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Method and device for producing high-strength and high-conductivity graphene copper-based powder material

A powder material, copper-based technology, applied in the field of preparation of new functional powder materials, can solve the problems of inability to solve the dispersion and compatibility of two-phase materials, great influence on the quality of later products, unsuitable for large-scale production, etc. , to achieve the effects of excellent electrical/thermal conductivity and mechanical properties, good light transmittance, and excellent comprehensive performance

Active Publication Date: 2016-09-28
SPECIAL EQUIP SAFETY SUPERVISION INSPECTION INST OF JIANGSU PROVINCE
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  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0006] The above-mentioned technical means for obtaining graphene / copper-based composite materials can be divided into two categories. One is to physically blend copper powder and graphene materials, and then perform corresponding post-processing to obtain composite materials. This technical route is still not available. Solve the problem of good dispersion and compatibility between two-phase materials; the other is to pre-treat copper powder, and then grow graphene to obtain composite materials. This technical route better solves the problem of two-phase materials. Excellent dispersion and compatibility, but the pretreatment of copper powder is complicated and time-consuming, and the quality of pretreatment has a great impact on the quality of later products, so it is not suitable for large-scale production

Method used

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  • Method and device for producing high-strength and high-conductivity graphene copper-based powder material
  • Method and device for producing high-strength and high-conductivity graphene copper-based powder material
  • Method and device for producing high-strength and high-conductivity graphene copper-based powder material

Examples

Experimental program
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Effect test

Embodiment 1

[0043] Such as figure 1 As shown, the device for producing high-strength and high-conductivity graphene copper-based powder materials provided by this embodiment includes a gas atomization powder making device, an air inlet device, a gas scrubbing device 15, a step-by-step temperature control device and a material speed reduction device 10 ;

[0044] Wherein, the gas atomization powder making device includes a high-pressure gas source system and a smelting chamber 3, an atomization chamber 6, and a collector 16 connected sequentially from top to bottom, and a crucible 4 is arranged inside the smelting chamber 3, and the crucible 4 A nozzle 5 for spraying liquid into the atomization chamber 6 is provided at the bottom, the high-pressure gas source system includes a high-pressure inert gas source 1 and a high-pressure inert gas source pressure regulating valve 2 for controlling the high-pressure inert gas source 1, and the high-pressure gas source system The inert gas source 1 ...

Embodiment 2

[0050] Such as figure 1 As shown, firstly, the air in the atomization chamber 6 and the collector 16 is drawn out through the gas scrubber 15; secondly, the argon gas source 13 and its pressure regulating valve 14 are opened to replenish the air in the atomization chamber 6 and the collector 16. Pure argon; the 3rd, repeat above-mentioned steps no less than three times, the air replacement in atomizing chamber 6 and collector 16 is clean; select methane) and its corresponding pressure regulating valve 14 to keep hydrogen entering the atomization chamber 6 with a flow of 300 sccm and methane at a flow rate of 20 sccm, and maintain the dynamic balance of the mixed gas through the scrubber 15; The 5kg copper material in 4 is heated to 1100°C for melting, and at the same time, the heating controller 9 is turned on to heat the resistance wire 6 to realize the temperature gradient of 1080°C, 950°C and 850°C from top to bottom of the heat radiation plate 8 and the atomization chamber...

Embodiment 3

[0053] The air pressure of the high-pressure inert gas source is different from the air flow and the diameter flow of the nozzle metal liquid, and the size of the gas atomized metal particles produced will also be different. Therefore, in order to obtain copper powder of different sizes, the air pressure and flow rate of the inert gas source can be adjusted. And choose different nozzle metal liquid diameter. If the basic steps described in Example 2 are adopted, the difference is that the high-pressure inert gas source 1 and the high-pressure inert gas source pressure regulating valve 2 are opened, and the gas pressure of 0.7MPa and 2m 3 The gas flow rate per minute enters the nozzle 5 with a diameter of 4mm of molten metal, sprays the molten high-temperature liquid copper into the atomization chamber 6, and obtains a graphene copper-based powder composite material with a larger particle equivalent diameter.

[0054] Gained graphene copper-based powder composite material Raman...

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Abstract

The invention provides a preparation method and device for producing a high-strength and high-conductivity graphene copper-based powder composite. The preparation method is characterized in that a melt copper gas atomizing type powder preparation technology is adopted, a multi-gas-channel controllable gas feeding system and a controllable gas scrubbing device are additionally arranged at the outer part of an atomizing chamber of a traditional powder preparation device, and a gradual temperature control device and a material speed reduction device are additionally arranged in the atomizing chamber, and on that basis, high-temperature melt copper can be atomized into fine high-temperature melt copper droplets under the impacting effect of high-speed gas flow, and then the high-temperature melt copper droplets enter an atomizing chamber atmosphere containing carbon source gas components with a certain ratio, thus a graphene material can realize in-situ wrapping growth on the surfaces of copper powder particles when the atomized melt copper droplets are subjected to temperature-controlled solidification and / or under the speed reduction effect of the material speed reduction device, and as a result, the high-strength and high-conductivity graphene copper-based powder composite can be obtained. The preparation method and the preparation device can be directly applied to an existing copper-based material atomizing type powder preparation industry; the prepared product is high in performance and additional value; the preparation method and the preparation device are applicable to technology improvement and product upgrading of a copper powder production industry.

Description

technical field [0001] The invention belongs to the technical field of preparation of novel functional powder materials, and in particular relates to a method and a device for producing graphene copper-based powder composite materials with high strength, high thermal conductivity and high conductivity. Background technique [0002] As a basic industrial material, copper powder is widely used in the world's auto industry parts, heat dissipation modules, electronic appliances, friction materials, conductive inks, oil bearings, electrical appliances, etc. Contact materials, electric carbon products, chemical contacts, diamond tools, filters, mechanical parts processing, electrical alloys and other fields, quasi-spherical and spherical copper powders are used in injection molding, welding materials, electronic material production fields, and play an important role in industrial production. play an important role. [0003] Due to reasons such as energy consumption and environmen...

Claims

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Application Information

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IPC IPC(8): B22F9/08B22F1/02
CPCB22F9/082B22F2009/086B22F2009/0844B22F1/16
Inventor 杨永强王勤生刘峥邓宏康孙小伟百坚毅金玲熊立斌
Owner SPECIAL EQUIP SAFETY SUPERVISION INSPECTION INST OF JIANGSU PROVINCE
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