A production process of tube billet alloy cn617 for ultra-supercritical thermal power units
A thermal power unit, ultra-supercritical technology, applied in the direction of improving process efficiency, improving energy efficiency, etc., can solve the problems of unfavorable hot processing of finished ingots, influence, and the range of parameters cannot be specific to actual production, etc.
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Embodiment 1
[0033] The technological measure that embodiment 1, embodiment 2 and embodiment 3 carry out jointly:
[0034] ① Alloy CN617 chemical composition distribution and control;
[0035] ② Calculate the amount of various returned steel and alloy materials required for smelting according to the alloy composition control requirements. Metal nickel, metal cobalt, metal chromium, metal molybdenum, metal aluminum, metal titanium, graphite electrodes and other materials are selected. Among them, the metal nickel and metal cobalt should be pre-treated to remove the surface film; the return material should be melted in advance, and the chemical composition is accurate. The raw materials of the furnace are kept clean and free of oil;
[0036] ③ Vacuumize to ensure that the vacuum degree is ≤10Pa; load the materials into the furnace in batches, and feed the electrochemical materials after loading the first batch of materials;
[0037] ④The charging sequence should follow the pure metal first...
Embodiment 2
[0057] Production of CN617B alloy, furnace number: 14240 170142, crucible capacity: 6 tons, ingot weight: 5448kg.
[0058] ①The composition of CN617 alloy is formulated and controlled according to Table 3;
[0059] ③Vacuumize, from low vacuum to high vacuum (10Pa to 2Pa). During this process, due to the melting and degassing of raw materials, the vacuum fluctuates continuously. Sampling and analysis of gas is used to monitor the gas change in molten steel;
[0060] [④ Loading sequence: Ni plate, metal Cr, Co plate, metal Mo, etc.;
[0061] ⑥After 7 hours of full melting, the full melting temperature is 1510°C;
[0062] ⑧The tapping temperature is 1490℃ for pouring;
[0063] The chemical composition and harvest of each stage are shown in Table 6.
[0064] Table 6%
[0065]
[0066] Finished gas: H: 1.3×10 -6 , O: 10×10 -6 , N: 20×10 -6 .
Embodiment 3
[0068] Production of Ni-Cr19-Co12-Mo9 alloy forging materials, furnace number 12242 210342, crucible capacity: 1 ton, ingot weight 976kg.
[0069] like figure 1 as shown,
[0070] ①Ni-Cr19-Co12-Mo9 alloy composition is formulated and controlled according to Table 2;
[0071] ③Evacuation vacuum degree reaches 8Pa and continuously deflates and degasses to complete melting with the melting of raw materials;
[0072] ④ Loading sequence: Ni plate, master alloy, metal Cr, Mo, Co;
[0073] ⑥Add Ta at the same time as the seasoning after full melting, stir for 20 minutes, and the result of full melting gas is O: 7×10 -6 , N:85×10 -6 , stirring and degassing during the refining process, the gas result O: 10×10 -6 , N:20×10 -6 The chemical composition analysis results of the finished product are shown in Table 7;
[0074] ⑨The pouring process controls the pouring speed, the pouring time is 2min, the pouring temperature is 1480°C, and one electrode is poured,
[0075] Table 7%
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