Preparing method for yellow paint
A yellow pigment and diazo technology, applied in chemical instruments and methods, coupling reaction of azo dyes, azo dyes, etc., can solve the problems of high oil absorption, low tinting strength, high color strength, etc., and achieve low oil absorption , strong tinting power, and the effect of improving transparency
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Embodiment 2
[0009] Embodiment 2, a preparation method of a yellow pigment, comprising the following steps: the following kg numbers are mass kg numbers, 1, put 1500 kg of water in the diazo tank, add 225 kg of hydrochloric acid, add 3,3'-dichlorobis Aniline hydrochloride 150kg, beating for 30 minutes and cooling down to 0°C, quickly adding solid sodium nitrite, reacting for 1 hour, until the starch-potassium iodide test paper is slightly blue, PH≦1, temperature 3°C; 2, add 2000kg of water to the dissolution tank , add 175 kg of liquid caustic soda, add 223 kg of N-acetylacetanilide and 0.6 kg of PMP, stir for 60 minutes, and dissolve transparently; 3, add 300 kg of water in the auxiliary material tank, heat up to 70 ° C, add 25 kg of quaternary ammonium salt, and dissolve until it is clear and transparent; 4, add 300kg of water to the rosin bucket, add 20kg of sodium hydroxide to boil, then add 30kg of disproportionated rosin, and add 5kg of hyperdispersant until it is clear and transparen...
Embodiment 3
[0010] Embodiment 3, a preparation method of a yellow pigment, comprising the following steps: the following kg numbers are mass kg numbers, 1, put 1500 kg of water in the diazo bucket, add 225 kg of hydrochloric acid, add 3,3`-dichlorobis Aniline hydrochloride 150kg, beating for 30 minutes, cooling down to -1°C, quickly adding solid sodium nitrite, reacting for 1 hour, until the starch-potassium iodide test paper is slightly blue, PH≦1, temperature 2°C; 2, add water to the dissolution tank 2000kg, add 175kg of liquid caustic soda, add 223 kg of N-acetylacetanilide and 0.6kg of PMP, stir for 50 minutes, and dissolve transparently; 3, add 300kg of water to the auxiliary material tank, heat up to 70°C, add 25kg of quaternary ammonium salt, 4. Add 300kg of water to the rosin bucket, add 20kg of sodium hydroxide to boil, then add 30kg of disproportionated rosin, and add 5kg of hyperdispersant after it is clear and transparent; 5. Add it to the coupling bucket 1000kg of water, add ...
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