Cellulose acetate electrostatic-spun film loaded AgCl-Ag catalyst and preparation method and application thereof
A cellulose acetate and electrospinning technology, applied in the direction of physical/chemical process catalysts, chemical instruments and methods, chemical/physical processes, etc., to achieve good practical application value, reduce usage, and cheap and easy-to-obtain raw materials
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Embodiment 1
[0026] (1) Weighing cellulose acetate, using acetone and N,N-dimethylacetamide with a mass ratio of 2:1 as a solvent, configured as a cellulose acetate electrospinning solution with a mass fraction of 12%;
[0027] (2) the cellulose acetate electrospinning solution of step (1) is transferred in the electrospinning equipment, under the condition that the static voltage is 15kv, the receiving distance is 11cm, and the advancing speed of the electrospinning solution is 1ml / h Carry out electrospinning, obtain cellulose acetate electrospinning film;
[0028] (3) Place the cellulose acetate electrospun membrane between two 80ml test tubes, and inject 0.02mol / L AgNO into the two test tubes respectively. 3 solution and NaCl solution, placed in the dark for 72 hours to obtain a cellulose acetate electrospun membrane supported AgCl catalyst;
[0029] (4) washing the AgCl catalyst supported on the cellulose acetate electrospun membrane with deionized water, irradiating with sunlight, an...
Embodiment 2
[0032] (1) Weighing cellulose acetate, using acetone and N,N-dimethylacetamide with a mass ratio of 2:1 as a solvent, configured as a cellulose acetate electrospinning solution with a mass fraction of 15%;
[0033] (2) the cellulose acetate electrospinning solution of step (1) is transferred in the electrospinning equipment, under the condition that the static voltage is 20kv, the receiving distance is 15cm, and the advancing speed of the electrospinning solution is 3ml / h Carry out electrospinning, obtain cellulose acetate electrospinning film;
[0034] (3) Place the cellulose acetate electrospun membrane between two 80ml test tubes, and inject 0.01mol / L AgNO into the two test tubes respectively. 3 solution and NaCl solution, placed in the dark for 72 hours to obtain a cellulose acetate electrospun membrane supported AgCl catalyst;
[0035] (4) washing the AgCl catalyst supported on the cellulose acetate electrospun membrane with deionized water, irradiating with sunlight, an...
Embodiment 3
[0038] (1) Weighing cellulose acetate, using acetone and N,N-dimethylacetamide with a mass ratio of 2:1 as a solvent, configured as a cellulose acetate electrospinning solution with a mass fraction of 14%;
[0039] (2) the cellulose acetate electrospinning solution of step (1) is transferred in the electrospinning equipment, under the condition that the static voltage is 18kv, the receiving distance is 12cm, and the advancing speed of the electrospinning solution is 2ml / h Carry out electrospinning, obtain cellulose acetate electrospinning film;
[0040] (3) Place the cellulose acetate electrospun membrane between two 80ml test tubes, and inject 0.02mol / L AgNO into the two test tubes respectively. 3 solution and NaCl solution, placed in the dark for 12 hours to obtain the AgCl catalyst supported on the cellulose acetate electrospun membrane;
[0041] (4) washing the AgCl catalyst supported on the cellulose acetate electrospun membrane with deionized water, irradiating with sun...
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