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Preparing method and application of catalyst

A catalyst and additive technology, applied in chemical instruments and methods, physical/chemical process catalysts, chemical/physical processes, etc., can solve problems such as blanks, achieve unique components, simple production process, prolong thermal stability and service life Effect

Inactive Publication Date: 2016-07-27
张平
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0003] Catalysts are also needed in the production process of insulation materials. The participation of catalysts can greatly improve the high-temperature resistance of finished products, but the current market is basically blank for such high-temperature-resistant catalysts.

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment approach 1

[0023] Embodiment 1: A preparation method of a catalyst, the raw materials of the following parts by weight are prepared according to the following steps:

[0024] 50 parts of light rare earth raw ore powder including lanthanum and cerium

[0025] Including 30 parts of heavy rare earth raw ore powder of yttrium

[0026] Microsilica fume 32 parts

[0027] Zirconia 17 parts

[0028] Borax 20 parts

[0029] Boron nitride 1 part

[0030] Titanium carbide 0.2 part

[0031] Tantalum carbide 0.4 parts

[0032] Additive 1 part

[0033] Described additive is boric acid;

[0034] Preparation steps:

[0035] 1) Dry ball milling the additive for 2 hours;

[0036] 2) Put the ball-milled additives together with other materials into a double-cone mixer and mix them thoroughly, and the mixing time is 20 hours;

[0037] 3) Pass through a 200-mesh sieve, pack, and serve.

Embodiment approach 2

[0038] Embodiment 2: a method for preparing a catalyst, the raw materials in the following parts by weight are prepared according to the following steps:

[0039] 60 parts of light rare earth raw ore powder including lanthanum and cerium

[0040] Including 40 parts of heavy rare earth raw ore powder of yttrium

[0041] Microsilica fume 38 parts

[0042] Zirconia 19 parts

[0043] Borax 24 parts

[0044] Boron nitride 3 parts

[0045] Titanium carbide 0.3 parts

[0046] Tantalum carbide 1.5 parts

[0047] The additive is calcium fluoride;

[0048] Preparation steps:

[0049] 1) Dry ball milling the additive for 10 hours;

[0050] 2) Put the ball-milled additives together with other materials into a double-cone mixer and mix them thoroughly, and the mixing time is 40 hours;

[0051] 3) Pass through a 200-mesh sieve, pack, and serve.

Embodiment approach 3

[0052] Embodiment 3: a method for preparing a catalyst, the raw materials in the following parts by weight are prepared according to the following steps:

[0053] 55 parts of light rare earth raw ore powder including lanthanum and cerium

[0054] Including 35 parts of heavy rare earth raw ore powder of yttrium

[0055] Microsilica fume 35 parts

[0056] Zirconia 18 parts

[0057] 22 parts of borax

[0058] Boron nitride 2 parts

[0059] Titanium carbide 0.25 parts

[0060] Tantalum carbide 0.45 parts

[0061] Additive 1.3 parts

[0062] The additives are half of strontium fluoride and half of aluminum fluoride;

[0063] Preparation steps:

[0064] 1) Dry ball milling the additive for 6 hours;

[0065] 2) Put the ball-milled additives together with other materials into a double-cone mixer and mix them thoroughly, and the mixing time is 30 hours;

[0066] 3) Pass through a 200-mesh sieve, pack, and serve.

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PUM

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Abstract

The invention relates to a preparing method and application of a catalyst. The catalyst comprises, by weight, 50-60 parts of raw light-rare-earth mineral powder containing lanthanum and cerium, 30-40 parts of raw heavy-rare-earth mineral powder containing yttrium, 32-38 parts of micro silicon powder, 17-19 parts of zirconium oxide, 20-24 parts of sodium borate, 1-3 parts of boron nitride, 0.2-0.3 part of titanium carbide, 0.4-0.5 part of tantalum carbide and 1-1.5 parts of addition agent; the addition agent is one or several of boric acid, strontium fluoride, calcium fluoride and aluminum fluoride. The preparing method includes the following steps that 1, the addition agent is subjected to dry ball grinding for 2 h-10 h; 2, the addition agent subjected to dry ball grinding and other materials are put into a bi-conical mixing machine to be fully mixed, and the mixing time is 20 h-40 h; 3, the mixture is screened through a 200-mesh screen and packaged, and the catalyst is obtained. Compared with the prior art, the catalyst is unique in component and simple in production technology; as rare earth elements are adulterated, the activity of the catalyst can be enhanced, the heat stability of the finished product can be improved, and the service life of the finished product can be prolonged.

Description

technical field [0001] The invention relates to a composition, in particular to a preparation method and application of a catalyst. Background technique [0002] In a chemical reaction, a substance that can change the chemical reaction rate of the reactant (both increase and decrease) without changing the chemical balance, and whose quality and chemical properties do not change before and after the chemical reaction is called a catalyst (a solid catalyst is also called a catalyst). called catalyst). According to statistics, more than 90% of industrial processes use catalysts, such as chemical, petrochemical, biochemical, and environmental protection. There is also a saying that a catalyst is involved in a chemical reaction. In a general chemical reaction, the role of the catalyst is to reduce the activation energy required for the reaction to occur, essentially turning a relatively difficult reaction into two easily occurring chemical reactions (the opposite is called inh...

Claims

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Application Information

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IPC IPC(8): B01J27/24
CPCB01J27/24
Inventor 张平
Owner 张平
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