Unlock instant, AI-driven research and patent intelligence for your innovation.

A kind of nematocide microcapsule and preparation method thereof

A nematicide and microcapsule technology, which is applied in the field of nematicide microcapsules and its preparation, can solve the problem that decomposition products are not completely biologically active, limit the utilization rate and efficacy of nematicides, harm humans, animals and soil beneficial organisms, etc. It can reduce the number and frequency of pesticide application, save the amount of pesticides, and save the cost of prevention and control.

Active Publication Date: 2018-07-03
YANGZHOU UNIV
View PDF3 Cites 0 Cited by
  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

In addition, due to high toxicity and large residues, the use of non-fumigant nematicides such as aldicarb, isofenphos-methyl, and carbofuran on vegetables has been banned in China. Therefore, it is imperative to develop low-toxicity and high-efficiency nematicides Row
[0003] At present, the main dosage forms of using nematicides to control root-knot nematodes are emulsifiable concentrates and granules, which have a short duration of action and require repeated application, which is cumbersome to operate, increases the cost of control, and harms humans, animals, and beneficial organisms in the soil, polluting the environment; in addition, Nematicides are easy to decompose under the influence of ultraviolet light or soil environment (such as humic acid, microorganisms) and other factors, and the decomposition products are not fully biologically active, which limits the utilization rate and efficacy of nematicides

Method used

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
View more

Image

Smart Image Click on the blue labels to locate them in the text.
Viewing Examples
Smart Image
  • A kind of nematocide microcapsule and preparation method thereof
  • A kind of nematocide microcapsule and preparation method thereof
  • A kind of nematocide microcapsule and preparation method thereof

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0027] 1) Weigh 0.20g of the nematocide original drug, dissolve it in 6.00g of dichloromethane, stir until the original drug is completely dissolved, then add 0.25g of ethyl cellulose into the solution, stir until the ethyl cellulose is completely dissolved, and prepare into a clear solution A containing nematocide and ethylcellulose;

[0028] 2) Weigh 12.75g of deionized water into a beaker, add 0.80g of emulsifier EL-40, and then magnetically stir until the emulsifier is completely dissolved to make a transparent solution B containing emulsifier;

[0029] 3) Mix the transparent solution A obtained in step 1) with the transparent solution B obtained in step 2), and cut at high speed (10000 rpm) for 4 minutes with a high-speed shearing machine to obtain an emulsion;

[0030] 4) removing dichloromethane from the emulsion obtained in step 3) by a rotary evaporator at 40° C. to obtain a suspension containing microspheres;

[0031] 5) The microsphere-containing suspension obtaine...

Embodiment 2

[0033] 1) Weigh 0.20g of the nematocide original drug, dissolve it in 5.00g of dichloromethane, stir until the original drug is completely dissolved, then add 0.15g of ethyl cellulose into the solution, stir until the ethyl cellulose is completely dissolved, and prepare into a clear solution A containing nematocide and ethylcellulose;

[0034] 2) Weigh 13.85g of deionized water into a beaker, add 0.80g of emulsifier EL-40, and then magnetically stir until the emulsifier is completely dissolved to make a transparent solution B containing emulsifier;

[0035] 3) Mix the transparent solution A obtained in step 1) with the transparent solution B obtained in step 2), and cut at high speed (10000 rpm) for 6 minutes with a high-speed shearing machine to obtain an emulsion;

[0036] 4) removing dichloromethane from the emulsion obtained in step 3) by a rotary evaporator at 40° C. to obtain a suspension containing microspheres;

[0037] 5) The microsphere-containing suspension obtaine...

Embodiment 3

[0039] 1) Weigh 0.20g of nematocide original drug, dissolve it in 4.00g of dichloromethane, stir until the original drug is completely dissolved, then add 0.15g of ethyl cellulose to the solution, stir until the ethyl cellulose is completely dissolved, and prepare into a clear solution A containing nematocide and ethylcellulose;

[0040] 2) Weigh 15.25g of deionized water into a beaker, add 0.40g of emulsifier EL-40, and then magnetically stir until the emulsifier is completely dissolved to make a transparent solution B containing emulsifier;

[0041] 3) Mix the transparent solution A obtained in step 1) with the transparent solution B obtained in step 2), and cut at high speed (10000 rpm) for 4 minutes with a high-speed shearing machine to obtain an emulsion;

[0042] 4) removing dichloromethane from the emulsion obtained in step 3) by a rotary evaporator at 40° C. to obtain a suspension containing microspheres;

[0043] 5) The suspension obtained in step 4) is filtered, was...

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
Login to View More

PUM

No PUM Login to View More

Abstract

The invention discloses a nematicide microcapsule, which is prepared from the following raw materials in mass percentage: capsule core 0.5-1%, organic solvent 20-35%, wall material 0.5-2%, emulsifier 1-6%, Water 56-78%; the capsule core is a nematicide. The present invention adopts the easily degradable macromolecular substance in the environment as the capsule wall material of the microcapsule, and the material is easy to obtain and has good environmental compatibility. The organic solvent that is easy to be recycled and reused is selected and emulsified by a high-shear emulsifier. A new type of nematocide microcapsule with controlled release has been prepared. The nematicide has excellent long-lasting performance, has the characteristics of light resistance, acid and alkali resistance, slow release, etc., and saves control costs and has high economic value. The invention can prepare the nematocide microcapsules with different particle sizes by using the solvent evaporation method, the preparation process is simple to operate, the cycle is short, and the organic solvent can be recycled and reused.

Description

technical field [0001] The invention belongs to the technical field of pesticide preparation, in particular to a nematocide microcapsule and a preparation method thereof. Background technique [0002] Root-knot nematode is one of the most diverse and most harmful nematode species among plant pathogenic nematodes. Its hosts include crops, trees, flowers, vegetables, etc. 3000 kinds of plants, especially Solanaceae, Cucurbitaceae, Brassicaceae Vegetables are more seriously affected. Chemical control is the most effective control method for root-knot nematodes, and it is also the mainstay of comprehensive nematode control, while the fumigant nematicide methyl bromide is banned because it kills beneficial nematodes and destroys the ozone layer in the atmosphere. In addition, due to high toxicity and large residues, the use of non-fumigant nematicides such as aldicarb, isofenphos-methyl, and carbofuran on vegetables has been banned in China. Therefore, it is imperative to develo...

Claims

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
Login to View More

Application Information

Patent Timeline
no application Login to View More
Patent Type & Authority Patents(China)
IPC IPC(8): A01N25/28A01N25/04A01N57/32A01N57/12A01N43/90A01N51/00A01N43/88A01P5/00
CPCA01N25/04A01N25/28A01N43/88A01N43/90A01N51/00A01N57/12A01N57/32
Inventor 冯建国杨益众郁倩瑶钱坤孙陈铖杨关天
Owner YANGZHOU UNIV