Photocurable adhesive film for organic electronic device seal, organic electronic device, and method for sealing same
一种有机电子器件、粘合剂膜的技术,应用在薄膜/薄片状的粘合剂、粘合剂类型、电固体器件等方向,能够解决有机发光元件损坏等问题,达到确保机械强度、简单工艺、少单件产品生产时间的效果
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Embodiment 1
[0086] Example 1: Formation of Curable Pressure Sensitive Adhesive Films and OEDs
[0087] By polymerizing a press comprising 15 parts by weight of butyl acrylate, 40 parts by weight of methyl ethyl acrylate, 20 parts by weight of isobornyl acrylate, 15 parts by weight of methyl acrylate and 10 parts by weight of hydroxyethyl acrylate Sensitive Adhesive An acrylic polymer having a glass transition temperature of approximately -20°C and a weight average molecular weight of 1,000,000 was prepared.
[0088] With respect to 100 parts by weight of acrylic polymer, by adding 0.2 parts by weight of isocyanate-based cross-linking agent (dicresyl diisocyanate, T-39M), 5 parts by weight of trimethylolpropane type epoxy resin (SR-TMP, SAKAMOTO), 0.25 parts by weight of triaryl sulfonate type cationic photopolymerization initiator (CPI-110A, SAN-APRO Ltd.), and ethyl acetate are used as solvent to prepare coating with 20% solid content cloth solution.
[0089] A 50-μm PET release film c...
Embodiment 2
[0092] All were carried out in the same manner as described in Example 1, except that 10 parts by weight of metal oxide (MgO) was added to the coating solution as a moisture adsorbent with respect to 100 parts by weight of the acrylic polymer. A step of.
Embodiment 3
[0094] All steps were performed as described in Example 1 except that no post-cure (aging process) was used.
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