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Method for extracting anoectochilus roxburghii and application of extracts of anoectochilus roxburghii

An extraction method and technology of clematis, applied in the directions of application, medical preparations containing active ingredients, pharmaceutical formulations, etc., can solve the problems of low comprehensive utilization rate of medicinal material resources, incomplete extraction of active ingredients, and extraction efficiency that cannot meet industrialization needs. , to achieve the effect of high utilization rate of medicinal material resources, improved batch processing capacity and processing speed, and improved extraction efficiency

Inactive Publication Date: 2015-11-25
HUAZHONG UNIV OF SCI & TECH +1
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0005] The technical problem to be solved by the present invention is to provide a method for extracting the extract of Aurantia clematis and the application of the extract, so as to overcome the incomplete extraction of active ingredients, low comprehensive utilization rate of medicinal material resources, and insufficient extraction efficiency in the existing extraction technology. Meet the needs of industrialization and other issues

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0050] Embodiment 1 blasting treatment

[0051] 1. Dry the clematis raw material, crush it through a 10-mesh sieve, preheat the clematis powder to 85°C with steam, and keep it for 10 minutes. Under 0.5MPa, cook in the vapor phase for 10 minutes, and release the pressure quickly. Collect the clematis powder after the blasting treatment, and use the aqueous solution to reflux extract the crushed clematis under the following conditions: solid-liquid ratio 1:30, extraction temperature 80°C, extraction time 0.5h, extraction times 2 times, filter , combined two filtrates.

[0052] Ⅱ. Dry the clematis raw material, crush it through a 10-mesh sieve, mix the clematis powder and water according to the ratio of 1:3 to make a homogenate, and use steam to preheat the homogenate to 100°C , maintained for 3 minutes, and the pre-compressed homogenate was steamed for 0.5 minutes at a temperature of 260° C. and a pressure of 2 MPa, and the pressure was quickly released. Collect the clematis ...

Embodiment 2

[0059] Embodiment 2 blasting treatment+subcritical water extraction

[0060] Ⅰ. Dry the clematis raw material, crush it through a 20-mesh sieve, mix the clematis powder and water according to the ratio of 1:2 to make a homogenate, and use steam to preheat the homogenate to 90°C , maintained for 5 minutes, and the pre-compressed homogenate was steamed for 6 minutes at a temperature of 200° C. and a pressure of 1 MPa, and the pressure was quickly released. Collect the Clematis clematis powder after blasting treatment, use water as the extraction solvent, according to the ratio of material to liquid 1:10, at a temperature of 100 ° C, a pressure of 5 MPa, subcritical extraction for 45 minutes, adjust the temperature to 200 ° C, pressure 10 MPa, subcritical extraction Extract for 75 minutes, spray dry to obtain the water extract.

[0061] Ⅱ. Dry the clematis raw material, crush it through a 20-mesh sieve, mix the clematis powder and water according to the ratio of 1:2 to make a ho...

Embodiment 3

[0070] Embodiment 3 blasting treatment+subcritical water extraction+subcritical alcohol extraction

[0071] Ⅰ. Dry the clematis raw material, crush it through a 20-mesh sieve, mix the clematis powder and water according to the ratio of 1:2 to make a homogenate, and use steam to preheat the homogenate to 90°C , maintained for 5 minutes, and the pre-compressed homogenate was steamed for 6 minutes at a temperature of 200° C. and a pressure of 1 MPa, and the pressure was quickly released. Collect the clematis powder after blasting treatment, use ethanol aqueous solution with a volume fraction of 10% as the extraction solvent, and perform subcritical extraction at a temperature of 150°C and a pressure of 8MPa for 20 minutes according to a solid-liquid ratio of 1:20, and adjust the temperature to 250°C , pressure 15MPa, subcritical extraction for 20min, and spray drying to obtain the water extract. The clematis powder after subcritical water extraction is subjected to subcritical e...

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Abstract

The invention relates to a method for extracting anoectochilus roxburghii and application of extracts of the anoectochilus roxburghii. The method includes steps of S1, drying and grinding anoectochilus roxburghii materials and feeding the anoectochilus roxburghii materials through sieves with the sizes of 10-20 meshes to obtain anoectochilus roxburghii powder; S2, carrying out explosion treatment on the anoectochilus roxburghii powder for 3min-30min by the aid of water vapor under the pressure of 0.5MPa-2MPa, allowing the anoectochilus roxburghii powder to be extracted by the aid of existing technologies in follow-up procedures after the anoectochilus roxburghii powder is subjected to explosion treatment, or allowing the anoectochilus roxburghii powder to be selectively extracted by the aid of sub-critical water and / or sub-critical alcohol. The water vapor is used as an explosion medium. The method and the application have the advantages that effective components such as polysaccharides, total flavonoids and total alkaloids in the anoectochilus roxburghii can be sufficiently enriched by the aid of the method, accordingly, the method is high in medicinal material resource utilization rate, the extraction rates of the effective components can be greatly increased, the extraction efficiency can be obviously improved, the batch processing capacity can be greatly improved, the processing speeds can be greatly increased, and the method is suitable for large-scale production.

Description

technical field [0001] The invention relates to the field of processing and application of Chinese herbal medicines, and more specifically, relates to an extraction method of Aurantia clematis and the application of the extract. Background technique [0002] Anoectochilus roxburghii, also known as Anoectochilus roxburghii, has a sweet and slightly bitter taste, flat nature, and slight coldness. It is regarded as a rare and precious medicinal material in Fujian, Taiwan and other provinces and Southeast Asia. Blood, expelling wind and dampness, detoxification, pain relief, antitussive and other effects, mainly for hemoptysis, bronchitis, nephritis, cystitis, diabetes, hematuria, rheumatoid arthritis, tumors and other difficult diseases. [0003] The traditional methods of taking clematis are making tea, stewing meat, decocting, etc. In recent years, there have been many reports on the finishing technology of clematis. CN103392877A patent discloses a processing method of clemat...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): A61K36/898A23L1/29A23L33/00
Inventor 余龙江张海全金文闻王昭毅
Owner HUAZHONG UNIV OF SCI & TECH
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