Lubricating grease for railway locomotive wheel rim and preparation method thereof
A railway locomotive and lubricating grease technology, which is applied in the field of lubricating grease, can solve the problems of extreme pressure and anti-wear agents that are not easy to degrade, do not have biodegradability, and low-temperature performance cannot meet the requirements, and achieve superior biodegradability and appearance Delicate, friction-reducing effect
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Embodiment 1
[0023] Raw material composition: base oil (polyα-olefin synthetic base oil and trimethylolpropane oleate) 58.55%, high alkali value synthetic calcium sulfonate 28.5%, 12-alkylbenzenesulfonic acid 1.5%, isopropanol 1.2 %, water 3%, acetic acid 0.4%, calcium hydroxide 1.84%, 12-hydroxystearic acid 2.01%, boric acid 2.51% and diphenylamine 0.5%, wherein the kinematic viscosity of the base oil at 40°C is 32mm 2 / s, the alkali value of high alkali value synthetic calcium sulfonate is 400mgKOH / g, and its kinematic viscosity at 40°C is 235mm 2 / s, and the pour point is -34°C.
[0024] Preparation:
[0025] (1) 18kg of polyalpha-olefin synthetic base oil PAO-6, 28.5kg of high alkali value synthetic calcium sulfonate, 1.5kg12-alkylbenzenesulfonic acid and 3kg of water are dropped into successively with heat transfer oil jacket heating, Mix in a 200L stainless steel airtight reactor with two-way paddles, and heat to 75°C to prepare the mixture;
[0026] (2) Add 1.2kg of isopropanol a...
Embodiment 2
[0030] Raw material composition: base oil (natural gas synthetic oil GTL100 and dioctyl sebacate) 58.63%, high alkali value synthetic calcium sulfonate 26.5%, 12-alkylbenzenesulfonic acid 1.62%, isopropanol 1.3%, water 3.5% %, 0.5% phosphoric acid, 2% calcium hydroxide, 2.2% 12-hydroxystearic acid, 2.75% boric acid and 1% phenyl-α-naphthylamine, wherein the kinematic viscosity of the base oil at 40°C is 20mm 2 / s, the alkali value of high alkali value synthetic calcium sulfonate is 400mgKOH / g, and its kinematic viscosity at 40°C is 235mm 2 / s, and the pour point is -34°C.
[0031] Preparation:
[0032] (1) Put 13kg of natural gas synthetic oil GTL100, 26.5kg of high alkali value synthetic calcium sulfonate, 1.62kg of 12-alkylbenzenesulfonic acid and 3.5kg of water into the 200L bidirectional paddle heated by heat transfer oil jacket Mix in a stainless steel airtight reaction kettle and heat to 80°C to prepare the mixture;
[0033] (2) Add 1.3kg of isopropanol and 0.5kg of ph...
Embodiment 3
[0037] The raw material composition is: base oil (natural gas synthetic oil GTL250 and dioctyl sebacate) 67.8%, high alkali value synthetic calcium sulfonate 21%, 12-alkylbenzenesulfonic acid 1.06%, isopropanol 1%, water 2.5%, 0.5% acetic acid, 1.3% calcium hydroxide, 1.45% 12-hydroxystearic acid, 1.8% boric acid and 1.5% phenyl-α-naphthylamine, wherein the kinematic viscosity of the base oil at 40°C is 28mm 2 / s, the alkali value of high alkali value synthetic calcium sulfonate is 400mgKOH / g, and its kinematic viscosity at 40°C is 235mm 2 / s, and the pour point is -34°C.
[0038] Preparation:
[0039] (1) Put 10.5kg of natural gas synthetic oil GTL250, 21.0kg of high alkali value synthetic calcium sulfonate, 1.06kg of 12-alkylbenzenesulfonic acid and 2.5kg of water in turn into the two-way paddle with heat transfer oil jacket heating Mix in a 200L stainless steel airtight reactor and heat to 80°C;
[0040] (2) Add 1.0kg of isopropanol and 0.5kg of acetic acid to the above ...
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