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A kind of water-oil two-soluble diamond grinding liquid and preparation method thereof

A water-oil two-soluble, diamond technology, applied in the field of polishing and precision grinding, can solve the problems of poor lubrication, low removal rate, difficult cleaning, etc., and achieve the effect of good lubricity, high surface finish and high grinding rate

Active Publication Date: 2017-12-01
HENAN UNION ABRASIVES
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

Although water-based abrasives are easy to clean and can currently produce a system with good suspension stability, their removal rate is low due to their poor lubricating effect, which is not conducive to the improvement of processing efficiency.
Although the removal rate of oil-based system is higher than that of water-based system, it is difficult to clean

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0027] A water-oil two-soluble diamond grinding liquid, prepared from the following raw materials in weight percentage: C16 isoparaffin 86.2%, stearic acid polyoxyethylene ether (5-10EO) 5%, oleic acid polyoxyethylene ether (2EO ) 5%, 2,6-di-tert-butyl mixed phenol 0.3%, 0.5 μm single crystal diamond powder 1.5%, and the balance is water.

[0028] (1) Mix the base oil, emulsifier, co-emulsifier and oil anti-aging agent evenly, then pour it into the reaction kettle, heat the reaction kettle, and heat it at 70°C for 10 minutes while stirring;

[0029] (2) Add the diamond abrasive into the water, put it in the ultrasonic wave and stir for 10 minutes, so that the diamond abrasive is evenly dispersed, and then take out the mixed solution;

[0030] (3) Slowly add the mixed solution dispersed with diamond abrasives into the reaction kettle, heat it at 70°C for 30 minutes under stirring conditions, and then lower it to room temperature under stirring conditions to obtain a water-oil t...

Embodiment 2

[0033] A water-oil two-soluble diamond grinding fluid, prepared from the following raw materials in weight percentage: C14 to C19 linear alkanes 79.6%, oleylamine polyoxyethylene ether (5-10EO) 4%, dodecylamine polyoxyethylene ether (5-10EO) 3%, stearic acid 2%, oleic acid 3%, 2,6-di-tert-butyl-2-dimethylamino-p-cresol 0.2%, 2.0 μm polycrystalline diamond powder 1.2%, the balance for water.

[0034] For the preparation method of the above-mentioned water-oil two-soluble diamond grinding liquid, refer to Example 1. The difference from Example 1 is that the heating time in step (1) is 20 minutes.

[0035] The viscosity of the water-oil two-soluble diamond grinding liquid prepared according to the above-mentioned method is 550cp as measured by a rotational viscometer, and the diamond abrasive has no obvious sedimentation phenomenon after being placed in the system for a long time. Polish 2-inch*6 sapphire wafers on a dedicated single-side grinding machine (AM company, model ASL-...

Embodiment 3

[0037] A water-oil two-soluble diamond grinding liquid is prepared from the following raw materials in weight percentage: C12 isoparaffin 80.0%, octadecylamine polyoxyethylene ether (5-10EO) 4%, lauric acid polyoxyethylene ether (5 -10EO) 3%, oleic acid diethanolamide 3%, cocoic acid diethanolamide 3%, 2,6-di-tert-butyl mixed phenol 0.3%, 3.0μm polycrystalline diamond micropowder 0.7%, the balance is water .

[0038]For the preparation method of the above-mentioned water-oil two-soluble diamond grinding liquid, refer to Example 1. The difference from Example 1 is that the heating time in step (1) is 15 minutes.

[0039] The viscosity of the water-oil two-soluble diamond grinding liquid prepared according to the above method is 400 cp measured by a rotational viscometer, and the diamond abrasive has no obvious sedimentation phenomenon after being placed in the system for a long time. Polish 2-inch*6 sapphire wafers on a dedicated single-side grinding machine (AM company, model...

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Abstract

The invention discloses water-soluble and oil-soluble diamond grinding liquid, and belongs to the field of precise finishing and polishing processing. The liquid is prepared by the following raw materials in percentages by weight: 54-87% of base oil, 5-15% of an emulsifier, 5-10% of a co-emulsifier, 0.1-1% of an anti-aging agent of oil products, 0.05-5% of a diamond abrasive, and the balance being water. The invention also discloses a preparation method of the water-soluble and oil-soluble diamond grinding liquid, and the method comprises the following steps: (1) the base oil, the emulsifier, the co-emulsifier and the anti-aging agent of oil products are mixed and poured into a reaction vessel, and heating is carried out with stirring at 70 DEG C for 10-20 minutes; (2) the diamond abrasive is added into water and placed in supersonic wave with stirring for 10 minutes, and mixed liquor is obtained; (3) the mixed liquor with dispersed diamond abrasive is slowly added into a reaction vessel, temperature is raised to 70 DEG C with stirring for 30 minutes, temperature is reduced to room temperature with stirring, and the water-soluble and oil-soluble diamond grinding liquid is obtained.

Description

technical field [0001] The invention belongs to the field of precision grinding and polishing processing, and in particular relates to a water-oil two-soluble diamond grinding fluid and a preparation method thereof. Background technique [0002] As the third-generation semiconductor material GaN after Si and GaAs, its application in devices is regarded as the most important event in semiconductors in the 1990s, which brought semiconductor light-emitting diodes and lasers to a new level. However, in In practical applications, GaN materials are difficult to produce, and thin films must be grown on other substrate materials. At present, there are many substrate materials for growing GaN materials, including sapphire, silicon carbide, silicon, magnesium oxide, etc., and sapphire is the most The main substrate material. [0003] The sapphire screen is artificially synthesized sapphire glass. Compared with the traditional glass display screen, the sapphire screen is harder and mo...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): C09K3/14
CPCC09K3/1463
Inventor 付存刘丹丹王森高礼明汪静
Owner HENAN UNION ABRASIVES
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