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Comprehensive chemical and physical treatment method of serpentine

A comprehensive treatment, chemical and physical technology, applied in the field of comprehensive chemical and physical treatment of serpentine, can solve the problems of low utilization rate of active ingredients, complicated treatment process, large consumption of raw materials, etc., and achieve superior stability and surface adsorption Strong, large surface energy effect

Active Publication Date: 2015-06-10
于拴全
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  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0017] In order to solve the problems of the existing serpentine treatment process complicated, poor product quality, low utilization rate of active ingredients, large consumption of raw materials, etc., the present invention provides a comprehensive chemical and physical treatment method for serpentine

Method used

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Embodiment Construction

[0030] A comprehensive chemical and physical treatment method for serpentine. After the serpentine is pulverized, calcium fluoride is used as an activator, sodium lauryl sulfate is used as a catalyst, and concentrated sulfuric acid is used to treat the serpentine powder, and the reaction generates gas, liquid and solid. Precipitation; gas ammonification to generate gas-phase white carbon black, liquid continues to separate, remove impurities, add ammonia water to precipitate magnesium, precipitate and roast to decompose to obtain active magnesium oxide, and the solution is crystallized to produce ammonium sulfate fertilizer.

[0031] Specifically include the following steps:

[0032] (1) The raw serpentine ore is crushed until the particle size of the powder is 0.048mm-0.074mm, and the serpentine mineral powder, concentrated sulfuric acid with a concentration of 98%, calcium fluoride, and sodium lauryl sulfate are mixed in a weight ratio of 1 : 2:2:0.1 ratio into the reactor, ...

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Abstract

The invention belongs to the technical field of comprehensive utilization of chemistry and chemical engineering of mineral resources and provides a comprehensive chemical and physical treatment method of serpentine for solving the problems of the existing serpentine treatment process of complicated manufacturing process, poor product quality, low utilization rate of effective components and great raw material consumption. The method comprises the following steps: crushing serpentine; by using calcium fluoride as an activating agent and using lauryl sodium sulfate as a catalyst, treating serpentine powder by using concentrated sulfuric acid, and reacting to generate a gas, liquid and a solid precipitate; ammonifying the gas to generate gas phase white carbon black, further separating the liquid, removing impurities, adding ammonia water to precipitate magnesium, precipitating and roasting to decompose to obtain active magnesium oxide, and crystallizing the solution to produce an ammonia sulfate chemical fertilizer. The serpentine is prepared into three main products, namely gas phase white carbon black, active magnesium oxide and the ammonia sulfate fertilizer, two byproducts, namely gypsum and solid phase iron as well as a kind of metal slag, no waste is produced, the serpentine is developed to the uttermost, and final development products are obtained to the uttermost. The raw materials are fully utilized, and the original components are converted into products with high added values.

Description

technical field [0001] The invention belongs to the technical field of chemical and chemical comprehensive utilization of mineral resources, and in particular relates to a comprehensive chemical and physical treatment method for serpentine. Background technique [0002] Serpentine is a general term for hydrous magnesium-rich silicate minerals, such as antigorite, lizardite, and chrysotile. Their color is generally green, but also light gray, white or yellow. Because they are often green and green like snake skin, hence the name. The structure of serpentine often has curls, like fibers. Such serpentine is often used as asbestos. Both massive and fibrous serpentine are lustrous, massive like wax and fibrous like silk. [0003] Serpentine is a mineral aggregate whose main components are serpentine minerals. Serpentine minerals mainly include chrysotile, scale serpentine and antigorite. They are all magnesium phyllosilicate minerals containing OH, and the general chemical ...

Claims

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Application Information

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IPC IPC(8): C01B33/18C01F5/06C01C1/24
Inventor 于拴全
Owner 于拴全
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