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Gold-bearing viscose and preparation method thereof

A viscose fiber, gold-loading technology, applied in fiber processing, medical science, absorbent pads, etc., can solve the problems of difficult control of nano-silver agglomeration, nano-silver oxidation, discoloration, application safety problems, etc., and achieve good reducibility and safety. Stability, stable solution properties, good biocompatibility

Inactive Publication Date: 2016-10-26
SUZHOU UNIV
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0004] 1. As the main raw material for preparing silver-loaded antibacterial dressings, the preparation method of nano-silver solution is complicated, and it is often necessary to add suitable reducing agents, stabilizers and dispersants. Even so, the agglomeration of nano-silver is still difficult to control, and the particles of nano-silver uneven size;
[0005] 2. During the processing of traditional nano-silver solutions used in medical dressings, the affinity between nano-silver particles and fiber materials is weak, and they often only rely on drying for fixation or need to select appropriate cross-linking agents and adhesives to fix nano-silver antibacterial agents on the surface. However, the application of these stabilizers, dispersants, cross-linking agents and adhesives will not only affect the feel and air permeability of medical dressings, but also bring potential application safety problems
[0007] 4. Nano silver is prone to oxidation and discoloration during use, which will affect the use effect
[0008] 5. Some people are prone to allergies to silver antibacterial materials
[0009] At present, there is no report on the related technology of gold-loaded viscose fiber, and the development of gold-loaded viscose fiber will expand the application range of nano-antibacterial materials

Method used

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Examples

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Effect test

Embodiment 1

[0025] A method for preparing a nano-gold solution. The specific steps are: dissolving 5g of β-cyclodextrin powder in 95g of deionized water, the temperature of the aqueous solution is 80°C, and stirring for 6 hours at 200 rpm until a transparent β-cyclodextrin is obtained. Fine aqueous solution; add 2g of sodium chloride powder into the β-cyclodextrin aqueous solution, continue stirring for 0.5h until the sodium chloride powder is completely dissolved; then add 0.5g of tetrachloroauric acid into the β-cyclodextrin containing sodium chloride In the aqueous solution, after stirring for 5 minutes to dissolve, insert the positive and negative electrodes of a DC power supply with a current of 0.5A and a voltage of 10V into the solution, increase the stirring speed to 1000 rpm, and put the prepared solution into a centrifuge after reacting for 2 hours After centrifuging for 10 min at 1000 rpm, impurities were removed to prepare a nano-gold solution.

[0026] Take 5 g of washed visc...

Embodiment 2

[0028] A method for preparing a nano-gold solution, the specific steps are: select 10g of β-cyclodextrin powder and dissolve it in 90g of deionized water, the temperature of the aqueous solution is 90°C, and stir at 400 rpm for 6 hours until a transparent β-cyclodextrin is obtained Fine aqueous solution; add 5g of sodium chloride powder into the β-cyclodextrin aqueous solution, and continue to stir for 1 hour until the sodium chloride powder is completely dissolved; then add 0.8g of tetrachloroauric acid into the β-cyclodextrin aqueous solution containing sodium chloride After stirring for 5 minutes to dissolve, insert the positive and negative electrodes connected to the DC power supply into the solution, adjust the current to 0.01-1A, the voltage to 5-30V, increase the stirring speed to 1500 rpm, and react for 4 hours. Put it into a centrifuge, centrifuge at 1000 rpm for 10 minutes, and then remove impurities to prepare a nano-gold solution.

[0029] Take 5 g of washed visco...

Embodiment 3

[0031] A method for preparing a nano-gold solution, the specific steps are: select 2g of β-cyclodextrin powder and dissolve it in 98g of deionized water, the temperature of the aqueous solution is 80°C, and stir at 200 rpm for 6 hours until a transparent β-cyclodextrin is obtained Fine aqueous solution; add 1g of sodium chloride powder into the β-cyclodextrin aqueous solution, continue stirring for 0.5h until the sodium chloride powder is completely dissolved; then add 0.2g of tetrachloroauric acid into the β-cyclodextrin containing sodium chloride In the aqueous solution, after stirring for 5 minutes to dissolve, insert the positive and negative electrodes connected to the DC power supply into the solution, adjust the current to 0.5A, the voltage to 5-30V, increase the stirring speed to 1000 rpm, and react for 2 hours. Put it into a centrifuge, centrifuge at 1000 rpm for 10 minutes, and then remove impurities to prepare a nano-gold solution.

[0032] Take 5 g of washed viscos...

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Abstract

The invention discloses gold-bearing viscose and a preparation method thereof. The preparation method comprises the following steps: dissolving beta-cyclodextrin in a water solution, then adding sodium chloride and hydrogen tetrachloroaurate hydrate, then inserting positive and negative electrodes connected with a direct current power supply in the solution and carrying out high speed stirring, thus preparing a nanogold solution; putting cleaned viscose in the nanogold solution to undergo dipping treatment, thus preparing the gold-bearing viscose. The method is simple in process, low in impurity content and firm in bonding between nanogold and the viscose. The gold-bearing viscose has excellent antibacterial properties.

Description

technical field [0001] The invention belongs to the technical field of nanomaterial preparation, and in particular relates to a gold-loaded viscose fiber and a preparation method thereof. Background technique [0002] Clinically, wounds are susceptible to infection and difficult to heal, which is caused by the rapid reproduction of pathogens such as Staphylococcus aureus, Candida albicans, and Escherichia coli in a warm and humid environment on the surface of the wound. To control wound bacterial growth and prevent wound infection, a variety of antimicrobial materials are commonly used to assist in controlling hemostasis, protect wounds, reduce infection, absorb secretions, maintain body temperature, and promote wound healing. [0003] Currently used mainly nano-silver antibacterial materials, such as the invention patent "Preparation method of a polysaccharide nano-silver colloidal solution" discloses a method of using polydextrose aqueous solution to prepare nano-silver an...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): D06M15/03D06M11/83A61L15/46A61L15/28D06M101/32
CPCD06M15/03A61L15/28A61L15/46A61L2300/102A61L2300/60A61L2300/802D06M11/83D06M2101/32C08L1/24
Inventor 王成陈宇岳姚理荣林红
Owner SUZHOU UNIV
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