A kind of flame-retardant sodium-ion battery electrolyte and its application
A sodium-ion battery and electrolyte technology, applied in battery electrodes, secondary batteries, circuits, etc., can solve the problem of less research on flame-retardant electrolytes for sodium batteries, and achieve good electrochemical performance, wide application market, and good flame retardancy performance effect
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Embodiment 1
[0031] The preparation process of methoxy pentafluorocyclotriphosphazene:
[0032] Ethoxypentachlorocyclotriphosphazene was added to 200g of acetonitrile with constant stirring, and 105g of NaF was added. After fluorination at 80°C for 5 hours, distillation was carried out to obtain methoxypentafluorocyclotriphosphazene.
Embodiment 2
[0034] The preparation process of 1-propoxy-pentafluorocyclotriphosphazene:
[0035] Put 8g of hexafluorocyclotriphosphazene in 90ml of chlorobenzene, add the catalyst ferric chloride and 1.6g of sodium propoxide under constant stirring, react for 4 hours at 80°C, carry out vacuum distillation, and obtain the derivative of phosphazene after refining. Compound: 1-propoxy-pentafluorocyclotriphosphazene.
Embodiment 3
[0037] The preparation process of hexaphenoxycyclotriphosphazene:
[0038] Put 34.8g of hexachlorocyclotriphosphazene crystals and hexane in a 500ml three-necked bottle equipped with a stirrer, a thermometer, and a back distillation condenser, stir until it dissolves evenly, and react with 50g of sodium phenoxide at a temperature of 70°C for 5 hours , Distilled and purified to obtain phosphazene derivatives: hexaphenoxycyclotriphosphazene.
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