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Preparation method of nitrogen doped and graphene loaded Cu-Cu2O nanocomposites

A technology of nanocomposite materials and nitrogen-doped graphene, applied in the field of preparation of nanocomposite materials, can solve problems that have not been reported in the literature, and achieve the effects of easy industrial production, simple preparation methods, simple and safe preparation methods

Active Publication Date: 2014-08-20
NORTHWESTERN POLYTECHNICAL UNIV
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

So far, on nitrogen-doped graphene supported Cu-Cu 2 The research work of O nanocomposites has not been reported in the literature

Method used

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  • Preparation method of nitrogen doped and graphene loaded Cu-Cu2O nanocomposites
  • Preparation method of nitrogen doped and graphene loaded Cu-Cu2O nanocomposites
  • Preparation method of nitrogen doped and graphene loaded Cu-Cu2O nanocomposites

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Experimental program
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Effect test

preparation example Construction

[0031] (1) Preparation of graphite oxide: place the flask in an ice-water bath, pour in an appropriate amount of concentrated sulfuric acid; mix 3g flake graphite powder, 1.5g NaNO 3 Pour into the flask, stir evenly, and then cool for 3h, so that the temperature of the system is 0°C; add 9g KMnO to the mixed solution 4 , stir evenly, and keep the system temperature below 20°C during this period; move the flask into an oil bath, keep the temperature at 35°C for 2 hours, add deionized water, and after 10 minutes, add diluted hydrogen peroxide to obtain a bright yellow solution; filter the reactants, and use Repeated washing with 10% hydrochloric acid and distilled water, suction filtration, and dialyzing the obtained viscous solid until the pH value is close to neutral; drying and grinding the obtained solid to obtain graphite oxide.

[0032] (2) Dispersion of graphene oxide: Weigh 60-100 mg of graphite oxide prepared in step 1, measure 300-500 mL of absolute ethanol, pour it in...

Embodiment 1

[0037] (1) Preparation of graphite oxide: place the flask in an ice-water bath, pour in an appropriate amount of concentrated sulfuric acid; mix 3g flake graphite powder, 1.5g NaNO 3 Pour into the flask, stir evenly, and then cool for 3h, so that the temperature of the system is 0°C; add 9g KMnO to the mixed solution 4 , stir evenly, and keep the system temperature below 20°C during this period; move the flask into an oil bath, keep the temperature at 35°C for 2 hours, add deionized water, and after 10 minutes, add diluted hydrogen peroxide to obtain a bright yellow solution; filter the reactants, and use Repeated washing with 10% hydrochloric acid and distilled water, suction filtration, and dialyzing the obtained viscous solid until the pH value is close to neutral; drying and grinding the obtained solid to obtain graphite oxide.

[0038] (2) Dispersion of graphene oxide: Weigh 80 mg of the graphite oxide prepared in step 1, measure 300 mL of absolute ethanol, pour it into a...

Embodiment 2

[0042] (1) Preparation of graphite oxide: place the flask in an ice-water bath, pour in an appropriate amount of concentrated sulfuric acid; mix 3g flake graphite powder, 1.5g NaNO 3 Pour into the flask, stir evenly, and then cool for 3h, so that the temperature of the system is 0°C; add 9g KMnO to the mixed solution 4 , stir evenly, and keep the system temperature below 20°C during this period; move the flask into an oil bath, keep the temperature at 35°C for 2 hours, add deionized water, and after 10 minutes, add diluted hydrogen peroxide to obtain a bright yellow solution; filter the reactants, and use Repeated washing with 10% hydrochloric acid and distilled water, suction filtration, and dialyzing the obtained viscous solid until the pH value is close to neutral; drying and grinding the obtained solid to obtain graphite oxide.

[0043] (2) Dispersion of graphene oxide: Weigh 80 mg of the graphite oxide prepared in step 1, measure 500 mL of absolute ethanol, pour it into a...

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Abstract

The invention relates to a preparation method of nitrogen doped and graphene loaded Cu-Cu2O nanocomposites. Copper phthalocyanine is used for providing a nitrogen source and a copper source, and the high-heat treatment is performed on mixed powder of the copper phthalocyanine and oxidized graphene in an argon atmosphere, so as to prepare the nitrogen doped and graphene loaded Cu-Cu2O nanocomposites. In the prepared nitrogen doped and graphene loaded Cu-Cu2O nanocomposites, Cu-Cu2O nanoparticles are loaded on nitrogen doped graphene sheets. The preparation method provided by the invention has the advantages of safety and simplicity, the yield is high and the recurrence and the industrial production are easy. The nitrogen doped and graphene loaded Cu-Cu2O nanocomposites which are produced by adopting the preparation method have good application prospects and economic values in aspects of photocatalysis, oxygen catalysis, supercapacitors and the like.

Description

technical field [0001] The invention belongs to a preparation method of nanocomposite materials, in particular to a nitrogen-doped graphene loaded Cu-Cu 2 Preparation method of O nanocomposites. Background technique [0002] Cu-Cu 2 O nanocomposites have special interface structures and electronic properties, low cost, and excellent performance, and have potential applications in the fields of information, catalysis, electronics, and energy storage. Therefore, Cu-Cu 2 O nanocomposites have received extensive attention and research. In 2011, Zhou Bo et al. (Bo Zhou, Hongxia Wang, Zhiguo Liu et al., Enhanced photocatalytic activity of flowerlike Cu 2 O / Cu prepared using solvent-thermal route[J],Materials Chemistry and Physics,126(2011)847-852.) Cu-Cu prepared by solvent thermal route 2 O nanocomposite material, and confirmed that the composite material has a good photocatalytic ability for the degradation of the dye Procean red. However, the solvothermal method it adopts...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): B01J27/24B01J37/16H01G11/30
CPCY02E60/13
Inventor 李贺军罗慧娟付前刚褚衍辉沈庆凉陈凤英
Owner NORTHWESTERN POLYTECHNICAL UNIV
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