ELISA method and kit for detecting classical swine fever virus antibody
An expression vector and in vitro expression technology, applied in the field of molecular biology, can solve the problems of limited production, inability to be used as a differential diagnosis test, high cost, etc., and achieve the effects of safe use, cheap culture medium, and high expression
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Embodiment 1
[0026] Example 1E rnsProtein expression and activity detection in vitro
[0027] 1. Construction of recombinant expression vector
[0028] 1.1 The classical swine fever virus (CSFV) E rns The protein gene was modified, the codons were selectively optimized, and an EcoRI restriction site was added to the 5' end of the fragment, and a NotI restriction site was added to the 3' end of the fragment. Optimized E rns The full-length sequence is shown in SEQ ID No.1, and the sequence is further obtained through artificial synthesis.
[0029] 1.2 Connect the artificially synthesized SEQIDNo.1 and the pGM-T plasmid to establish a reaction system at a ratio of 5:1, then gently add 10 μL of the ligated product to DH5α competent cells, and gently rotate the EP tube to mix the contents , placed on ice for 30 minutes. After heat shock in a water bath at 42°C for 90 sec, quickly transfer to ice, place for 2-3 min, add 800 μL LB liquid medium, and shake at 200 rpm for 45-60 min to revive ...
Embodiment 2
[0047] The establishment of embodiment 2 swine fever virus antibody detection ELISA method
[0048] 1. Establishment of ELISA method for detection of classical swine fever virus antibody
[0049] Determination of Antigen E Using Square Array Titration rns The optimal antigen coating concentration and the dilution of the pig serum to be tested are determined, and the optimal reaction program is determined at the same time. Using the ratio of the OD values of positive and negative serum wells, that is, the P / N value, as an index, a comparative test was carried out on items such as the concentration of the coated antigen, the dilution factor of the serum, the optimum working concentration of the enzyme conjugate, and the reaction time of each step to determine the optimal results. Suitable reaction conditions, the purified recombinant E rns The protein was diluted to an appropriate concentration with 0.025 mol / L carbonate buffer (pH 9.6), coated with a 96-well microtiter plat...
Embodiment 3
[0071] The composition of embodiment 3 test kits
[0072] ELISA plate: coated with E rns For recombinant protein, the coating concentration is 6.25 μg / mL, 50 μL per well;
[0073] Enzyme-labeled secondary antibody: horseradish peroxidase-labeled rabbit anti-pig IgG;
[0074] Chromogenic solution: 3′, 3′, 5′, 5′-tetramethylbenzidine (TMB) single-phase solution
[0075] Stop solution: 2MH 2 SO 4 the solution
[0076] Diluent: washing solution containing 5% skimmed milk
[0077] Washing solution: PBST
[0078] Positive standard: known swine fever positive serum
[0079] Negative standard: known swine fever negative serum
[0080] Note: Negative and positive standard products were purchased from the National Veterinary Microbiology Collection Center.
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