Ferrite sintered body and ferrite core and coil parts
A technology for ferrite cores and coil components, applied in magnetic materials, electrical components, magnetic objects, etc., can solve the problems of lower Curie temperature and lower magnet properties, and achieve the effect of excellent properties and high reliability
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Embodiment 1
[0050]A ferrite sintered body with various changes in the main component composition and production conditions was produced, and the magnetic permeability and Curie temperature were confirmed. The preparation method of the sample is shown below. First, powders of iron oxide, zinc oxide, nickel oxide, and copper oxide having an average particle diameter of 1 μm were prepared. Then, zinc oxide, nickel oxide, and copper oxide were weighed so as to have the compositions shown in Table 1. Next, the iron oxide was weighed so that it was equivalent to the copper oxide used as the second raw material, and the balance was used as the first raw material.
[0051] Then, after crushing and mixing the iron oxide, zinc oxide and nickel oxide respectively weighed as the first raw material with a ball mill, they were calcined at 750° C. for 2 hours in a reducing atmosphere, and the obtained calcined body was crushed to obtain First raw material. In addition, iron oxide and copper oxide for...
Embodiment 2
[0063] A ferrite sintered body in which the heating rate during firing was variously changed was produced, and the magnetic permeability and mechanical properties were confirmed. In addition, the temperature rise rate at the time of baking of each sample was made into the temperature shown in Table 2, and the preparation method was the same as the sample No. 11 of Example 1 except for that. In Example 1, the rate of temperature increase during firing was 100° C., and Sample No. 30 was the same as Sample No. 11.
[0064] In addition, for the half peak width, the value of half the width between diffraction peaks at which 2θ is 1 / 2 the intensity maximum value of the X-ray diffraction peak intensity of 35° or more and 36° or less is shown in Table 2. In addition, regarding mechanical properties, three-point bending strength was measured in accordance with JISR1601-2008. In addition, the magnetic permeability and the mol% of the main component were obtained by the same method as i...
Embodiment 3
[0069] The average particle size D of the ground after making the re-calcined 50 The relationship between the magnetic permeability and the mechanical properties of the ferrite sintered body with various changes was confirmed. In addition, the average particle diameter D of the recalcination of each sample was 50 It was the size shown in Table 3, and the manufacturing method other than that was the same as that of sample No. 11 of Example 1. The average particle diameter D of the calcining again of embodiment 1 50 It is 0.80 μm, and sample No. 40 is the same as sample No. 11. In addition, the difference between sample No. 42 and sample No. 43 is only the rate of temperature rise during firing.
[0070] About the average particle size D after recalcination 50 , was measured by a laser diffraction scattering method using a MICROTRAC device (MT3300EXII manufactured by Nikkiso). In addition, for each sample, I was obtained from the diffraction pattern obtained by XRD. 3 / I ...
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Abstract
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