Preparation method for environment-friendly stone deruster

A rust remover and stone technology, which is applied in the field of preparation of environmentally friendly stone rust removers, can solve problems such as environmental pollution, stone surface damage, and affect the service life of stone materials, and achieves simple preparation process, improved rust removal performance, and good market prospects. Effect

Active Publication Date: 2015-10-28
江苏凯信环保材料有限公司
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0004] Existing rust removers are easy to damage the surface of the stone w...

Method used

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  • Preparation method for environment-friendly stone deruster

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0017] A preparation method of environment-friendly stone material derusting agent, comprises the following steps:

[0018] (1) In parts by weight, put 51 parts of hydrochloric acid, 3 parts of lauryl polyoxyethylene ether, 7 parts of triethanolamine, 2 parts of zinc stearate and 9 parts of thiourea dioxide in a mixer, and stir at 40 °C for 20 minutes , to obtain mixture 1, wherein the mixer speed is 150 r / min;

[0019] (2) Add 10 parts of hexamethylenetetramine, 1 part of ammonium molybdate, 2 parts of benzotriazole, 1 part of isobornyl acrylate, 2 parts of diphthalate to mixture 1 obtained in step (1). Butyl ester and 1 part of ethylenediaminetetramethylenephosphonic acid were heated to 60°C within 3 minutes, sonicated for 10 minutes, cooled to 40°C, and continued to be sonicated for 10 minutes to obtain mixture 2;

[0020] (3) Put the mixture 2 obtained in step (2) in a blender, and stir at room temperature for 30 minutes to obtain the environmentally friendly stone rust r...

Embodiment 2

[0022] A preparation method of environment-friendly stone material derusting agent, comprises the following steps:

[0023] (1) In parts by weight, put 73 parts of hydrochloric acid, 19 parts of sorbitan fatty acid ester, 18 parts of triethanolamine, 14 parts of zinc stearate and 15 parts of thiourea dioxide in a mixer, and stir at 60°C 40min, obtain mixture one, wherein the stirrer rotating speed is 300 r / min;

[0024] (2) Add 17 parts of hexamethylenetetramine, 6 parts of ammonium molybdate, 8 parts of benzotriazole, 5 parts of isobornyl acrylate, 9 parts of diphthalate to the mixture 1 obtained in step (1). Butyl ester and 7 parts of ethylenediaminetetramethylenephosphonic acid were heated to 80°C within 6 minutes, sonicated for 15 minutes, cooled to 60°C, and continued to be sonicated for 15 minutes to obtain mixture 2;

[0025] (3) Put the mixture 2 obtained in step (2) in a blender, and stir at room temperature for 50 minutes to obtain the environmental-friendly stone r...

Embodiment 3

[0027] A preparation method of environment-friendly stone material derusting agent, comprises the following steps:

[0028] (1) In parts by weight, put 55 parts of hydrochloric acid, 7 parts of sodium dodecylsulfonate, 9 parts of triethanolamine, 4 parts of zinc stearate and 11 parts of thiourea dioxide in a mixer, and stir at 45 °C 25min, obtain mixture one, wherein the mixer speed is 200 r / min;

[0029] (2) Add 11 parts of hexamethylenetetramine, 3 parts of ammonium molybdate, 3 parts of benzotriazole, 2 parts of isobornyl acrylate, and 3 parts of diphthalate to mixture 1 obtained in step (1). Butyl ester and 3 parts of ethylenediaminetetramethylenephosphonic acid were heated to 65°C within 4 minutes, sonicated for 11 minutes, cooled to 45°C, and continued to be sonicated for 12 minutes to obtain mixture 2;

[0030] (3) Put the mixture 2 obtained in step (2) in a blender, and stir at room temperature for 35 minutes to obtain the environmentally friendly stone rust remover, ...

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Abstract

The invention discloses a preparation method for an environment-friendly stone deruster. The preparation method comprises the following steps: placing hydrochloric acid, an emulsifier, triethavolamine, zinc stearate and thiourea dioxide into a stirring machine in parts by weight, and stirring at the temperature of 40-60 DEG C; adding hexamethylenetetramine, ammonium molybdate, benzotriazole, isobornyl acrylate, dibutyl phthalate and ethylene diamine tetramethylene phosphonic acid, heating to 60-80 DEG C within 3-6 min, performing ultrasonic treatment for 10-15 min, cooling to 40-60 DEG C, and continuously performing ultrasonic treatment for 10-15 min; placing the mixture into the stirring machine, and stirring at the ordinary temperature to obtain the environment-friendly stone deruster. The derusting performance of the deruster prepared by the method is improved, and the deruster has no impact on the surface of stone, meanwhile is simple in preparation process, avoids environment pollution, and has an excellent market prospect.

Description

technical field [0001] The invention relates to stone derusting technology, in particular to a preparation method of an environment-friendly stone derusting agent. Background technique [0002] Stone rust remover is to use professional stone chemical cleaning products to clean the natural and acquired rust spots on the surface and shallow surface of the stone, so as to restore the texture, appearance and decorative effect of the stone itself. [0003] The material composition inside the stone contains hematite and pyrite. These iron minerals are oxidized in contact with the air to form ferric oxide (rust), which seeps out through the capillary pores of the stone. At the same time, the stone cannot be used during use. Avoid contact with iron objects. The residues of these iron objects are coated on the surface of the stone and will be oxidized to form rust pollution. [0004] Existing derusting agents are easy to damage the surface of the stone while derust...

Claims

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Application Information

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IPC IPC(8): C04B41/53
Inventor 李康
Owner 江苏凯信环保材料有限公司
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