fiber and biomass technology, which is applied in the field of anti-ultraviolet biomass polyester fiber and its preparation, can solve the problems of consumption, large raw materials and energy, and high production costs, and achieve improved hydrophilicity, enhanced anti-aging, The effect of improving performance

Active Publication Date: 2014-03-26
TIANE CHEM FIBER GROUP CORP BAODING +1
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

The production cost is high, and consumes a lot of raw materials and energy, and generates a lot of by-products

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0044] Step 1: Preparation of Biomass Polyester Chips

[0045] Add 160kg of bio-based 2,5-furandioic acid and 65kg of bio-based ethylene glycol, 8kg of bio-based 1,3-propanediol in the reactor, wherein the component of bio-based ethylene glycol: the quality of ethylene glycol The fraction is 90%, the mass fraction of 1,2-propanediol is 5%, the mass fraction of 1,2-butanediol is 2%, the mass fraction of pentanediol is 2%, and the mass fraction of sorbitol is 1%. The amount of the catalyst was 275 ppm each of titanium dioxide and antimony trioxide, which were 45.65 g, respectively. 46 g of trimethyl phosphate and 69 g of antioxidant 1010 were added. After mixing uniformly, the esterification reaction was carried out at 225° C. under the pressure of 0.343MPa, and the reaction time was 4h. After esterification, the product was transported to the polycondensation kettle, and at the same time, the temperature was raised to 260°C for polycondensation reaction, and the polycondensat...

Embodiment 2

[0051] Step 1: Preparation of Biomass Polyester Chips

[0052] In the reactor, add the bio-based 2 of 166kg, 5-furandioic acid and the bio-based ethylene glycol of 93kg, the bio-based 1,3-propylene glycol of 11kg, wherein the component of bio-based ethylene glycol is: The mass fraction is 99.2%, the mass fraction of 1,2-propanediol is 0.4%, the mass fraction of 1,2-butanediol is 0.2%, the mass fraction of pentanediol is 0.1%, and the mass fraction of sorbitol is 0.1%, The added catalyst was 120 ppm of tetrabutyl titanate, and it was 19.92 g. 52g of trimethyl phosphate was added, and after mixing uniformly, the esterification reaction was carried out at 280° C. and 0.323MP, and the reaction time was 0.5h. After the esterification, the product was transported to the polymerization kettle, and at the same time, the temperature was raised to 290° C. to carry out the polycondensation reaction, and the polycondensation time was 2h. Finally, the all-bio-based polyester is obtained,...

Embodiment 3

[0058] Step 1: Preparation of Biomass Polyester Chips

[0059] Add the bio-based 2 of 166kg in the reactor, and the bio-based ethylene glycol of 5-furandioic acid and 80kg, the bio-based 1,3-propylene glycol of 9kg, wherein the component of bio-based ethylene glycol is: The mass fraction is 95%, the mass fraction of 1,2-propanediol is 2%, the mass fraction of 1,2-butanediol is 1.5%, the mass fraction of pentanediol is 1%, and the mass fraction of sorbitol is 0.5% , the added catalyst is antimony trioxide, 550ppm, 91.3g. 49 g of alkyl phosphoric acid diester and 49 g of antioxidant 168 were added. After mixing evenly, the esterification reaction was carried out at 240° C. under the pressure of 0.443MPa, and the reaction time was 1.5h. After esterification, the product was transported to the polymerization kettle, and at the same time, the temperature was raised to 280° C. to carry out the polycondensation reaction, and the polycondensation time was 5h. Finally, the all-bio-b...

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Abstract

The invention discloses an uvioresistant type biomass polyester fiber and a preparation method of the uvioresistant type biomass polyester fiber. The uvioresistant type biomass polyester fiber is characterized in that the uvioresistant type biomass polyester fiber is prepared from the following raw materials in percentage by weight: 1-5% of uvioresistant type master batches and the balance of biomass polyester chips. The preparation method comprises the step of performing melt spinning on the uvioresistant type master batches and the biomass polyester chips to obtain the uvioresistant type biomass polyester fiber. The bio-based polyester raw material is prepared from bio-based ethylene glycol and bio-based 1, 3-propylene glycol through biological fermentation and purification, the traditional petroleum base ethylene glycol is replaced, environment protection and sustainable development are facilitated, and nano titanium nitride has small grain diameter and large specific surface area and has the efficacy on ultra violent resistance.

Description

technical field [0001] The invention relates to an ultraviolet-resistant biomass polyester fiber and a preparation method thereof, belonging to the technical field of functional fibers. Background technique [0002] With the development of the global economy, the demand for oil is increasing day by day, while oil resources are decreasing day by day, the contradiction between oil supply and demand is increasing day by day, and the war for oil is intensifying. All over the world, efforts are being made to research and explore the use of the inexhaustible biological resources on the earth. Utilizing renewable biomass resources, developing bio-based chemical industry, and replacing petrochemical products is the only way to solve the resource and energy crisis and an important way to sustainable development. Therefore, the development of raw materials that can reduce or replace petroleum is a very important research direction. [0003] Polyester polyester fiber itself has excel...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): D01F6/92D01F1/10C08G63/672C08G63/85
Inventor 王朝生王华平陈向玲
Owner TIANE CHEM FIBER GROUP CORP BAODING
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