Synthesis method of damascene metal nanoparticle graphene
A technology of nano-particles and metal embedding, which is applied in the field of one-step synthesis of metal nanoparticles embedded in graphene sheets, achieving excellent performance and simple and easy methods
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Embodiment 1
[0019] Control the mass ratio of dicyandiamide and glucose to be 40:1, control the ratio of carbon in cobalt chloride and glucose to be 0.01%, dissolve the three with deionized water, evaporate to dryness at 75°C, and obtain the intermediate product in Under the condition of nitrogen protection, calcining at 700° C. to obtain the graphene material embedded with cobalt nanoparticles.
[0020] Such as figure 1 As shown, the X-ray diffraction pattern of the graphene material inlaid with the synthesized cobalt nanoparticles, it can be seen that the synthesized nanoparticles can be well aligned with the standard PDF card of Co, which proves that our nanoparticles are Co, not Oxides or carbides of Co.
[0021] Such as figure 2 As shown, the transmission electron microscope photo of the graphene material embedded with cobalt nanoparticles, it can be seen that the particle size distribution of the nanoparticles prepared by us is uniform, and the graphene sheet is relatively thin. ...
Embodiment 2
[0023] Control the mass ratio of dicyandiamide and glucose to be 40:1, control the ratio of carbon in cobalt chloride and glucose to be 0.01%, dissolve the three with deionized water, evaporate to dryness at 75°C, and obtain the intermediate product in Under the condition of nitrogen protection, calcining at 850° C. to obtain a graphene material embedded with cobalt nanoparticles.
Embodiment 3
[0025] Control the mass ratio of dicyandiamide and glucose to be 40:1, control the ratio of carbon in cobalt chloride and glucose to be 0.01%, dissolve the three with deionized water, evaporate to dryness at 75°C, and obtain the intermediate product in Under the condition of nitrogen protection, calcining at 1000° C. to obtain a graphene material embedded with cobalt nanoparticles.
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