Preparation method for portable minitype clean-energy storage device
A technology of clean energy and storage equipment, applied in the field of preparation of portable clean energy micro storage equipment, can solve the problems of excellent stability and rate performance, low price, etc., and achieve the effect of easy portability, easy operation, and simple preparation process
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specific Embodiment approach 1
[0022] Specific implementation mode 1: This implementation mode is a preparation method of a portable clean energy micro-storage device, which is carried out through the following steps:
[0023] 1. Cleaning of the collector: place the collector in water for ultrasonic cleaning for 5 minutes to 120 minutes, then place it in ethanol for ultrasonic cleaning for 5 minutes to 300 minutes, and finally place it in dilute hydrochloric acid solution with a concentration of 0.01mol / L~6mol / L for ultrasonic cleaning 5min~200min, get a clean current collector;
[0024] 2. Mix the cobalt nitrate solution with a concentration of 0.0001mol / L~1mol / L and the urea solution with a concentration of 0.0001mol / L~1mol / L and stir for 5min~720min to obtain a mixed solution A. The current collector is immersed in the mixed solution A, and then transferred to the reactor, and heated at a temperature of 90°C to 200°C for 0.5h to 72h, then the product is taken out of the reactor, and the product is washed...
specific Embodiment approach 2
[0030] Embodiment 2: This embodiment differs from Embodiment 1 in that in Step 1, it is placed in a dilute hydrochloric acid solution with a concentration of 0.08 mol / L and ultrasonically cleaned for 40 minutes. Others are the same as the first embodiment.
specific Embodiment approach 3
[0031] Embodiment 3: This embodiment is different from Embodiment 1 or Embodiment 2 in that: in step 2, the temperature is 100° C. for 1 hour. Others are the same as those in Embodiment 1 or 2.
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