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Lycopene microcapsule granules and preparation process thereof

A technology for lycopene and a preparation process, which is applied to the field of lycopene microcapsule particles and the preparation process thereof, can solve the problems of poor fluidity, poor release, and insufficient uniformity of product particles, and achieves improved water solubility, palatability, The effect of maintaining biological activity and good diffusion of cold water

Inactive Publication Date: 2015-03-25
武汉志邦化学技术有限公司
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

For the selection of microcapsule coating materials, leather gelatin or animal gelatin is mostly used in traditional techniques. Although coating can also be completed to a certain extent, and the cost is relatively low, leather gelatin and animal gelatin often contain more Harmful substances such as cadmium, arsenic, and aflatoxin have been unable to meet the current product safety and hygiene standards
In addition, gelatin-coated products have poor fluidity and poor water solubility, especially not conducive to cold water diffusion and poor release, which greatly affects the use effect of the product
[0003] In addition, granulation spray is a commonly used technical method. Spray granulation inevitably involves product coating. The quality of the coating effect mainly depends on the coating material and drying technology. How to disperse the material particles as homogeneously as possible , complete heat and mass transfer in an instant, avoid material sticking or sticking to the wall, and complete drying is a technical problem faced in this field. The combination of spraying and drying technology in the traditional process is relatively simple, resulting in product coating. The stability is poor, and the product particles are not uniform enough
At present, most of the production equipment of lycopene microcapsules cannot be fully dried during the production process due to unreasonable structural design, resulting in defects such as uneven material particles and sticky particles, which affect the product. The quality and efficiency of continuous production, it is difficult to achieve effective recycling of coating components scattered in granulation, sieving, drying and other processes, resulting in a large waste of resources

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0022] (1) Add porous starch, natural VE oil and lycopene crystal powder into sunflower oil, dissolve completely at a temperature of 35°C and drain the oil. Filter the oil drain pipe with a 120-mesh stainless steel screen. Porous starch, natural VE oil, The ratio by weight of lycopene solid powder and sunflower oil to porous starch: natural VE oil: lycopene crystal powder: sunflower oil is 0.5:0.001:0.5:1.

[0023] (2) Add purified water into the emulsification kettle, the weight-number ratio of purified water to lycopene crystal powder is 1:4.5, while the jacket is heating up, press cassava modified starch: corn syrup: trehalose: lycopene crystal powder as 0.5:3.0:0.5:1 weight ratio, feed cassava modified starch, corn syrup, trehalose, stir to dissolve completely, and control the temperature at 40°C; add the lycopene mixture to the emulsification tank, and the temperature in the emulsification tank is 55°C , measure the viscosity, and control it at 30-60 centipoise, control t...

Embodiment 2

[0028] (1) Add porous starch, natural VE oil and lycopene crystal powder to corn oil, dissolve completely at a temperature of 40°C and drain the oil. Filter the oil drain pipe with a 120-mesh stainless steel screen. Porous starch, natural VE oil and tomato The weight ratio of lycopene crystal powder and corn oil to porous starch: natural VE oil: lycopene crystal powder: corn oil is 1:0.01:3:4.

[0029](2) Add purified water into the emulsification tank, the ratio of purified water to lycopene crystal powder is 1:5.0, and the ratio of tapioca modified starch: corn syrup: trehalose: tomato The ratio of lycopene crystal powder is 1: 5.0:1.5:1, feed cassava modified starch, corn syrup, and trehalose, stir to dissolve completely, control the temperature at 50°C, add the lycopene mixture into the emulsification kettle, and the temperature in the emulsification kettle is 55°C , measure the viscosity, control it at 30-60 centipoise, control the temperature at 58°C during the measureme...

Embodiment 3

[0034] (1) Add porous starch, natural VE oil and lycopene crystal powder into sunflower oil, dissolve completely at a temperature of 45°C and drain the oil, filter the oil drain pipe with a 120-mesh stainless steel screen, porous starch, natural VE oil, The weight ratio of lycopene solid powder and sunflower oil is 2:0.001:4:5 for porous starch: natural VE oil: lycopene crystal powder: sunflower oil;

[0035] (2) Add purified water into the emulsification tank, the ratio of purified water to lycopene is 1:5, and the jacket is heated up while the ratio is tapioca modified starch: corn syrup: trehalose: lycopene The ratio of crystal powder is 1.5:5.0:1:1, feed cassava modified starch, corn syrup, trehalose, stir to dissolve completely, control the temperature at 50°C, add the lycopene mixture into the emulsification kettle, the temperature in the emulsification kettle is 58°C, measure Viscosity should be controlled at 30-60 centipoise, the temperature should be controlled at 58°...

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PUM

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Abstract

The invention relates to lycopene microcapsule granules and a preparation process thereof. Lycopene crystal powder, sunflower oil or corn oil, porous starch, oxidized starch, modified cassava starch, corn syrup, trehalose, natural VE oil are used as main raw materials, a process is reasonably improved and optimized to be used for greatly shortening the production time, the entire production process is controlled, the drying is carried out layer by layer and the recycling is carried out step by step. Obtained products are spherical, the surfaces of the products are smooth and trim, the biological activity of the products is kept, the products can be well solved in cold water, the use, storage and transportation are relatively well facilitated, no organic solvent or harmful substance is left, the safety, liquidity, taste and water solubility of the products are greatly improved, and resource waste is reduced. By adopting the process, the yield of the lycopene microcapsule granules is high, and the process is suitable for being used for large scale preparation of the lycopene microcapsule granules, and is used for achieving the continuous mass production and reducing the production cost.

Description

Technical field [0001] The invention involves the production technology field of lycopene microcarbon particles, which specifically involves a kind of lycopene microcarbon particles and their preparation processes. Background technique [0002] In the production process of lycopene microcarbon particles, spray drying and microcapsule coats are the two most critical technical steps, which directly affects the safety, liquidity, taste, and water -soluble of the product.Micro -capsule wall material refers to the shell material used to cover the core material when microcapsule, also known as the capsule material, capsule, shell material.Most of the micro -capsule wall materials are inert polymer, semi -synthetic polymer, and synthetic polymer materials.Among them, natural polymer materials have the advantages of non -toxic, good membrane, good stability, etc., and have more applications, but the mechanical strength is poor and the weight of the raw materials is unstable.Small molecul...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): A23L1/09A23L1/29A23P1/04A23L29/30A23P10/35
CPCA23L3/46A23V2002/00A23V2250/213
Inventor 何同胜关荣荣申永存
Owner 武汉志邦化学技术有限公司
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