Preparation method for Pd / PANI nano composite material
A nano-composite material, stable technology, applied in chemical instruments and methods, organic compounds/hydrides/coordination complex catalysts, chemical/physical processes, etc. High-level problems, to achieve the effect of protecting physical health, simple and easy operation, and reducing the amount of use
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Embodiment 1
[0026] 1. Weigh 0.8gSDS, 0.012gNaCl, 0.0058gPdCl 2 and 2 mL of water in a reaction vessel, placed in a water bath at 33 ° C to dissolve, to obtain a yellow-brown viscous liquid, under magnetic stirring, 2.95 mL of cyclohexane was added dropwise to obtain a yellow-brown unstable emulsion, and then added dropwise 0.38mL of n-amyl alcohol to obtain a translucent yellow-brown stable gel, namely component A;
[0027] 2. Place component A under a 15W energy-saving lamp for parallel irradiation for 36 hours, and the yellow-brown stable gel reacts to dark brown to obtain component B;
[0028] 3. Add 0.024 ml of An to component B and stir to obtain component C;
[0029] 4. Add 0.0596g APS, 0.012g NaCl, 2.3ml water, and 0.8g SDS to a 50ml beaker to dissolve, and place it in a water bath at 34.9°C to dissolve to obtain a colorless transparent viscous liquid. Add 2.96mL of cyclohexane dropwise under magnetic stirring alkane to obtain a milky white unstable emulsion, then 0.25 mL of n-am...
Embodiment 2
[0034] 1. Weigh 0.8gSDS, 0.012gNaCl, 0.0058gPdCl 2 and 2.2 mL of water in a reaction vessel, placed in a water bath at 34.8 ° C to dissolve, to obtain a yellow-brown viscous liquid, 2.96 mL of cyclohexane was added dropwise under magnetic stirring to obtain a yellow-brown unstable emulsion, and then added dropwise Add 0.34mL n-amyl alcohol to obtain a translucent yellow-brown stable gel, namely component A;
[0035] 2. Place component A under a 3W energy-saving lamp for parallel irradiation for 60 hours, and the yellow-brown stable gel reacts to dark brown to obtain component B;
[0036] 3. Add 0.024 ml of An to component B and stir to obtain component C;
[0037] 4. Add 0.0596g APS, 0.012g NaCl, 2.5ml water, and 0.8g SDS to a 50ml beaker to dissolve, and place it in a water bath at 35.6°C to dissolve to obtain a colorless transparent viscous liquid. Add 3.00mL of cyclohexane dropwise under magnetic stirring alkane to obtain a milky white unstable emulsion, then 0.23 mL of n...
Embodiment 3
[0041] 1. Weigh 0.8gSDS, 0.012gNaCl, 0.0058gPdCl 2 and 2.5mL of water in a reaction vessel, sealed and dissolved in a water bath at 36.5°C to obtain a yellow-brown viscous liquid, and 2.98mL of cyclohexane was added dropwise under magnetic stirring to obtain a yellow-brown unstable emulsion, then Add 0.20 mL of n-amyl alcohol dropwise to obtain a translucent yellow-brown stable gel, namely component A;
[0042] 2. Place component A under a 65W energy-saving lamp for parallel irradiation for 24 hours, and the yellow-brown stable gel reacts to dark brown to obtain component B;
[0043] 3. Add 0.0024ml of An to component B and stir to obtain component C;
[0044] 4. Add 0.0596g APS, 0.012g NaCl, 3.0ml water, and 0.8g SDS to a 50ml beaker to dissolve, seal it and dissolve it in a water bath at 37.0°C to obtain a colorless transparent viscous liquid. Add 2.96mL ring under magnetic stirring. hexane to obtain a milky white unstable emulsion, then dropwise add 0.20 mL of n-amyl alco...
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