Filling method of granular water-absorbing agent and sampling method of granular water-absorbing agent filling
A filling method and granular technology, which can be used in sampling devices, chemical instruments and methods, transportation and packaging, etc., can solve the problems of physical property reduction and physical property deviation, and achieve the effect of reducing deviation and less consumer complaints
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manufacture example 1-1
[0419] Polymerization process, gel fine granulation (disintegration) process, drying process, pulverization process, classification process, surface crosslinking process (spraying process of surface crosslinking agent, heating process), cooling process, sizing process and product The devices in the storage / filling process are connected by a conveying device, and a continuous manufacturing device capable of continuously performing each process is used, and the same operation is performed with reference to Example 3 described in International Publication No. 2011 / 126079 to manufacture a particulate water-absorbing agent . However, at this time, an equivalent amount of ethylene carbonate was used instead of 1,4-butanediol used as a surface crosslinking agent.
[0420] In this way, the mass average particle diameter (D50) was about 370 micrometers, the logarithm standard deviation (σζ) of the said particle size distribution was about 0.34, and the particulate water-absorbing agent...
experiment example 1-1
[0424] use figure 1 The filling apparatus shown is used to fill the particulate water-absorbing agent (a) obtained in Production Example 1-1 above. In addition, the raw material of the suspending belt 20 is cloth, and it has the structure which has a clearance gap with the contact part with the filling container 16, and the contact part with the suspension part 22 (the same applies hereinafter).
[0425] The vibration generating device is composed of two unbalanced mass types. In order to suppress the vibration in the horizontal direction, the rotation direction of the vibration motor is set in the opposite direction, so that they are inverse cycles to each other, so that the vibration angle reaches 90±5°.
[0426] In the vibration at the time of no load, the vibrating body was set so as to achieve an amplitude of 0.28 [mm], a vibration frequency of 60 [Hz], an acceleration of 2.0 [G], and a vibration index of 27.1. In addition, the vibration is linear vibration, and the vib...
experiment example 2-1
[0435] The vibration conditions were changed as follows, and the same operation as in Experimental Example 1-1 was performed.
[0436] The vibration generating device is composed of two unbalanced mass types. In order to suppress the vibration in the horizontal direction, the rotation direction of the vibration motor is set in the opposite direction, so that they are inverse cycles to each other, so that the vibration angle reaches 90±5°. In the vibration at the time of no load, the vibrating body was set so as to have an amplitude of 1.10 [mm], a vibration frequency of 30 [Hz], an acceleration of 2.0 [G], and a vibration index of 35.8. In addition, the vibration is linear vibration, and the vibration angle is in the range of 90±5°. The tray is made of plastic, measures 110 cm in length and 110 cm in width, and weighs 10.4 kg.
[0437] Sampling and transportation were carried out in the same manner as in Experimental Example 1-1 to obtain a "filled particulate water-absorbing...
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