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Technology for preparing highly pure crude rice bran oil

A high-purity technology for crude rice bran oil, which is applied in the fields of edible oil/fat, fat oil/fat production, and fat oil/fat refining, etc., can solve the problems of low oil yield, expensive equipment and high technology, and achieves the reduction of impurity content, The effect of low energy consumption and high oil yield in the production process

Inactive Publication Date: 2016-04-06
JIANGSU KANG ZHI YUAN GRAIN & OIL
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0002] Rice bran is an important by-product in the rice processing process. Rice bran is rich in fat, accounting for 18% to 25%. The main component of rice bran oil is fatty acid glyceride. %, linoleic acid 29% to 42%, and also contains vitamins and other ingredients; due to the fatty acid composition and some special ingredients in rice bran oil, rice bran oil has extremely high nutritional value and medicinal value, and is increasingly valued by people; The traditional method is to use rice bran as feed to feed livestock and poultry, which greatly reduces its nutritional value and resource value, resulting in serious waste of resources, or as fuel or discarded, causing pollution to the environment
[0003] There are three production processes for rice bran oil production: one is mechanical pressing, the other is solvent leaching, and the third is supercritical extraction; these three methods have their own characteristics: the rice bran oil extracted by traditional mechanical pressing has good oil quality, The color is good-looking, edible and pure, but the oil yield is low; the solvent leaching method can greatly increase the oil yield, and it is easy to produce on a large scale, but the color of the oil is darker and the crude oil contains more non-oily substances; supercritical The oil used in the extraction method is better, but it requires high technology and expensive equipment, and it is impossible to produce it on a large scale today.

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0017] A kind of process for preparing high-purity rice bran crude oil provided in this embodiment comprises the following specific steps:

[0018] (1) After wet puffing, the rice bran has a crushing degree of 50 mesh and a water content of 7%. The leaching solvent isopropanol is added according to the ratio of material to liquid 1:5 (W / V), and the pH value is 6.4; at the same time, the mass of rice bran is 0.1 % papain, 10 times the amount of water, stir evenly; the extraction time is 4h;

[0019] (2) Refining: The initial temperature of alkali refining is 45°C, the concentration of KOH is 18.5%, the excess alkalinity is 0.4%, and it is filtered, and the impurity content in the rice bran crude oil obtained after filtering is controlled below 0.2%;

[0020] (3) Acid hydration degumming: The acid hydration degumming method mainly uses a dilute solution of medium-strong acids such as phosphoric acid, citric acid, oxalic acid, tartaric acid, etc., mixes it with rice bran crude oi...

Embodiment 2

[0024] The invention provides a process for preparing high-purity rice bran crude oil, which comprises the following specific steps:

[0025] (1) After wet puffing, the rice bran has a crushing degree of 50 mesh and a water content of 7%. Add the leaching solvent isopropanol according to the ratio of material to liquid 1:5 (W / V), and the pH value is 6.5; at the same time, the mass of rice bran added is 0.11 % papain, 11 times the amount of water, stir evenly; the extraction time is 6h;

[0026] (2) Refining: The initial temperature of alkali refining is 45°C, the concentration of KOH is 18.5%, the excess alkalinity is 0.4%, and it is filtered, and the impurity content in the rice bran crude oil obtained after filtering is controlled below 0.2%;

[0027] (3) Acid hydration degumming: The acid hydration degumming method mainly uses a dilute solution of medium-strong acids such as phosphoric acid, citric acid, oxalic acid, tartaric acid, etc., mixes it with rice bran crude oil at...

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PUM

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Abstract

The invention discloses a technology for preparing highly pure crude rice bran oil. The technology comprises the steps of extraction, purification, acid hydration degumming, dewaxing and depickling, wherein depickling is characterized in that an esterification reaction of alcohols and fatty acids is carried out at 55-65DEG C under normal pressure by using an acidic catalyst, such as benzene sulfonic acid, p-toluenesulfonic acid, solid super acid, and highly acidic resin to remove fatty acids in grease and fatty acids in rice bran oil. The technology for preparing highly pure crude rice bran oil reserves glycerate and other beneficial components in the rice bran oil, and brings a wide development space for realizing optimal reasonable utilization of agriculture resources, maximized rural economic benefits and highest peasant income as an agriculture economy growth point.

Description

technical field [0001] The invention relates to the field of deep processing of agricultural by-products, in particular to a process for preparing high-purity crude rice bran oil. Background technique [0002] Rice bran is an important by-product in the rice processing process. Rice bran is rich in fat, accounting for 18% to 25%. The main component of rice bran oil is fatty acid glyceride. %, linoleic acid 29% to 42%, and also contains vitamins and other ingredients; due to the fatty acid composition and some special ingredients in rice bran oil, rice bran oil has extremely high nutritional value and medicinal value, and is increasingly valued by people; The traditional method is to use rice bran as feed to feed livestock and poultry, which greatly reduces its nutritional value and resource value, resulting in a serious waste of resources, or as fuel or discarded, causing pollution to the environment. [0003] There are three production processes for rice bran oil productio...

Claims

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Application Information

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IPC IPC(8): C11B1/04C11B1/00C11B3/00A23D9/04
Inventor 李勃
Owner JIANGSU KANG ZHI YUAN GRAIN & OIL
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