Medium-deep well crosslinked polymer gel plugging agent and preparation method thereof
A technology of cross-linked polymer and plugging agent, applied in the field of oil drilling, can solve the problems of short validity period, prone to complex downhole, poor plugging efficiency, etc.
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Embodiment 1
[0023] A kind of preparation method of cross-linked polymer gel plugging agent for middle and deep wells of the present invention, comprises the following steps successively:
[0024] ⑴ Prepare raw materials with the following components and weight content, refined cotton sodium salt solution: 120 parts, acrylamide: 75 parts, ammonium persulfate: 13 parts, cerium sulfate: 2 parts, β-D-mannuronic acid (M): 4 parts, ammonium dihydrogen phosphate: 1 part, composite portland cement slurry: 100 parts and hybrid microfiber: 150 parts; the water-cement ratio of the composite portland cement slurry is 0.44;
[0025] (2) Add acrylamide to the refined cotton sodium salt solution, stir at a high speed of 400r / min for 10 minutes to fully mix the two, then stir at a medium speed at a speed of 300r / min, heat to 60°C while stirring at a medium speed maintain a constant temperature;
[0026] (3) Continuously feed nitrogen gas into the reaction product of step (2) and the reaction vessel. Aft...
Embodiment 2
[0032] A kind of preparation method of cross-linked polymer gel plugging agent for middle and deep wells of the present invention, comprises the following steps successively:
[0033] ⑴ Prepare raw materials with the following components and weight content, refined cotton sodium salt solution: 120 parts, acrylamide: 80 parts, ammonium persulfate: 15 parts, cerium sulfate: 3 parts, β-D-mannuronic acid (M): 4 parts, ammonium dihydrogen phosphate: 1.2 parts, composite Portland cement slurry: 100 parts and hybrid microfiber: 180 parts; the water-cement ratio of the composite Portland cement slurry is 0.44;
[0034] (2) Add acrylamide to the refined cotton sodium salt solution, stir at a high speed of 400r / min for 10 minutes to fully mix the two, then stir at a medium speed at a speed of 300r / min, heat to 60°C while stirring at a medium speed maintain a constant temperature;
[0035] (3) Continuously feed nitrogen gas into the reaction product of step (2) and the reaction vessel. ...
Embodiment 3
[0041] A kind of preparation method of cross-linked polymer gel plugging agent for middle and deep wells of the present invention, comprises the following steps successively:
[0042] ⑴ Prepare raw materials for the following components and weight content, refined cotton sodium salt solution: 120 parts, acrylamide: 85 parts, ammonium persulfate: 17 parts, cerium sulfate: 5 parts, β-D-mannuronic acid (M): 4 parts, ammonium dihydrogen phosphate: 1.5 parts, composite Portland cement slurry: 100 parts and hybrid microfiber: 200 parts; the water-cement ratio of the composite Portland cement slurry is 0.44;
[0043] (2) Add acrylamide to the refined cotton sodium salt solution, stir at a high speed of 400r / min for 10 minutes to fully mix the two, then stir at a medium speed at a speed of 300r / min, heat to 60°C while stirring at a medium speed maintain a constant temperature;
[0044] (3) Continuously feed nitrogen gas into the reaction product of step (2) and the reaction vessel. A...
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