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Preparation method of Mosla chinensis volatile oil microcapsules

A technology of volatile oil and Radix japonica, applied in the field of volatile oil processing of Radix Radix et Rhizoma, can solve problems such as damage and loss of functional components of volatile oil of Radix Radix et Rhizoma, and achieve the effects of increasing the scope of application, short testing time, and rounded particles.

Inactive Publication Date: 2014-08-20
NANCHANG UNIV
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0004] During the storage process of the volatile oil of Jiangxiangrui, some volatile and easily oxidized components, when the temperature exceeds a certain range, will cause the loss and damage of the functional components of the Jiangxiangrui volatile oil

Method used

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  • Preparation method of Mosla chinensis volatile oil microcapsules

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Experimental program
Comparison scheme
Effect test

Embodiment 1

[0027] After crushing, Jiangxiang sieves through a 40-mesh sieve, add 10-15 times of water, stir and soak for half an hour; add the volatile oil extractor to boil for 4 hours, collect the volatile oil from the lower end of the measuring device; add anhydrous sodium sulfate to the volatile oil Remove moisture. Prepare a 50°C homogeneous aqueous solution with a ratio of 25% of gum arabic and maltodextrin at a ratio of 5:5, add 12% of the core and wall material ratio of the volatile oil of Rhizoma chinensis, and stir evenly. Pass the emulsion through an ultrasonic cell crusher with a duty cycle of 5s-5s and work 60 times to emulsify the homogeneous emulsion. Stir the water bath at 60 °C for 4 h. The microcapsule powder is dried and collected by a spray dryer. The spray drying inlet air temperature is 220°C, and the outlet air temperature is 120°C.

[0028] Determination of oil content on the surface of microcapsules by ultraviolet spectrophotometry: take a certain concentratio...

Embodiment 2

[0034] After crushing, Jiangxiang sieves through a 40-mesh sieve, add 10-15 times of water, stir and soak for half an hour; add the volatile oil extractor to boil for 4 hours, collect the volatile oil from the lower end of the measuring device; add anhydrous sodium sulfate to the volatile oil Remove moisture. Prepare a 60°C homogeneous aqueous solution with a ratio of 25% of gum arabic and maltodextrin in a ratio of 3:5, add 10% of the core and wall material ratio of the volatile oil of Rhizoma chinensis, and stir evenly. Pass the emulsion through an ultrasonic cell crusher with a duty cycle of 5s-5s and work 40 times to emulsify the homogeneous emulsion. Place in a water bath at 40°C for 4 h while stirring evenly. The microcapsule powder is collected by drying in a spray drying tower. The spray drying inlet air temperature is 180°C, and the outlet air temperature is 104°C. It has been determined that the microencapsulation efficiency of the volatile oil of Jiangxiangrui is...

Embodiment 3

[0036]After crushing, Jiangxiang sieves through a 40-mesh sieve, add 10-15 times of water, stir and soak for half an hour; add the volatile oil extractor to boil for 4 hours, collect the volatile oil from the lower end of the measuring device; add anhydrous sodium sulfate to the volatile oil Remove moisture. Prepare 30% concentration of gum arabic and maltodextrin in a ratio of 4:5 at 60°C and stir it uniformly for later use, add 10% of the core wall material ratio of the volatile oil of fenugreek, and stir evenly. Pass the emulsion through an ultrasonic cell crusher with a duty cycle of 5s-5s and work 50 times to emulsify the homogeneous emulsion. In a water bath at 40°C for 4 h, heating and stirring while in the water bath. The microcapsule powder is collected by drying in a spray drying tower. The inlet air temperature for spray drying is 200°C, and the outlet air temperature is 108°C. It has been determined that the microencapsulation efficiency of the volatile oil of J...

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Abstract

The invention provides a preparation method of Mosla chinensis essential oil microcapsules. The method comprises the following steps: drying Mosla chinensis, crushing, and extracting Mosla chinensis essential oil by adopting a water steam distillation process; preparing a certain concentration of an aqueous solution of Arabic gum and maltodextrin, adding the above Mosla chinensis volatile oil, homogenize-mixing uniformly, and stirring in a water bath at a certain temperature; and carrying out spray drying by using a spray drying instrument to obtain Mosla chinensis volatile oil microcapsule particles. The method has the advantages of simplicity, feasibility, and easy control of preparation conditions; and the obtained microcapsule particles have the advantages of good quality of the Mosla chinensis volatile oil, good thermal stability and dissolving dispersibility, uniformity, good fluidity and special smell of the Mosla chinensis volatile oil. The Mosla chinensis volatile oil capsules can be widely applied in the industries of foods, medicines, cosmetics and the like, and has a wide application range.

Description

technical field [0001] The invention relates to oil processing technology, in particular to the processing of the volatile oil of Jiangxiangrui. Background technique [0002] Herbs ( Herba Moslae ) also known as Banbiansu[ E. ciliata (Thunb) Hyland ], usually refers to the labiatae plant Shixiang ( Mosla chinesis Maxim ) or Jiang Xiangru ( Mosla chinensis "jiangxiangru" ) dry aerial parts. Spicy and sweet in taste, warm in nature, non-toxic. It is recorded in "Famous Doctors", "Picture Herbal Classic", and "Compendium of Materia Medica" in ancient my country. Jiangxiang is an authentic medicinal material in Jiangxi with a long history of cultivation. It is mainly distributed in Xinyu City, Zhangshu City, Fenyi County, Yushui District and other places. In summer, when the stems and leaves are luxuriant and the flowers are in full bloom, choose sunny days to harvest, remove impurities, and dry in the shade. It has the functions of expelling summer heat, promoting dam...

Claims

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Application Information

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IPC IPC(8): C11B9/02B01J13/02
Inventor 聂少平邵灯寅谢明勇
Owner NANCHANG UNIV
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