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Method for processing base oil of tea oil cosmetic

A processing method and base oil technology, which are applied in cosmetics, cosmetic preparations, cosmetic preparations, etc., can solve the problems of excessive alkali, increase loss and loss, and reduce product quality, and achieve acid value and peroxide value. The effect of low processing yield and quality improvement

Active Publication Date: 2016-02-03
RES INST OF SUBTROPICAL FORESTRY CHINESE ACAD OF FORESTRY
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0003] Adopt existing method, because what adopt is hydration degumming, and do not add acid before washing, can cause the partial emulsification of oil inevitably, because can't solve the difficult problem of emulsification in the tea oil processing; Higher temperature and more excess alkali will inevitably lead to the loss of a large amount of neutral oil, so the yield of finished oil is lower
Since the quality control of degummed oil fails to meet the processing quality requirements of light-colored decolorized oil, and the types and proportions of decolorizers used are unreasonable, it is difficult to meet the requirements for one-time decolorization, and secondary decolorization has to be carried out, which increases production costs and reduces production costs. Productivity
The low temperature not used in the deodorization process, because the process temperature used is the same as that of the camellia oil process, the loss of camellia oil during processing and the loss of non-micronutrients in the oil are much larger than this process, including natural antioxidants, etc. reduced product quality
Due to the lack of proper concentration and dosage of citric acid in the processing process, the long-term low-temperature acid reaction was not carried out, and the acid was not added to further remove metal ions before the alkali refining oil was washed, and the processing temperature was high, which made the color return problem of the product more obvious.

Method used

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  • Method for processing base oil of tea oil cosmetic

Examples

Experimental program
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Effect test

Embodiment 1

[0024] Embodiment 1: The camellia oil pressed crude oil (acid value 1.5mgKOH / g) that meets the national standard is finely filtered, and the impurity content after fine filtration is less than 0.1%. At normal temperature, add 50% citric acid solution accounting for 2% of the oil weight to carry out acid reaction, and carry out vigorous stirring. The reaction time is 150min; After 30 minutes, the reacted camellia oil was heated to 75°C, and the oil and soap were separated; the tea oil after de-soaping was added with acid, and washed with water; before washing, 50% citric acid aqueous solution accounting for 0.02% of the oil weight was added and mixed evenly, and The oil temperature is increased to 85°C, the water temperature is 90°C, and the amount of water added accounts for 10% of the oil weight; after washing the oil to remove soap, vacuum drying, and then polishing and filtering, so that the moisture content of the dry oil is less than 0.01%, and the impurity content is less...

Embodiment 2

[0025] Embodiment 2: Finely filter the pressed camellia oil (acid value 2.0 mgKOH / g) that meets the national standard, and the impurity content after finely filtering is less than 0.1%. Under normal temperature, add 52% citric acid solution that accounts for 1.8% of oil weight to carry out acid reaction, and carry out strong stirring, and the reaction time is 180min; After 25 minutes, the reacted camellia oil was heated to 75°C, and the oil and soap were separated; the tea oil after de-soaping was added with acid, and washed with water; before washing, 52% citric acid aqueous solution accounting for 0.02% of the oil weight was added and mixed evenly, and The oil temperature is increased to 87°C, the water temperature is 92°C, and the amount of water added accounts for 12% of the oil weight; after the oil is washed with water to remove the soap, it is vacuum-dried, and then polished and filtered, so that the moisture content of the dried oil is less than 0.01%, and the impurity ...

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Abstract

The invention discloses a method for processing base oil of a tea oil cosmetic. The method comprises the steps that 1, tea oil squeezed crude oil meeting the national standard is finely filtered, and a citric acid solution accounting for 0.02% of oil weight is added; 2, after an acid reaction, caustic soda liquid is added at normal temperature for an alkali reaction, and after the tea oil is heated, soap removing is carried out; 3, acid is added to the tea oil obtained after soap removal, washing is carried out, and after the washed oil is subjected to vacuum drying, polishing filter is carried out; 4, the tea oil obtained after polishing filter is heated, and meanwhile a mixed decolorising agent is added for decoloration in a bleaching tower; 5, the decolored oil is deodorized at low temperature; 6, the deodorized oil is winterized and filtered, and then the base oil of the tea oil cosmetic is obtained if the oil passes inspection. After the method is adopted, the color reversion problem of the base oil is solved, the micronutrient content of the product is effectively increased, production cost is obviously reduced, the processing rate is greatly increased, the product can be directly smeared as suntan oil and can also be used for daily skin care, and the life quality of people is improved.

Description

technical field [0001] The invention relates to the field of camellia oil cosmetic base oil, in particular to a processing method of camellia oil cosmetic base oil. Background technique [0002] The processing method of the existing camellia oil cosmetics base oil, the processing technology adopted is basically similar to the soybean oil refining process, is to hydrate the camellia seed crude oil with alkali refining, wash, dry, decolorize, deodorize, and then winterize (similar to corn oil) . Specifically: After filtering the crude oil of the pressed oil, heat it to 70-80°C, add 15 degrees of Baume liquid caustic soda for alkali refining, the reaction time is about 20 minutes, after the oil and soap are separated, heat it to 85-95°C and add oil Wash with 10% hot water at 90°C, then vacuum dry; add activated clay and activated carbon to the dried oil and mix evenly (activated clay: activated carbon = 20:1), heat to 105-115°C for 30 minutes, filter and enter deodorization T...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C11B3/00C11B3/04C11B3/06A61K8/92A61Q19/00A61Q17/04
Inventor 郭少海王亚萍罗凡费学谦姚小华
Owner RES INST OF SUBTROPICAL FORESTRY CHINESE ACAD OF FORESTRY
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