A kind of organic-inorganic composite nanofiber membrane filter material and preparation method thereof
A nanofiber membrane and inorganic composite technology, applied in the field of textile materials, can solve the problems of low specific surface area and porosity, difficulty in reaching the nanometer level of fiber diameter, expensive equipment, etc., achieve excellent flexibility and plasticity, and the film forming process is simple and fast , improve the filtering effect
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Embodiment 1
[0055] The dried 1KgPVA- co -PE masterbatch and 4Kg cellulose acetate butyrate (CAB) were uniformly mixed, extruded and granulated in a twin-screw extruder at a temperature of 175°C, and 5Kg of PVA-co-PE / CAB composite material was prepared , and then the composite material is spun by a melt spinning machine to obtain a composite fiber; the composite fiber is refluxed in acetone at 60°C for 72 hours to extract cellulose acetate butyrate, and the composite fiber after extracting cellulose acetate butyrate is subjected to normal temperature Dried to prepare PVA with an average diameter of 200 nm- co - PE nanofibers; 10 g of nanofibers and 1.1 g of calcium carbonate microparticles are dispersed in 1 L of ethanol, emulsified by an emulsifier to form a mixed suspension of nanofibers and calcium carbonate microparticles. at 2 m 2 The upper surface of the 20gsm PP melt-blown nonwoven fabric is coated with a mixed suspension, the coating thickness is 10 μm, and dried at room temperat...
Embodiment 2
[0057] After drying, 1Kg of PP masterbatch and 4Kg of cellulose acetate butyrate (CAB) were uniformly mixed, extruded and granulated in a twin-screw extruder at a temperature of 145°C, and 5Kg of PP / CAB composite material was prepared. Then the composite material is spun by a melt spinning machine to obtain a composite fiber; the composite fiber is refluxed in acetone at 60°C for 72 hours to extract cellulose acetate butyrate, and the composite fiber after extraction of cellulose acetate butyrate is dried at room temperature , to prepare PP nanofibers with PP as the continuous phase and an average diameter of 100 nm; disperse 10 g of nanofibers and 1.1 g of titanium dioxide microparticles in 1 L of ethanol, and emulsify them with an emulsifier to form nanofibers and titanium dioxide microparticles mixed suspension. at 2 m 2 The upper surface of 20gsm PP spunbonded nonwoven fabric is coated with mixed suspension, the coating thickness is 8 μm, and dried at room temperature, an...
Embodiment 3
[0059] After drying, 1Kg of PET masterbatch and 4Kg of cellulose acetate butyrate (CAB) were uniformly mixed, extruded and granulated in a twin-screw extruder at a temperature of 240°C, and 5Kg of PET / CAB composite material was prepared. Then the composite material is spun by a melt spinning machine to obtain a composite fiber; the composite fiber is refluxed in acetone at 60°C for 72 hours to extract cellulose acetate butyrate, and the composite fiber after extraction of cellulose acetate butyrate is dried at room temperature , to prepare PET nanofibers with PET as the continuous phase and an average diameter of 80 nm; disperse 10 g of nanofibers and 1.1 g of activated carbon microparticles in 1 L of ethanol, and emulsify through an emulsifier to form a mixture of nanofibers and activated carbon microparticles Mix the suspension. at 2 m 2 The upper surface of the 40gsm PET melt-blown nonwoven fabric is coated with a mixed suspension, the coating thickness is 4 μm, and dried ...
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