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Method for extracting capsaicin crystals from capsicum essence

A technology of capsaicin and capsaicin, which is applied in organic chemistry, carboxylic acid amide separation/purification, etc., can solve the problems of equipment investment, high safety and operation requirements, cumbersome operation steps of organic solvent method, and large amount of organic solvent, etc. Reach the effects of low requirements on reaction conditions and production equipment, shorten extraction time, and reduce solvent usage

Inactive Publication Date: 2017-08-11
广西恒得润辣素有限公司
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

The operation steps of the organic solvent method are cumbersome, and the amount of organic solvent is large, so it is difficult to popularize and apply; the supercritical carbon dioxide fluid extraction method uses a solvent method to extract the crude capsicum essence, and then puts the crude capsicum essence into the extraction kettle in the supercritical device, and opens the extraction The circulation loop "extraction-separation-extraction" is used to extract and control the pressure of carbon dioxide to obtain capsaicin with high purity. However, this method has high requirements for equipment investment, safety and operation, and the production cost is also high, which is not conducive to production and application. Enzymatic extraction also has certain limitations, such as higher requirements on test conditions such as temperature, pH value and action time, and the types of applicable enzymes are also very limited, which restricts the popularization and use of this method

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0029] (1) Take the commercially available Tianzhitianjiao as raw material, carry out cleaning pretreatment, remove impurities, dry until the water content is not higher than 8%, crush, pass through a 60-mesh sieve to obtain chili powder;

[0030] (2) Put 9.2Kg of chili powder and 0.8Kg of β-cyclodextrin in a planetary mill or a vibration mill for 10 minutes to obtain a mixed powder;

[0031] (3) Take 10Kg of mixed micropowder and 80L of 65% ethanol for mixing, stir for 25min, let stand, and then separate the impurity precipitate and filtrate with a high-speed centrifuge at a speed of 10000r / min; repeat the ethanol extraction of the impurity precipitate 3 times, Repeat centrifugation, and finally combine all filtrates;

[0032] (4) The filtrate of step (3) was concentrated under reduced pressure under the conditions of a vacuum pressure of 0.1 mPa and a temperature of 55° C., and ethanol was recovered to obtain a crude capsicum extract in the form of a dark red viscous liquid.

Embodiment 2

[0034] (1) Take the Sichuan Chaotian pepper purchased from the market as the raw material, carry out cleaning pretreatment, remove impurities, dry until the water content is not higher than 8%, crush, pass through an 80-mesh sieve to obtain chili powder;

[0035] (2) Put 9.8Kg of chili powder and 0.2Kg of β-cyclodextrin in a planetary mill or a vibration mill for 30 minutes to obtain a mixed powder;

[0036] (3) Take 10Kg of mixed micropowder and 150L of 50% ethanol to mix, stir for 10min, let stand, then use a high-speed centrifuge at 8000r / min to separate the impurity precipitate and filtrate; repeat the ethanol extraction of the impurity precipitate twice, Repeat centrifugation, and finally combine all filtrates;

[0037] (4) The filtrate of step (3) is concentrated under reduced pressure under the conditions of a vacuum pressure of 0.1 mPa and a temperature of 45° C., and ethanol is recovered to obtain a crude capsicum extract in the form of a dark red viscous liquid.

Embodiment 3

[0039] (1) Take the commercially available Tianzhitianjiao as raw materials, carry out cleaning pretreatment, remove impurities, dry until the moisture content is not higher than 8%, crush, pass through a 100-mesh sieve to obtain chili powder;

[0040] (2) Put 9.5Kg of chili powder and 0.5Kg of β-cyclodextrin in a planetary mill or a vibration mill for 20 minutes to obtain a mixed powder;

[0041] (3) Take 10Kg of mixed micropowder and 120L of 60% ethanol to mix, stir for 20min, let stand, then use a high-speed centrifuge at a speed of 12000r / min to separate the impurity precipitate and filtrate; repeat the ethanol extraction of the impurity precipitate 3 times, Repeat centrifugation, and finally combine all filtrates;

[0042] (4) The filtrate of step (3) is concentrated under reduced pressure under the conditions of a vacuum pressure of 0.1 mPa and a temperature of 50° C., and ethanol is recovered to obtain a crude capsicum extract in the form of a dark red viscous liquid.

[0043] ...

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Abstract

The invention discloses a method for extracting capsaicin crystals from oleoresin capsicum. The method comprises the following steps that chilli powder is extracted with an aqueous alkaline solution in a single-stage continuous countercurrent ultrasonic extraction machine, wherein the aqueous alkaline solution is prepared from sodium chloride, sodium acetate, sodium hydroxide and beta-cyclodextrin; filtrate obtained through filtering separation is processed through the steps of concentration, ethanol extraction, reduced pressure distillation, petroleum ether low-temperature recystalization and the like, and then the high-purity needle-shaped capsaicin crystals are obtained. According to the method, a continuous countercurrent and ultrasonic extraction technique, a micro-cutting interaction technique and the like are combined on the basis of a common solvent method, the extraction time is shortened, the solvent using amount is decreased, the recycle rate and the purity of the capsaicin crystals can be effectively increased, the whole operation process is easy and convenient, the requirements for the reaction condition and production equipment are low, and the method is a capsaicin crystal extraction technology which is suitable for industrialized popularization.

Description

Technical field [0001] The invention belongs to the technical field of capsaicin extraction, and specifically relates to a method for extracting capsaicin crystals from capsaicin extract. Background technique [0002] Capsaicin, also known as capsaicin, capsaicin, etc., generally contains the highest content in the peptide compartment tissue (seed-producing part), diaphragm tissue, and the middle part of the peel in the fruit. It is the main chemical substance that causes the spicy taste of pepper. This spicy ingredient was first isolated from the pepper fruit by Thres (1876). Afterwards, scholars analyzed its chemical composition in detail and found that the spicy ingredient in pepper is composed of a series of homologs: capsaicin family, Dihydrocapsaicin family, homocapsaicin family, nordihydrocapsaicin family, p-methyl capsaicin family, p-methyl capsaicin saturated chain hydrocarbon family, p-methyl capsaicin ene chain family, etc., among which capsaicin family Mainly. Capsa...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): C07C231/24C07C233/20
Inventor 杨红梅
Owner 广西恒得润辣素有限公司
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