Preparation and release method of a composite inhibitor containing oxidized self-heating temperature-controlled cell coat

A technology of inhibitors and aftercoats, which is applied in mining equipment, earthwork drilling, safety devices, etc., can solve the problems of short inhibitory function time, inability to effectively control spontaneous combustion areas in goafs, and strong fluidity of inhibitors. No toxic and side effects, maintain the inhibitory function for a long time, good dispersion effect

Inactive Publication Date: 2017-04-05
CHINA UNIV OF MINING & TECH
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  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0005] Technical problem: The purpose of this invention is to provide a method for preparing and releasing a composite inhibitor containing oxidized self-heating temperature-controlled cell coat, which solves the problem that the existing inhibitors have strong fluidity, keep the inhibitory function for a short time, and cannot effectively control the goaf Zone Spontaneous Area Problems

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  • Preparation and release method of a composite inhibitor containing oxidized self-heating temperature-controlled cell coat

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preparation example Construction

[0034] The preparation method: first, put the inhibitor, flame retardant, active reinforcing agent, functionalized ionic liquid, and solidified material into the container according to the mass ratio, add water in a specified proportion and stir, and wait to mix evenly; secondly , put the composite barrier compound material into the cooling and cooling process to form low-temperature solidified particles in the mold; at the same time, put the organic polymer temperature-controlled aftercoating material into the container in proportion, and stir it until it is evenly mixed and heated to a molten state ; Finally, put the low-temperature cured inhibitor particles into a specific mold containing the polymer temperature-controlled coating material in the molten state, and the temperature-controlled coating material will solidify when cooled, forming a uniform temperature-controlled coating on the surface of the low-temperature inhibitor particles, and finally forming Composite inhib...

Embodiment 1

[0041] Embodiment 1: The inhibitor includes high water-containing composite inhibitor particles and temperature-controlled coating material and preparation method:

[0042] The high-water-containing composite retardant particles include: chemical retardant, flame retardant, active reinforcing agent, functionalized ionic liquid, solidified material and moisture; its mass percentage is: chemical retardant accounts for 35%, flame retardant Accounted for 13%, active reinforcing agent accounted for 8%, functionalized ionic liquid accounted for %, cured material accounted for 6% and water accounted for 28%;

[0043] Described inhibitor is: calcium chloride, magnesium chloride and ammonium chloride;

[0044] Described flame retardant is: magnesium hydroxide;

[0045] The active reinforcing agent is: aliphatic sodium sulfamate and light calcium carbonate;

[0046] The functionalized ionic liquid is: tributylphosphine diethyl phosphate and tributylphosphine methylsulfate;

[0047] T...

Embodiment 2

[0055] Embodiment 2: The inhibitor includes high water-containing composite inhibitor particles and temperature-controlled coating material and preparation method:

[0056] The high-water-containing composite retardant particles include: chemical retardant, flame retardant, active reinforcing agent, functionalized ionic liquid, solidified material and moisture; its mass percentage is: chemical retardant accounts for 30%, flame retardant 10%, active reinforcing agent 5%, functional ionic liquid 5%, curing material 5% and water 25%;

[0057] Described inhibitor is: water glass and sodium percarbonate;

[0058] Described flame retardant is: magnesium hydroxide;

[0059] The active reinforcing agent is: ash calcium powder;

[0060] The functionalized ionic liquid: functionalized 1-acetate ethyl-3-methylimidazolium borate tetrafluoride;

[0061] Described curing material: dicalcium silicate;

[0062] The temperature-controlling coating material consists of piperic acid, epoxy r...

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Abstract

The invention discloses a preparation method and a release method for a composite inhibition substance with oxidation and self-heating temperature-control secundine, and belongs to the preparation method and the release method of the composite inhibition substance. Water is taken as a solvent, and a composite inhibition substance particle with high water content comprises an inorganic inhibitor, a functional ionic liquid, a flame retardant, an activator and a curing material; temperature-control inhibition substance secundine comprises a composite high polymer oxidation and self-heating material. The composite inhibition substance particle having high water content and containing the oxidation and self-heating temperature-control secundine is dispersed to a mining region; when the mining region is spontaneously heated to a temperature 55 DEG C or less, the composite inhibition substance with high water content is in a good packaging state; when the mining region is spontaneously heated to a temperature of 55-65 DEG C, most temperature-control secundine made of the composite high polymer oxidation and self-heating material is automatically degraded and cracked, so that the composite inhibition substance with high water content inside is released to prevent residual coals in the mining region from spontaneous combustion. The composite inhibition substance with oxidation and self-heating temperature-control secundine has the advantages of good dispersion, strong stability, long inhibition function retaining time and small coal bed inclined angle interference and is capable of automatically degrading, cracking and releasing the inhibitor after spontaneously raising the temperature to a certain temperature.

Description

technical field [0001] The invention relates to a method for preparing and releasing a composite inhibitor, in particular to a method for preparing and releasing a composite inhibitor containing an oxidized self-heating temperature-controlled cell coat. Background technique [0002] my country is not only the country with the largest coal production in the world, but also one of the countries with the most serious spontaneous combustion of coal seams. Every year, the number of coal mine deaths in my country is 200 times that of the United States, more than 10 times that of India, and the death rate per million tons is 10 times that of the world average. According to statistics, mines with spontaneous combustion hazard account for about 51.3% of the key state-owned coal mines in my country, accounting for more than 90% of the total mine fires. Therefore, coal spontaneous combustion in goafs not only poses a major threat to the lives of miners and national property, but also ...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): C09K21/02C09K21/04E21F5/08
Inventor 王凯蒋曙光蒋君仪欧雪梅吴征艳邵昊王亚军张卫清周松
Owner CHINA UNIV OF MINING & TECH
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