Preparing methods of red raspberry seed extract product and red raspberry polymerization fruit juice and applications thereof
A technology of red raspberry seeds and extracts, applied in the fields of application, food preparation, food science, etc., can solve unresolved red raspberry seeds, which cannot fully maintain nutrients and biological functions, and increase the natural nutrients of red raspberry juice and other issues to achieve the effect of improving drinking value and nutritional value
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[0023] The invention provides a kind of preparation method of red raspberry seed extract, comprises the following steps:
[0024] 1) Crush the red raspberry seeds into powder, soak the crushed red raspberry seeds in 65-75% ethanol solution for 12-24 hours;
[0025] 2) After the treatment in step 1), reflux extraction is carried out, the extract is filtered, the filtered extract is evaporated by a rotary evaporator, and the solvent is recovered to obtain the red raspberry seed extract.
[0026] In a preferred embodiment, the mass of the pulverized red raspberry seeds in step 1) and the added volume of ethanol are 1:10.
[0027] In a preferred embodiment, the reflux temperature in step 2) is 75-85°C, and the reflux extraction time is 3h-5h.
[0028] In a preferred embodiment, it also includes purifying the red raspberry seed extract prepared in step 2).
[0029]In a preferred embodiment, the purification condition is that the solution obtained in step 2) is passed through the ...
Embodiment 1
[0045] Preparation method of red raspberry seed extract:
[0046] 1. Use a crusher to crush the red raspberry seeds into a powder state;
[0047] 2. In the extraction tank, soak the crushed red raspberry seeds with 70% ethanol solution for 12 hours (add the extractant at a ratio of 1:10 (g:ml)), and reflux and extract at 80°C for 3 hours. Filter the extract through a filter;
[0048] 3. Use a rotary evaporator to evaporate the filtered extract, and recover the solvent to obtain the crude extraction mixture of red raspberry seeds;
[0049] 4. Purification of red raspberry seed extract: Pass the mixed liquid of red raspberry seed crude extraction through the resin column at a flow rate of 2BV.h. Until it becomes turbid, the adsorbed red raspberry seed extract is finally eluted with 95% ethanol, and the eluate is collected. Rotary evaporation, solvent recovery, vacuum drying below 70°C for 2 hours, the dried product obtained is the red raspberry seed extract.
Embodiment 2
[0051] Preparation method of red raspberry seed extract:
[0052] 1. Use a crusher to crush the red raspberry seeds into a powder state;
[0053] 2. In the extraction tank, soak the crushed red raspberry seeds with 65% ethanol solution for 24 hours (add the extractant at a ratio of 1:10 (g:ml)), and then reflux and extract at 85°C for 3 hours. Filter the extract through a filter;
[0054] 3. Use a rotary evaporator to evaporate the filtered extract, and recover the solvent to obtain the crude extraction mixture of red raspberry seeds;
[0055] 4. Red raspberry seed extract: pass the mixed liquid of red raspberry seed crude extraction through the resin column at a flow rate of 2BV.h. When the macroporous resin is completely adsorbed, use distilled water to clean the impurities through the resin column until the cleaning water is not turbid. , and finally the adsorbed flavonoids were eluted with 95% ethanol, and the eluate was collected. Rotary evaporation, solvent recovery, ...
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