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Preparation method of high thermal conductivity nano-carbon copper foil

A nano-carbon, high thermal conductivity technology, used in cooling/ventilation/heating transformation, coating, epoxy coating, etc., can solve problems such as hindering the effective transfer of heat, and achieve flexible and controllable coating thickness and high coating accuracy. , good coating effect

Active Publication Date: 2018-03-02
李鹏
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

However, the easy agglomeration of nanoparticles will seriously hinder the effective transfer of heat, so the dispersion of nanoparticles has become a difficult point in the research of the preparation method of thermal conductive composites.

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0018] A preparation method of high thermal conductivity nano-carbon copper foil, which comprises the following process steps:

[0019] a) Configure binder: pour 5% polyvinylidene fluoride into 95% N-methylpyrrolidone by weight percentage, and stir at room temperature for 0.5~2 hours;

[0020] b) Configure heat dissipation slurry: pour 1% graphene, 15% carbon nanotubes, 20% silicon carbide, and 20% boron nitride into 25% N-methylpyrrolidone by weight percentage, and stir at room temperature for 0.5 ~3 hours, then add 19% of the binder prepared in step a, and continue to stir for 2~8 hours;

[0021] c) Coating and drying treatment: apply the heat-dissipating slurry prepared in step b evenly to the surface of the copper foil with a smooth roller coating process, and then heat and dry the treatment. The heating temperature is 85~95°C, and the heating time is 2~ In 10 minutes, the desired high thermal conductivity nano-carbon copper foil can be obtained.

Embodiment 2

[0023] A preparation method of high thermal conductivity nano-carbon copper foil, which comprises the following process steps:

[0024] a) Configure binder: pour 40% epoxy resin into 60% N,N-dimethylformamide by weight percentage, and stir at room temperature for 0.5~2 hours;

[0025] b) Configure heat dissipation slurry: pour 15% graphene, 14% carbon nanotubes, 1% silicon carbide, and 25% boron nitride into 25% N,N-dimethylformamide by weight percentage, and Stir at room temperature for 0.5 to 3 hours, then add 20% of the binder prepared in step a, and continue to stir for 2 to 8 hours;

[0026] c) Coating and drying treatment: apply the heat-dissipating slurry prepared in step b evenly on the surface of the copper foil with a smooth roller coating process, and then heat and dry the treatment. The heating temperature is 75~85°C, and the heating time is 2~ In 10 minutes, the desired high thermal conductivity nano-carbon copper foil can be obtained.

Embodiment 3

[0028] A preparation method of high thermal conductivity nano-carbon copper foil, which comprises the following process steps:

[0029] a) Configure binder: pour 30% polyurethane into 70% acetone by weight percentage, and stir at room temperature for 0.5~2 hours;

[0030] b) Configure heat dissipation slurry: pour 20% graphene, 1% carbon nanotubes, 15% silicon carbide, and 25% boron nitride into 25% acetone by weight percentage, and stir at room temperature for 0.5 to 3 hours. Then add 14% in the prepared binder of step a, and continue to stir for 2 to 8 hours;

[0031] c) Coating and drying treatment: apply the heat-dissipating slurry prepared in step b evenly to the surface of the copper foil with a smooth roller coating process, and then heat and dry the treatment. The heating temperature is 45~55°C, and the heating time is 2~ In 10 minutes, the desired high thermal conductivity nano-carbon copper foil can be obtained.

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PUM

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Abstract

The invention relates to a preparation method of high thermal conductivity nano-carbon copper foil, comprising the following process steps: a) configuring a binder; b) configuring a heat dissipation slurry; c) coating and heating and drying treatment: the heat dissipation prepared in step b The slurry is evenly coated on the surface of the copper foil, and then heated and dried to obtain the desired high thermal conductivity nano-carbon copper foil.

Description

technical field [0001] The invention relates to a preparation method of a high thermal conductivity composite material, in particular to a preparation method of a high thermal conductivity nano-carbon copper foil. Background technique [0002] With the rapid development of microelectronics integration technology, the size and volume of electronic components are shrinking sharply. The resulting heat dissipation difficulties have seriously affected the accuracy and life of electronic devices, and have become the technical bottleneck of device miniaturization. This restricts the further development of integrated technology. Some data show that the stability of electronic devices decreases by about 10% for every 2°C increase in temperature; if it reaches 50°C, its lifespan is only about 17% of that at 25°C. Therefore, timely and efficient cooling of electronic devices is the key to their reliable use. Traditional heat-conducting materials such as metals, inorganic ceramics, an...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): C09D127/16C09D163/00C09D175/04C09D133/04C09D7/61H05K7/20
Inventor 屈洁昊
Owner 李鹏
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