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Antibacterial and deodorant high-water-absorbent resin and preparation method thereof

A technology of superabsorbent resin and formula, which is applied in deodorizing superabsorbent resin and its preparation, and antibacterial fields, which can solve the problems of user's physical injury and potential safety hazards, and achieve avoidance of rash, high safety and compatibility good sex effect

Inactive Publication Date: 2016-01-06
QUANZHOU BLD SCI TECH IND CO LTD
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0014] In summary, at present, in the known technical field, the antibacterial effect is mainly achieved by adding nano-silver ions or quaternary ammonium salt ions, but the above-mentioned method is used in personal daily necessities for women and children, which may cause potential safety hazards, which may cause harm to the user's health. Harm, there is no inquiry about the high antibacterial and deodorizing superabsorbent resin made of tea as a natural functional additive. Based on this, the present invention provides a pure natural superabsorbent resin with high antibacterial and deodorizing functions , the superabsorbent resin maintains high water absorption rate, high water retention rate, high absorption rate and high pressure resistance performance, and at the same time, it provides safe, comfortable and healthy products for women and children

Method used

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  • Antibacterial and deodorant high-water-absorbent resin and preparation method thereof

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0039] Accurately weigh 200g of acrylic acid, 60g of sodium hydroxide, 300g of deionized water, 0.1g of N,N'-methylenebisacrylamide, 0.025g of sodium sulfite, 0.025g of sodium persulfate, 15g of tea powder, polyethylene glycol dishrinkle Glyceryl ether, Polyethylene Glycol 200 are prepared according to the following steps:

[0040] 1), after mixing acrylic acid and deionized water, adding sodium hydroxide for neutralization, the degree of neutralization is 82%;

[0041] 2) Add tea powder to the reaction system, stir and mix, then oscillate ultrasonically for 10 minutes, add N,N'-methylenebisacrylamide, continue stirring for 5 minutes, then gradually raise the temperature to 60°C, then add sodium sulfite and sodium persulfate to trigger Polymerization reaction 90s, obtains gel-like polymer;

[0042] 3), granulate the gel-like polymer obtained in step 2), and dry at a temperature of 160° C. for 30 minutes to obtain a granular polymer;

[0043] 4) Mix deionized water and compos...

Embodiment 2

[0045] Accurately weigh 200g of acrylic acid, 60g of sodium hydroxide, 200g of deionized water, 2g of N,N'-methylenebisacrylamide, 0.1g of sodium sulfite, 0.1g of sodium persulfate, 30g of tea extract concentrate, polyethylene glycol di Glycidyl ether, polyethylene glycol 200 are prepared by the composite cross-linking agent 0.5g of 1:1 molar ratio configuration, then according to the following steps:

[0046] 1), after mixing acrylic acid and deionized water, adding sodium hydroxide for neutralization, the degree of neutralization is 72%;

[0047] 2) Add tea extract to the reaction system, stir and mix, then oscillate ultrasonically for 10 minutes, add N,N'-methylenebisacrylamide, continue stirring for 5 minutes, then gradually raise the temperature to 60°C, then add sodium sulfite and sodium persulfate Initiate the polymerization reaction for 90s to obtain a gel-like polymer;

[0048] 3), granulate the gel-like polymer obtained in step 2), and dry at a temperature of 160° C...

Embodiment 3

[0051] Accurately weigh 200g of acrylic acid, 60g of sodium hydroxide, 260g of deionized water, 0.1g of N,N'-methylenebisacrylamide, 0.1g of sodium sulfite, 0.1g of sodium persulfate, 60g of tea extract, polyethylene glycol di Glycidyl ether and pentaerythritol are prepared according to the molar ratio of 1:1 and 0.5 g of composite cross-linking agent is prepared according to the steps of Example 2 to obtain the superabsorbent resin of the present invention.

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Abstract

The invention discloses antibacterial and deodorant high-water-absorbent resin having the formula comprising the following components in parts by weight: 200 parts of acrylic acid, 40-80 parts of sodium hydroxide, 200-300 parts of deionized water, 0.02-2 parts of a beginning cross-linking agent, 4-100 parts of a tea leaf powder or a tea leaf extract, 0.05-0.6 part of an initiator, and 0.2-4 parts of a composite cross-linking agent. The high-water-absorbent resin can be widely applied in hygienic liquid-absorbing products; the added tea leaves and the extract thereof endow the high-water-absorbent resin with excellent antibacterial deodorant properties, and do not affect various absorption properties of the high-water-absorbent resin. The high-water-absorbent resin has the advantages of easily available raw materials, low cost, significant effects, and great economic benefits, social benefits and environmental benefits.

Description

technical field [0001] The invention relates to the technical field of functional water-absorbing resins, in particular to an antibacterial and deodorizing superabsorbent resin and a preparation method thereof. Background technique [0002] Super absorbent polymer (SAP). [0003] It is a general term for high molecular polymers with high water absorption and water retention properties. [0004] In the early 1950s, the Goodrich Company of the United States developed cross-linked polyacrylic acid resins, and then Russell and others at the Northern Research Center of the United States Department of Agriculture began to study the grafting technology of starch and acrylonitrile in 1961; in 1978, Japan’s Sanyo Chemical Corporation developed And industrialized production of starch-grafted polyacrylic acid copolymerized superabsorbent resin. [0005] In China, the research on superabsorbent resin started in the early 1980s. Due to objective factors such as late start and short dev...

Claims

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Application Information

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IPC IPC(8): C08F220/06C08F120/06C08F2/44C08K5/00C08J3/24C08L33/02
Inventor 江毓铭郑叙炎林团员郑盛景林承锋伍佰芳
Owner QUANZHOU BLD SCI TECH IND CO LTD
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