A Continuous Flow Rotary Shaft Reactor and Its Application
A technology of rotating shafts and reactors, which is applied in chemical/physical/physicochemical fixed reactors, chemical methods for reacting liquids with liquids, chemical methods for reacting liquids with gaseous media, etc., and can solve product purity, Influenced by particle size and distribution, it is not suitable for use by small processing enterprises, and it cannot react with materials, etc., to achieve the effect of simple structure and operation, large specific gravity, and easy precipitation
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Embodiment 1
[0037] A continuous flow rotating shaft reactor, comprising a power unit 2 and a reactor body;
[0038] The power unit 2 is a motor;
[0039] The reactor body includes a shell 1, a jacket 6 and a rotating shaft 5. A jacket 6 is set inside the housing 1, and the jacket 6 surrounds the rotating shaft 5. The space between the rotating shaft 5 and the jacket 6 is The cavity is a reaction space 50;
[0040] A first material inlet 3 is provided on the upper part of the housing 1 close to the power device 2, a second material inlet 9 is provided on the symmetrical lower part, and a product outlet 7 is provided on the upper part of the housing 1 away from the power device 2;
[0041] The rotating shaft 5 is connected to the output shaft of the power unit 2; the rotating shaft 5 is installed horizontally; and the reactor and the power unit are all arranged on the support 15;
[0042] The 5-axis surface of the rotating shaft is smooth;
[0043] A seal 10 is provided between the rotat...
Embodiment 2
[0049] see figure 2 Shown, the application of a kind of continuous flow rotary shaft reactor of the present invention in multiphase flow reaction process, with gas-liquid reaction LiOH and CO 2 Reaction produces Li 2 CO 3 For example:
[0050] The ratio of the length of the rotating shaft to the radius of the cross-section used in the experiment is 10:1, and the rotating shaft reactor with a cavity volume of 50 L puts the LiOH solution in the raw material tank 12, and the solution will be pumped into the tank at 20 L / h with a volume of In the chamber of the 50L rotating shaft reactor, the pH value is adjusted to 9, and the CO 2The gas is passed into the cavity of the rotating shaft reactor, and the speed of the rotating shaft is adjusted to 500 rpm. The gas and liquid are fully contacted under the action of the guide thread of the rotating shaft, and the mixed precipitate is passed into a centrifuge for dehydration and washing, and then passed into a drying tank to adjust...
Embodiment 3
[0052] see figure 2 Shown, the application of a kind of continuous flow rotary axis reactor of the present invention in multiphase flow reaction process, with gas-liquid reaction LiOH and CO 2 Reaction produces Li 2 CO 3 as an example
[0053] The ratio of the length of the rotating shaft to the radius of the cross section used in the experiment is 10:1, and the rotating shaft reactor with a cavity volume of 50L puts the LiOH solution in the raw material tank, and the solution will be pumped into the 50L reactor at a rate of 12L / h by the action of the pump. In the cavity of the rotating shaft reactor, the pH value is adjusted to 10, and at the same time, the CO 2 The gas is passed into the chamber of the rotating shaft reactor, and the speed of the rotating shaft is adjusted to 400rpm. The gas and liquid are fully contacted under the action of the guide thread of the rotating shaft, and the mixed precipitate is passed into a centrifuge for dehydration and washing, and the...
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