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Method for simultaneously extracting soybean oil and soybean milk powder by aqueous enzymatic method

A simultaneous extraction and soybean oil technology, which is applied in milk substitutes, dairy products, fat oil/fat production, etc., can solve the problems of high cost of enzyme preparations, little research on soybean oil and soybean milk powder, and long reaction time

Inactive Publication Date: 2016-04-20
NORTHEAST AGRICULTURAL UNIVERSITY
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

At present, the extraction of soybean oil by aqueous enzymatic method is mostly limited to laboratory research. Due to the problems of high cost of enzyme preparation, long reaction time, and difficulty in demulsification in the process of oil extraction by aqueous enzymatic method, it is rarely put into production practice. There are few studies on the industrial production of soybean oil and soybean milk powder by aqueous enzymatic method

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0017] After peeling the soybeans, use a QM ball mill to perform ultrafine grinding for 20-40 minutes under the condition of the grinding speed of 80-100r / min. min and die hole diameter of 18 mm to obtain the puffed product; add water to the enzymolysis reaction kettle, pass in steam at 55°C for heating, add the puffed product to the heated water and mix to obtain a mixed solution, Use 2mol / L NaOH solution to adjust the initial pH of the mixture to 8.5, add 3.5‰ Alcalase alkaline protease to the mixture under the condition of a material-to-liquid ratio of 1:7 for enzymolysis for 50 minutes, and use a three-phase horizontal method after enzymolysis Centrifuge to separate the emulsified oil, hydrolyzate and residue; use a disc centrifuge to centrifuge the emulsified oil to obtain soybean oil and water phase, add the water phase to the hydrolyzate and mix well, and then carry out vacuum in the concentration tower concentrated, spray-dried after concentration to obtain soybean mil...

Embodiment 2

[0019] After peeling the soybeans, use a QM ball mill to perform ultrafine grinding for 20-40 minutes under the condition of the grinding speed of 80-100r / min. min and die hole diameter of 18mm to obtain the puffed product; add water to the enzymolysis reaction kettle, pass in steam at 50°C for heating, add the puffed product to the heated water and mix to obtain a mixed solution, Use 2mol / L NaOH solution to adjust the initial pH of the mixture to 8.5, add 4‰ Alcalase alkaline protease to the mixture under the condition of a material-to-liquid ratio of 1:8 for enzymolysis for 40min, and use a three-phase horizontal method after enzymolysis Centrifuge to separate the emulsified oil, hydrolyzate and residue; use a disc centrifuge to centrifuge the emulsified oil to obtain soybean oil and water phase, add the water phase to the hydrolyzate and mix well, and then carry out vacuum in the concentration tower concentrated, spray-dried after concentration to obtain soybean milk powder...

Embodiment 3

[0021] After peeling the soybeans, use a QM ball mill to perform ultrafine grinding for 20-40 minutes under the condition of the grinding speed of 80-100r / min. min and the die hole diameter is 18mm to obtain the puffed product; add water to the enzymolysis reaction kettle, pass in steam at 60°C for heating, add the puffed product to the heated water and mix to obtain a mixed solution, Use 2mol / L NaOH solution to adjust the initial pH of the mixed solution to 8.5, add 3‰ Alcalase alkaline protease to the mixed solution under the condition of a material-to-liquid ratio of 1:6 for enzymatic hydrolysis for 60 minutes, and use a three-phase horizontal method after enzymatic hydrolysis Centrifuge to separate the emulsified oil, hydrolyzate and residue; use a disc centrifuge to centrifuge the emulsified oil to obtain soybean oil and water phase, add the water phase to the hydrolyzate and mix well, and then carry out vacuum in the concentration tower concentrated, spray-dried after co...

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PUM

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Abstract

The invention relates to a method for synchronously extracting soybean oil and soybean milk powder by an aqueous enzymatic method, which belongs to the technical field of plant grease processing. The method comprises the following steps: 1) dehulling soybeans and performing ultramicro grinding on the soybeans, extruding the soybeans and puffing the ground material to obtain a puffed product; 2) adding water into an enzymatic hydrolysis reaction vessel, heating steam and adding the puffed product to obtain mixed liquor, adjusting pH value of the mixed liquor, adding alkali protease for performing enzymatic hydrolysis, using a horizontal centrifuge after enzymatic hydrolysis is carried out for performing centrifugation to obtain emulsified oil, a hydrolysate and residues; and 3) using a disk centrifuge for performing centrifugation on the emulsified oil to obtain the soybean oil and a water phase, adding the water phase into the hydrolysate for concentration, and drying the material to obtain the soybean milk powder. The method has the advantages of simple process, short reaction time, less enzyme usage amount and low cost, and the prepared soybean oil has no solvent residues and has high quality. The soybean milk powder can be prepared when the soybean oil is prepared, the soybean milk powder can keep partial fat, and has advantages of rich bean fragrance, abundant nutrition, and good brewing property, and is suitable for continuous industrial production.

Description

technical field [0001] The invention belongs to the technical field of vegetable oil processing, and mainly relates to a method for synchronously extracting soybean oil and soybean milk powder by an aqueous enzymatic method. Background technique [0002] The traditional methods of producing vegetable oil are mainly pressing and leaching. The pressing method has a simple process and less supporting equipment, which can maintain the special flavor of the product, but the oil extraction rate is low, the energy consumption is high, and the cost is high. Moreover, the protein denaturation of the cake after pressing is serious, and the protein utilization rate is low, resulting in a serious waste of vegetable protein. . The leaching method has high production efficiency and low residual oil rate, but this method requires a lot of equipment, large investment, large loss of oil flavor and residual organic solvents, and requires refining treatment, and also pollutes the environment....

Claims

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Application Information

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IPC IPC(8): C11B1/02C11B1/04C11B3/16A23C11/10A23L11/65
CPCA23C11/103C11B1/025C11B1/04C11B3/16
Inventor 江连洲齐宝坤李杨隋晓楠王中江
Owner NORTHEAST AGRICULTURAL UNIVERSITY
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