Preparation method of okra colored viscose fiber and obtained leisure wear
A technology of viscose fiber and okra, which is applied in the field of preparation of okra colored viscose fiber, can solve the problems of unbalanced optimal harvesting time and loss of farmers, and achieve excellent mechanical properties, avoid skin damage, and improve comfort Effect
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Embodiment 1
[0029] Prepare okra colored viscose fiber 1, following steps:
[0030] Step 1. Preparation: Take 200 kg of okra 17 days after flowering and put it in boiling water for 20 minutes, take it out and dry it at 70°C, grind it into 30-mesh okra powder, add it to the same mass fraction as the okra powder with a mass fraction of 60 % ethanol aqueous solution, after soaking for 30min, dry at 50°C, add 1 times the mass fraction of okra powder to 5% CuSO4 aqueous solution, soak at 40-50°C for 20-30min, then dry at 50°C Dry, wash with water to remove residual copper sulfate, filter, and dry at 50°C again to obtain 38.1kg of secondary okra powder;
[0031] Step 2, preparing nanofibers: put the secondary okra powder obtained in step 1 into a ball mill and add a mass fraction of 1.2% dihydrolipoic acid aqueous solution to grind for 25 hours. The quality of the dihydrolipoic acid aqueous solution is six times that of the okra powder. 12 hours to obtain nanofiber powder with a particle size o...
Embodiment 2
[0043] Prepare okra colored viscose fiber 2, following steps:
[0044] Step 1. Preparation: Take 200 kg of okra 20 days after flowering and put it in boiling water for 30 minutes, take it out and dry it at 50°C, grind it into 50-mesh okra powder, add it to the same mass fraction as the okra powder with a mass fraction of 60 % ethanol aqueous solution, after soaking for 30min, dry at 60°C, add 5% CuSO4 aqueous solution whose mass fraction is 2 times that of okra powder, soak at 40°C for 30min, then dry at 50°C, wash with water to remove Copper sulfate residue, filter, and dry again at 50°C to obtain 39.4kg of secondary okra powder;
[0045] Step 2, preparing nanofibers: put the secondary okra powder obtained in step 1 into a ball mill and add a mass fraction of 1% dihydrolipoic acid aqueous solution to grind for 20 hours. The quality of the dihydrolipoic acid aqueous solution is four times that of the okra powder. 12 hours to obtain nanofiber powder with a particle size of 20-...
Embodiment 3
[0057] Prepare okra colored viscose fiber 3, following steps:
[0058] Step 1. Preparation: Take 200 kg of okra 15 days after flowering and put it in boiling water for 10 minutes, take it out and dry it at 80°C, grind it into 50-mesh okra powder, add it to the same mass fraction as the okra powder with a mass fraction of 60 % ethanol aqueous solution, after soaking for 30min, dry at 60°C, add 1 times the mass fraction of okra powder to 5% CuSO4 aqueous solution, soak at 40°C for 30min, then dry at 50°C, and wash to remove Copper sulfate remains overnight, filtered, and dried at 50°C again to obtain 36.1kg of secondary okra powder;
[0059] Step 2, preparing nanofibers: put the secondary okra powder obtained in step 1 into a ball mill and add a mass fraction of 2% dihydrolipoic acid aqueous solution to grind for 30 hours. The quality of the dihydrolipoic acid aqueous solution is four times that of the okra powder. 12 hours to obtain nanofiber powder with a particle size of 20-...
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