Preparation process of wet-process superfine modified calcium carbonate

A preparation process and ultra-fine technology, applied in chemical instruments and methods, inorganic compound addition, inorganic pigment treatment, etc., can solve the problems of high production cost, low production efficiency, high oil absorption value, etc., and achieve low production cost and high production efficiency , The effect of low oil absorption value

Inactive Publication Date: 2015-07-01
江西科越科技有限公司
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

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Problems solved by technology

[0003] The fineness of traditional superfine calcium carbonate physical dry milling is below 3000 mesh, which is difficult to refine and cannot meet the requirements of high-end industries.
However, the nano-calcium carbonate product prepared by the calcination method is too fine, has high oil absorption value, insufficient rigidity, and high cost.
In addition, the dry calcination process requires a large amount o

Method used

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  • Preparation process of wet-process superfine modified calcium carbonate
  • Preparation process of wet-process superfine modified calcium carbonate

Examples

Experimental program
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Effect test

Embodiment 1

[0023] Embodiment 1, wet process ultrafine modified calcium carbonate preparation process, is characterized in that the preparation process concrete steps of wet process ultrafine modified calcium carbonate are as follows:

[0024] (1) Clean and screen the calcite ore;

[0025] (2) Coarsely crushing the cleaned and screened calcite;

[0026] (3) Carry out fine crushing on the coarsely crushed calcite;

[0027] (4) Use a mill to dry-grind the finely crushed calcite;

[0028] (5) Classify the calcite powder obtained after dry grinding, and collect 600-mesh fine powder;

[0029] (6) Mix the collected 600-mesh calcite powder with water, wherein the solid content is 70%;

[0030] (7) Add solid content of 6‰ modifier sodium stearate to the slurry obtained in step (6) for modification treatment, then enter wet grinding, add grinding media zirconia microbeads and dispersant sodium polyacrylate to the grinding , the volume ratio of grinding medium to slurry is 1:1.5, and the speed ...

Embodiment 2

[0037] Embodiment 2, wet process ultrafine modified calcium carbonate preparation process, is characterized in that the preparation process concrete steps of wet process ultrafine modified calcium carbonate are as follows:

[0038] (1) Clean and screen the calcite ore;

[0039] (2) Coarsely crushing the cleaned and screened calcite;

[0040] (3) Carry out fine crushing on the coarsely crushed calcite;

[0041] (4) Use a mill to dry-grind the finely crushed calcite;

[0042] (5) Classify the calcite powder obtained after dry grinding, and collect 600-mesh fine powder;

[0043] (6) Mix the collected 600-mesh calcite powder with water, wherein the solid content is 80%;

[0044](7) Add the slurry obtained in step (6) to the modifier sodium stearate with a solid content of 9‰ for modification treatment, and then enter the wet grinding process. During the grinding, add grinding media zirconia microbeads and dispersant sodium polyacrylate, The volume ratio of grinding media to sl...

Embodiment 3

[0051] Embodiment 3, wet process ultrafine modified calcium carbonate preparation process, is characterized in that the preparation process concrete steps of wet process ultrafine modified calcium carbonate are as follows:

[0052] (1) Clean and screen the calcite ore;

[0053] (2) Coarsely crushing the cleaned and screened calcite;

[0054] (3) Carry out fine crushing on the coarsely crushed calcite;

[0055] (4) Use a mill to dry-grind the finely crushed calcite;

[0056] (5) Classify the calcite powder obtained after dry grinding, and collect 600-mesh fine powder;

[0057] (6) Mix the collected 600 mesh calcite powder with water, wherein the solid content is 75%;

[0058] (7) Add a solid content of 12‰ modifier sodium stearate to the slurry obtained in step (6) for modification treatment, and then enter wet grinding, and add grinding media zirconia microbeads and dispersant sodium polyacrylate to the grinding , the volume ratio of the grinding medium to the slurry is 1:...

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Abstract

The invention discloses a preparation process of wet-process superfine modified calcium carbonate. The preparation process comprises the following steps: performing cleaning and screening, rough crushing, fine crushing, dry grinding and grading on calcite ores; collecting fine powder of 600 meshes and preparing slurry with water in such a manner that the solid content is 70%-80%; adding a modifier sodium stearate to the slurry for modification treatment and then performing wet grinding, and adding a grinding medium zirconium oxide microspheres and a dispersant sodium polyacrylate during grinding, wherein the volume ratio of the grinding medium to the slurry is 1: 1.5, and the dosage of the modifier is 0.6%-1.2% of the solid content; and putting the slurry obtained after the wet grinding through a vibrating screen, collecting the obtained wet-process superfine modified calcium carbonate slurry into a slurry barrel for flashing drying, collecting the finished product and packaging. The new preparation process is adopted; the wet grinding-modifying integrated technique and the flashing drying technique are adopted so that the production efficiency is high and the production cost is low; the product has the advantages of small particle size, low oil absorption value, high activity and the like; and the major product quality indices are at the international leading level.

Description

technical field [0001] The invention relates to the technical field of preparation and processing of ultrafine calcium carbonate nano powder, in particular to a preparation process of wet ultrafine modified calcium carbonate. Background technique [0002] Ultrafine calcium carbonate has special application properties due to its small particle size, uniform particle size and high surface activity. It is widely used in various industries such as coatings, plastics, papermaking, and inks. [0003] The traditional superfine calcium carbonate physical dry grinding production fineness is below 3000 mesh, which is difficult to refine and cannot meet the requirements of high-end industries. However, the nano-calcium carbonate product prepared by the calcination method is too fine, has high oil absorption value, insufficient rigidity, and high cost. In addition, the dry calcination process requires a large amount of coal, high production costs, large resource consumption, serious c...

Claims

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Application Information

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IPC IPC(8): C09C1/02C09C3/04C09C3/06C09C3/08C09C3/10D21H17/69
Inventor 仇路陈建平
Owner 江西科越科技有限公司
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