Lubricating grease for rims of locomotives and method for preparing lubricating grease

A technology for railway locomotives and lubricating grease, applied in the field of lubricating grease, can solve the problems of unsatisfactory low temperature performance, no biodegradability, and extreme pressure anti-wear agent is not easy to degrade, etc. Degradable, fine-looking effect

Active Publication Date: 2016-08-31
JIANGSU LOPALTECH
View PDF5 Cites 8 Cited by
  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

There are few domestic reports on lubricating grease for railway locomotive wheels. Most of them are made of mineral oil as base oil, fatty acid mixed lithium soap as thickener and various additives. The low temperature performance cannot meet the requirements, and it has no reliable Biodegradable, polluting the environment
The patent number is CN103013627, the invention titled "a biodegradable lubricating grease for locomotive rims and its preparation method", discloses the use of lithium soap or calcium soap to thicken ester oil and vegetable oil, and adds a variety of additives, not only The high temperature resistance and oxidation resistance are poor, and the selected extreme pressure antiwear agent is not easy to degrade, which will still cause pollution to the environment. At present, domestic products of this kind mainly rely on imports, and the price is relatively high.

Method used

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
View more

Image

Smart Image Click on the blue labels to locate them in the text.
Viewing Examples
Smart Image
  • Lubricating grease for rims of locomotives and method for preparing lubricating grease
  • Lubricating grease for rims of locomotives and method for preparing lubricating grease
  • Lubricating grease for rims of locomotives and method for preparing lubricating grease

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0023] Raw material composition: base oil (polyα-olefin synthetic base oil and trimethylolpropane oleate) 58.55%, high alkali value synthetic calcium sulfonate 28.5%, 12-alkylbenzenesulfonic acid 1.5%, isopropanol 1.2 %, water 3%, acetic acid 0.4%, calcium hydroxide 1.84%, 12-hydroxystearic acid 2.01%, boric acid 2.51% and diphenylamine 0.5%, wherein the kinematic viscosity of the base oil at 40°C is 32mm 2 / s, the alkali value of high alkali value synthetic calcium sulfonate is 400mgKOH / g, and its kinematic viscosity at 40°C is 235mm 2 / s, and the pour point is -34°C.

[0024] Preparation:

[0025] (1) 18kg of polyalpha-olefin synthetic base oil PAO-6, 28.5kg of high alkali value synthetic calcium sulfonate, 1.5kg12-alkylbenzenesulfonic acid and 3kg of water are dropped into successively with heat transfer oil jacket heating, Mix in a 200L stainless steel airtight reactor with two-way paddles, and heat to 75°C to prepare the mixture;

[0026] (2) Add 1.2kg of isopropanol a...

Embodiment 2

[0030] Raw material composition: base oil (natural gas synthetic oil GTL100 and dioctyl sebacate) 58.63%, high alkali value synthetic calcium sulfonate 26.5%, 12-alkylbenzenesulfonic acid 1.62%, isopropanol 1.3%, water 3.5% %, 0.5% phosphoric acid, 2% calcium hydroxide, 2.2% 12-hydroxystearic acid, 2.75% boric acid and 1% phenyl-α-naphthylamine, wherein the kinematic viscosity of the base oil at 40°C is 20mm 2 / s, the alkali value of high alkali value synthetic calcium sulfonate is 400mgKOH / g, and its kinematic viscosity at 40°C is 235mm 2 / s, and the pour point is -34°C.

[0031] Preparation:

[0032] (1) Put 13kg of natural gas synthetic oil GTL100, 26.5kg of high alkali value synthetic calcium sulfonate, 1.62kg of 12-alkylbenzenesulfonic acid and 3.5kg of water into the 200L bidirectional paddle heated by heat transfer oil jacket Mix in a stainless steel airtight reaction kettle and heat to 80°C to prepare the mixture;

[0033] (2) Add 1.3kg of isopropanol and 0.5kg of ph...

Embodiment 3

[0037] The raw material composition is: base oil (natural gas synthetic oil GTL250 and dioctyl sebacate) 67.8%, high alkali value synthetic calcium sulfonate 21%, 12-alkylbenzenesulfonic acid 1.06%, isopropanol 1%, water 2.5%, 0.5% acetic acid, 1.3% calcium hydroxide, 1.45% 12-hydroxystearic acid, 1.8% boric acid and 1.5% phenyl-α-naphthylamine, wherein the kinematic viscosity of the base oil at 40°C is 28mm 2 / s, the alkali value of high alkali value synthetic calcium sulfonate is 400mgKOH / g, and its kinematic viscosity at 40°C is 235mm 2 / s, and the pour point is -34°C.

[0038] Preparation:

[0039] (1) Put 10.5kg of natural gas synthetic oil GTL250, 21.0kg of high alkali value synthetic calcium sulfonate, 1.06kg of 12-alkylbenzenesulfonic acid and 2.5kg of water in turn into the two-way paddle with heat transfer oil jacket heating Mix in a 200L stainless steel airtight reactor and heat to 80°C;

[0040] (2) Add 1.0kg of isopropanol and 0.5kg of acetic acid to the above ...

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
Login to view more

PUM

PropertyMeasurementUnit
pour pointaaaaaaaaaa
pour pointaaaaaaaaaa
pour pointaaaaaaaaaa
Login to view more

Abstract

The invention discloses lubricating grease for rims of locomotives and a method for preparing the lubricating grease. The lubricating grease comprises base oil, high-alkali-value synthetic sulfonate, alkyl benzene sulfonic acid, 12-hydroxy stearic acid, antioxidants and the like. The method includes mixing the high-alkali-value synthetic sulfonate, the alkyl benzene sulfonic acid, water and a part of the base oil with one another to obtain mixtures, heating the mixtures and then adding isopropyl alcohol and inorganic acid into the mixtures to obtain gel; adding calcium hydroxide emulsion and boric acid solution into the gel, carrying out reaction to obtain reaction products and dehydrating the reaction products; adding another part of the base oil and the 12-hydroxy stearic acid into the reaction products and carrying out reaction; adding the remaining base oil and the antioxidants into the reaction products to obtain the lubricating grease. The lubricating grease and the method have the advantages that the lubricating grease is excellent in high-temperature resistance, low-temperature resistance, low-temperature pumpability, fog forming property, extreme-pressure abrasion resistance, water resistance, adhesion and antirust property; the required content of the high-alkali-value synthetic sulfonate required for preparing the lubricating grease by the aid of the method is reduced by approximately 5% as compared with existing lubricating grease, with the consistency identical to the consistency of the lubricating grease, prepared by the aid of an existing method, and the low-temperature flowability and the fog forming performance of the lubricating grease can be greatly improved.

Description

technical field [0001] The invention belongs to the field of lubricating grease, in particular to a lubricating grease for railway locomotive rims and a preparation method thereof. Background technique [0002] When the train is running, because the train is tilted during operation, the wheel rim is in contact with the inner side of the rail, resulting in frequent friction. Especially when the train is running on a curved road section, due to centrifugal force, the wheels are squeezed to the rails, causing severe friction between the inner surface of the rails and the wheel rims and severe wear, shortening the service life of the rails and wheels. Lubricating rails and wheels with wheel rim lubricants is the most effective way to reduce friction between wheel rims and rails, reduce locomotive power loss, improve wheel-rail interaction and reduce wheel-rail wear. [0003] According to the characteristics of the wheel flange lubrication, the wheel flange grease should have th...

Claims

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
Login to view more

Application Information

Patent Timeline
no application Login to view more
Patent Type & Authority Applications(China)
IPC IPC(8): C10M169/04C10N30/06C10N30/08C10N30/12
CPCC10M169/045C10M2201/062C10M2201/085C10M2201/087C10M2205/0206C10M2207/021C10M2207/122C10M2207/144C10M2207/2825C10M2207/2835C10M2215/064C10M2219/044C10M2219/046C10N2030/06C10N2030/08C10N2030/12C10N2030/26C10N2030/76C10N2020/02C10N2010/04
Inventor 杨操
Owner JIANGSU LOPALTECH
Who we serve
  • R&D Engineer
  • R&D Manager
  • IP Professional
Why Eureka
  • Industry Leading Data Capabilities
  • Powerful AI technology
  • Patent DNA Extraction
Social media
Try Eureka
PatSnap group products