Polycarboxylate-based water reducing agent with integrated functions of water reduction and slump retaining
A technology of polycarboxylic acid series and water reducing agent, which is applied in the field of polycarboxylic acid series water reducing agent to achieve the effects of ensuring slump, no slump loss, good dispersibility and water reduction.
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Embodiment 1
[0031] Put 360 g of isopentenol polyoxyethylene ether macromonomer with a molecular weight of 2400 into 180 g of deionized water, stir and dissolve at 60° C., and add 1.40 g of hydrogen peroxide after it is completely dissolved. Dissolve 1.0 g of thioglycolic acid and 0.55 g of vitamin C in 120 g of deionized water, and mix well to obtain liquid A. Mix 33g of acrylic acid, 25g of hydroxyethyl acrylate and 65g of deionized water to obtain liquid B. After adding hydrogen peroxide for 15 minutes, keep the temperature at 60°C, and add liquid A and liquid B dropwise at the same time, wherein liquid A is added dropwise for 2.5 hours, and liquid B is added dropwise for 2 hours. After the dropwise addition, keep the temperature for 1 hour, then lower the temperature to 40°C, add 10g of 40% sodium hydroxide solution by mass fraction, add tap water to adjust the solution concentration to 60%, and obtain the polycarboxylic acid-based water reducer of the present invention.
Embodiment 2
[0033] Put 360g of isopentenol polyoxyethylene ether macromonomer with a molecular weight of 2400 and 5g of sodium methacrylate into 180g of deionized water, stir and dissolve at 60°C, and add 1.40g of hydrogen peroxide after it is completely dissolved. Dissolve 0.5g of mercaptopropionic acid and 0.55g of vitamin C in 120g of deionized water, and mix well to obtain liquid A. Mix 33g of acrylic acid, 35g of hydroxybutyl acrylate and 65g of deionized water to obtain liquid B. After adding the hydrogen peroxide for 15 minutes, keep the temperature at 60°C, and add liquid A and liquid B dropwise at the same time, wherein liquid A is added dropwise for 2 h, and liquid B is added dropwise for 1.5 h. After the dropwise addition, keep the temperature for 1 hour, then lower the temperature to 40°C, add 10g of 40% sodium hydroxide solution by mass fraction, add tap water to adjust the solution concentration to 50%, and obtain the polycarboxylic acid-based water reducer of the present in...
Embodiment 3
[0035] Put 360 g of isopentenol polyoxyethylene ether macromonomer with a molecular weight of 2400 into 200 g of deionized water, stir and dissolve at 60° C., and add 1.60 g of hydrogen peroxide after it is completely dissolved. Dissolve 1.5g of mercaptopropionic acid and 0.55g of vitamin C in 120g of deionized water, and mix well to obtain liquid A. Mix 30g of methacrylic acid, 28g of hydroxypropyl acrylate and 65g of deionized water to obtain liquid B. After adding hydrogen peroxide for 15 minutes, keep the temperature at 60°C, and add liquid A and liquid B dropwise at the same time, wherein liquid A is added dropwise for 2.5 hours, and liquid B is added dropwise for 2 hours. After the dropwise addition, keep the temperature for 1 hour, then lower the temperature to 40°C, add 10g of 40% sodium hydroxide solution by mass fraction, add tap water to adjust the solution concentration to 70%, and obtain the polycarboxylic acid-based water reducer of the present invention.
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