Method for fast low-temperature growing of various graphical three-dimensional graphenes
A graphene and patterning technology, which is applied in the field of rapid growth of various types of patterned three-dimensional graphene at low temperature and three-dimensional graphene production, can solve the problems of complicated steps, complicated technical process, unfavorable large-scale production, etc., and achieves simple steps. Effect
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Embodiment 1
[0022] This embodiment provides a method for rapidly growing various types of patterned three-dimensional graphene at low temperature. The flowchart of the method is as attached figure 1 As shown, the specific steps are as follows:
[0023] (1) Make mask pattern: choose a 6cm×6cm size copper plate as the base material of the mask, and use casting technology to make the following figure 2 The long strip mask pattern shown;
[0024] (2) Fix the mask and the growth substrate: select a silicon substrate with the same size of 6cm×6cm as the substrate for growing three-dimensional graphene, and cover the patterned mask on the growth substrate to fix the two;
[0025] (3) Low-temperature growth of three-dimensional graphene: Place the fixed mask and growth substrate in a microwave CVD vacuum chamber, vacuum with a mechanical pump to a pressure of 10 mbar, pass in hydrogen gas at a flow rate of 30 sccm, and then use argon gas carrier Enter the carbon source, the carbon source is ethanol, th...
Embodiment 2
[0027] This embodiment provides a method for rapidly growing various types of patterned three-dimensional graphene at low temperature. The flowchart of the method is as attached figure 1 As shown, the specific steps are as follows:
[0028] (1) Making the mask pattern: choose a nickel plate with a size of 5cm×5cm as the mask substrate, and use laser direct writing technology to make a petal-shaped mask pattern on the nickel plate;
[0029] (2) Fix the mask and the growth substrate: select a quartz substrate with a size of 5cm×5cm as the substrate for growing three-dimensional graphene, and cover the patterned mask on the growth substrate to fix the two;
[0030] (3) Low-temperature growth of three-dimensional graphene: place the fixed mask and growth substrate in a microwave CVD vacuum chamber, vacuum with a mechanical pump to a pressure of 50 mbar, and pass in hydrogen gas at a flow rate of 80 sccm, and then use argon gas carrier Enter the carbon source, the carbon source is methane...
Embodiment 3
[0032] This embodiment provides a method for rapidly growing various types of patterned three-dimensional graphene at low temperature. The flowchart of the method is as attached figure 1 As shown, the specific steps are as follows:
[0033] (1) Making the mask pattern: Choose a ceramic material with a size of 4cm×4cm as the base material of the mask, and use the molding technology to make a square mask pattern on the nickel plate;
[0034] (2) Fix the mask and the growth substrate: choose a copper plate with a size of 4cm×4cm as the substrate for growing three-dimensional graphene, and place the patterned mask on the growth substrate to fix the two;
[0035] (3) Low-temperature growth of three-dimensional graphene: Place the fixed mask and growth substrate in a microwave CVD vacuum chamber, vacuum with a mechanical pump to a pressure of 100 mbar, pass in hydrogen gas at a flow rate of 100 sccm, and then use argon gas carrier Enter the carbon source, the carbon source is ethylene, the...
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