Taxus chinensis oil and extracting method thereof

An extraction method, the technology of yew oil, which is applied in the direction of fat oil/fat production, fat oil/fat refining, fat production, etc., can solve the problems of extracting yew oil from yew seeds that have never been seen, and achieve good temperature resistance and high concentration chunky effect

Active Publication Date: 2016-03-23
GUANGDONG HEJI BIOTECH CO LTD
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

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Problems solved by technology

The Northeast Base Research Institute has also done key experiments on yew. The research and separation technology have not been reported in various information materials to extract yew oil from yew seeds.

Method used

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  • Taxus chinensis oil and extracting method thereof

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Experimental program
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Effect test

Embodiment 1

[0016] Extraction method of yew oil: remove the pulp (aril) from fresh yew seeds and elute to obtain 500g of pure yew seeds, bake, dry, crush into 40-60 mesh, treat with microwave equipment for 1-2min, and then put into In the solvent method extractor, the ratio of raw material to solvent is 1:6, heated at 30-35°C, and the dynamic leaching time is 2-3h. Repeat this method for filtering the solution for 3 times, combine and filter the extraction solution, vacuum distillation and concentration to obtain oil . The vacuum process temperature is controlled within 55°C to extract oil. The solvent is recovered and reused, and the yew crude oil obtained by the solvent method is desolvated, impurity-removed and refined by a supercritical CO? device, with a pressure of 26mpa, a temperature of 42°C, a CO? , finely filtered to obtain 169.5 grams of yellowish and transparent yew oil, with a yield of 33.9%.

[0017] Choose the No. 6 extraction solvent oil that is harmless to human body, h...

experiment example

[0020] Taxus oil chemical composition analysis content weight percent comprises as follows:

[0021] Operating conditions:

[0022] Column: Quartz capillary column: length 60m, inner diameter about 0.25mm.

[0023] Stationary phase: 100% dimethyl polysiloxane packing.

[0024] Film thickness: 0.25 μm.

[0025] Chromatographic oven temperature: linearly programmed temperature rise from 60°C to 280°C at a rate of 2°C / min, and finally kept at 280°C for 15 minutes.

[0026] Injection port temperature: 280°C.

[0027] Detector: Quadrupole mass spectrometer detector.

[0028] Carrier gas: helium.

[0029] Carrier gas flow rate: 1.5ml / min.

[0030] Injection volume: about 0.2 μl.

[0031] Split ratio: 1 / 100.

[0032] 　 Pentane 1.265 　 Octane 1.374 　 trans-2-Heptenal 0.999 　 Trans-2-Decenal Trans-2-Decenal 1.922 　 2,4-Nonadienal 2,4-Nonenal 0.962 　 2,4-Decadienal 2,4-Decadienal 1.993 　 Methyl 5,9-heptadecadienoate 3.596 ...

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Abstract

The invention relates to a method for extracting plant oil from plants, in particular to taxus chinensis oil and an extracting method thereof. The extracting method comprises the following steps that seeds of taxus chinensis fruit are taken as raw materials, oil is obtained through extraction by adopting a microwave method and a solvent method, residual solvent odor and impurities are removed through a supercritical CO2 method, standing, refined filtering and refining are performed on a re-extraction product under the low temperature condition, and then the taxus chinensis oil is obtained. According to the method, re-extracting and refining are performed by adopting the microwave-assistant method and the solvent method to be combined with supercritical CO2 technology equipment, and therefore not only is the basic characteristic that the biological activity is not destroyed under the low temperature condition guaranteed, but also the residual solvent odor and the impurities are removed more effectively and the high standard of the green quality is achieved.

Description

technical field [0001] The invention relates to a method for extracting vegetable oil from plants, namely yew oil and its extraction method. Background technique [0002] In the prior art "Changbai Mountain Plant Resources Chronicle", "Handbook of Chemical Separation of Traditional Chinese Medicine", and "Modern Chinese Medicine Pharmacology", yew is a red bean plant and has another name called yew. There are about 11 species in the world, and there are four varieties in my country. Its seeds are used as a diuretic and menstrual medicine in the folk, but it has not been recorded in commonly used traditional Chinese medicine literature. In recent years, paclitaxel, an effective anti-tumor ingredient, has been isolated from the bark, stem, and leaves of various plants of the genus Taxus, which has attracted great attention from scholars and research departments at home and abroad, and has become a research hotspot. From the functional value of the clinical curative effect, th...

Claims

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Application Information

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IPC IPC(8): C11B1/00C11B1/10C11B3/00
CPCC11B1/00C11B1/10C11B3/006
Inventor 何廷刚艾勇张兵芦建仁
Owner GUANGDONG HEJI BIOTECH CO LTD
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