Powdery ardealite filler and preparation thereof
A phosphogypsum and powdery technology, which is applied in the field of powdery phosphogypsum filler and its preparation, can solve the problems of affecting the color of the product, affecting the thermal stability, internal structure damage, etc., and achieve the improvement of comprehensive mechanical properties and heat resistance and mechanical properties, and the effect of improving thermal stability
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Embodiment 1
[0017] A powdery phosphogypsum filler, raw materials include: 110kg phosphogypsum, 4kg dispersant, 6kg corn stalk lignin.
[0018] The mass ratio of the dispersant is: paraffin wax, citric acid ester, stearate, polypropylene wax, polyethylene wax=1:1:1:1:1.
[0019] The preparation method is as follows: heating and sintering the phosphogypsum until the surface temperature of the phosphogypsum is 180-190°C, grinding the phosphogypsum to a particle size of 70 μm, and cooling to normal temperature to obtain β-type hemihydrate gypsum; adding processing aids and dispersants and Mix for 6 minutes at a rotational speed of 708 r / min, and then maintain at a constant temperature of 75° C. for 35 minutes, and then grind into powder to obtain powdery phosphogypsum filler.
[0020] The temperature-increasing sintering is performed at a temperature of 100° C. for 20 minutes, and then the temperature is raised at a rate of 7° C. / min.
Embodiment 2
[0022] A powdery phosphogypsum filler, raw materials include: 140kg phosphogypsum, 2.6kg dispersant, 4.8kg coniferous lignin.
[0023] The dispersant is citrate.
[0024] The preparation method is as follows: heat up phosphogypsum and sinter until the surface temperature of phosphogypsum is 188°C, grind to a particle size of 73 μm, cool to room temperature, and obtain β-type hemihydrate gypsum; Mix at 780r / min for 7min, then place at 70°C for constant temperature curing for 50min, and then grind into powder to obtain powdery phosphogypsum filler.
[0025] The temperature-increasing sintering is performed at a temperature of 100° C. for 20 minutes, and then the temperature is raised at a rate of 5° C. / min.
Embodiment 3
[0027] A powdery phosphogypsum filler, raw materials include: 130kg phosphogypsum, 2kg dispersant, 4kg bamboo alkali lignin.
[0028] The mass ratio of the dispersant is: paraffin wax, citric acid ester, polypropylene wax, polyethylene wax=1:1:1:2.
[0029] The preparation method is as follows: heating and sintering the phosphogypsum until the surface temperature of the phosphogypsum is 185°C, grinding the phosphogypsum to a particle size of 75-80 μm, and cooling to normal temperature to obtain β-type hemihydrate gypsum; adding processing aids and dispersants and Mix for 5 minutes at a rotational speed of 700 r / min, and then maintain at a constant temperature of 87° C. for 60 minutes, and then grind into powder to obtain powdery phosphogypsum filler.
[0030] The temperature-increasing sintering is performed at a temperature of 100° C. for 20 minutes, and then the temperature is raised at a rate of 8° C. / min.
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