Pigment ink for inkjet printing of high fastness textile and preparation method thereof

A technology of inkjet printing and pigment ink, which is applied in the fields of fine chemical industry and material science to achieve good color fastness, good storage stability, and the effect of improving color brilliance

Active Publication Date: 2014-06-04
JIANGSU GEMEIGAO DEV CO LTD
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0004] Although there are many methods for improving the stability and color fastness of textile inkjet printing pigment inks, using branched polymer-coated pigment nanoparticles as colorants (pigment / branched polymer nanocomposite particles), by adding other solvents and There are few reports on the additives used to make inkjet printing soil ink

Method used

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Examples

Experimental program
Comparison scheme
Effect test

example 1

[0017] 15g of branched styrene with a mass fraction of 5%. Maleic anhydride copolymer (branching degree 0.2, molecular weight 8000) was dissolved in 70g acetone, and 16g of 5% mass fraction was added C. I. Pigment Yellow 14 was stirred and mixed, and after 0.5h of high-speed dispersion treatment, 199g of methanol with a mass fraction of 30% was slowly added dropwise, and continued to disperse for 0.5h after the end, and then centrifuged, filtered, washed, dried, and ground to obtain C. I. Pigment yellow 14 / branched styrene-maleic anhydride copolymer nanocomposite particles; 24g with a mass fraction of 24% C. I. Pigment Yellow 14 / branched styrene. Add maleic anhydride copolymer composite particles into deionized water with a mass fraction of 76%, adjust the pH value to 7.2, and disperse at a high speed at 70°C for 1 hour to obtain C. I. Pigment Yellow 14 / branched styrene-maleic anhydride copolymer nanocomposite particle dispersion, ready for use.

[0018] Will account fo...

example 2

[0021]23g of branched styrene with a mass fraction of 15%. Methyl methacrylate copolymer (branching degree is 0.6, molecular weight is 10000) is dissolved in the 85g acetone that mass fraction is 35%, adds the carbon black that 25g mass fraction is 15% and stirs and mixes, starts after 8h high-speed dispersion treatment Slowly add 167g of petroleum ether with a mass fraction of 70%, and continue to disperse for 0.5h after the end, and then centrifuge, filter, wash, dry, and grind to obtain carbon black / branched styrene. Methyl methacrylate copolymer composite particles; 24g of carbon black / branched styrene-methyl methacrylate copolymer composite particles with a mass fraction of 24% were added to 76g of deionized water with a mass fraction of 76%, adjusted The pH value is 8.3, and the carbon black / branched styrene is obtained by high-speed dispersion at 70°C for 1 hour. Methyl methacrylate copolymer nanocomposite particle dispersion.

[0022] The carbon black / branched styren...

example 3

[0025] Dissolve 35g of branched polyamide-ester copolymer (branching degree: 0.28, molecular weight: 25,000) with a mass fraction of 10% in 28g of methanol, and add 36g of a mass fraction with a mass fraction of 10%. I. Pigment blue 15:3 Stir and mix, after 5.4 hours of high-speed dispersion treatment, slowly add 133g of phase separation agent deionized water with a mass fraction of 60%, continue to disperse for 0.5 hours after the end, and then centrifuge, filter, wash, dry, Grind C. I. Pigment blue 15:3 / branched polyamide. Ester copolymer composite particles; 24g C. I. Add pigment blue 15:3 / branched polyamide-ester copolymer composite particles to 76g deionized water, adjust the pH value to 9.1, and disperse at a high speed at 70°C for 1 hour to obtain C. I. Pigment blue 15:3 / branched polyamide. Ester copolymer nanocomposite particle dispersion.

[0026] The C that will account for 40% of the total mass percentage of ink. I. Pigment blue 15:3 / branched polyamide. E...

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Abstract

The invention discloses a pigment ink for inkjet printing of high fastness textile and a preparation method thereof. The ink comprises the following components by mass percent: 30-50% of pigment/branched polymer nano composite particle dispersoid, 10-50% of water soluble cosolvent, 1-5% of non-ionic surfactant, and the balance of deionized water. The preparation method comprises the following steps: sequentially adding the pigment/branched polymer nano composite particle dispersoid, a water-soluble cosolvent and a non-ionic surfactant into the deionized water in proportion, mixing uniformly, stirring by a stirrer at a speed of 500-1000rpm (revolutions per minute) for 20-40 minutes, regulating pH value of the ink to be 7-9, and filtering by virtue of a 500nm microfiltration membrane so as to obtain the coating ink. The ink needs no adhesive, the grain size of the pigment particle in the ink is less than 200nm, and the ink has good storage stability; after jet printing, the textile is baked so as to obtain good color fastness, thus improving the brightness.

Description

technical field [0001] The invention relates to the technical fields of fine chemical industry and material science, in particular to a pigment ink for ink-jet printing of textiles with high fastness and a preparation method thereof. Background technique [0002] Textile inkjet printing technology is a new printing technology that integrates computer network system, digital processing and information system, precision machining and high-quality fine chemical materials. This technology does not require plate making and can be printed directly on fabrics. Printing precision, realize small batch, multi-variety, multi-color printing, has broad development prospects. Ink is an important consumable for textile inkjet printing, and its quality is closely related to the quality of printed fabrics. The research and development of ink is a key factor to promote the progress of textile inkjet printing technology. At present, the ink used for inkjet printing of textiles is still mainly...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C09D11/322D06P5/30D06P1/52
Inventor 陆建辉付少海王玉丰
Owner JIANGSU GEMEIGAO DEV CO LTD
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