A method for large-scale preparation of graphene
A graphene and graphite intercalation technology, applied in the graphene field, can solve problems such as intensified invalid decomposition, hindered diffusion, poor quality and performance of graphene products, etc., to promote effective decomposition reactions, suppress invalid decomposition, and optimize complexation effects Effect
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Embodiment 1
[0065] A method for large-scale preparation of graphene, comprising the following steps:
[0066] a. The graphite intercalation compound powder is added to the composite expansion solution, and then the expansion reaction is carried out under the condition of 20-50 ° C for 2-6 hours to obtain a highly expanded worm-like graphene aggregate suspension, wherein each The processing capacity of graphite intercalation compound for 1 ton of composite expansion liquid is 9-15Kg;
[0067] b, filtering the worm-like graphene aggregate suspension to obtain the worm-like graphene aggregate;
[0068] c, successively use metal ion complexing agent and water to wash the worm-like graphene aggregates, after the metal ion complexing agent washing is completed and after the water washing is completed, the worm-like graphene aggregates need to be filtered, and finally the pH value is obtained. 6-8 worm-like graphene aggregate wet material;
[0069] d. adding the washed vermicular graphene aggr...
Embodiment 2
[0076] A method for large-scale preparation of graphene, comprising the following steps:
[0077] A, graphite intercalation compound powder is added in the composite expansion liquid, then under the condition of 25 DEG C, the expansion reaction is carried out for 3 hours to obtain the highly expanded worm-like graphene aggregate suspension, wherein, every 1 ton of compound expansion The processing capacity of the graphite intercalation compound of the liquid is 9Kg;
[0078] b, filtering the worm-like graphene aggregate suspension to obtain the worm-like graphene aggregate;
[0079] c, successively use metal ion complexing agent and water to wash the worm-like graphene aggregates, after the metal ion complexing agent washing is completed and after the water washing is completed, the worm-like graphene aggregates need to be filtered, and finally the pH value is obtained. 6-8 worm-like graphene aggregate wet material;
[0080] d, adding the wet material of the worm-like graphe...
Embodiment 3
[0089] A method for large-scale preparation of graphene, comprising the following steps:
[0090] A, graphite intercalation compound powder is added in the composite expansion liquid, then under the condition of 35 DEG C, the expansion reaction is carried out for 4 hours to obtain the highly expanded worm-like graphene aggregate suspension, wherein, every 1 ton of compound expansion The processing capacity of the graphite intercalation compound of the liquid is 11Kg;
[0091] b, filtering the worm-like graphene aggregate suspension to obtain the worm-like graphene aggregate;
[0092] c, successively use metal ion complexing agent and water to wash the worm-like graphene aggregates, after the metal ion complexing agent washing is completed and after the water washing is completed, the worm-like graphene aggregates need to be filtered, and finally the pH value is obtained. 6-8 worm-like graphene aggregate wet material;
[0093] d, adding the wet material of the vermicular grap...
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